The Multinuclear Approach To Nmr Spectroscopy

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The Multinuclear Approach to NMR Spectroscopy

Author : J.B. Lambert
Publisher : Springer Science & Business Media
ISBN 13 : 9400971303
Total Pages : 552 pages
Book Rating : 4.4/5 (9 download)

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Book Synopsis The Multinuclear Approach to NMR Spectroscopy by : J.B. Lambert

Download or read book The Multinuclear Approach to NMR Spectroscopy written by J.B. Lambert and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 552 pages. Available in PDF, EPUB and Kindle. Book excerpt: The field of nuclear magnetic resonance has experienced a number of spectacular developments during the last decade. Fourier transform methodology revolutionized signal acquisition capabilities. Superconducting magnets enhanced sensitivity and produced considerable improvement in spectral dispersion. In areas of new applicat ions, the life sciences particularly bene fited from these developments and probably saw the largest increase in usage. NMR imaging promises to offer a noninvasive alternative to X rays. High resolution is now achievable with solids, through magic angle spinning and cross polarization, so that the powers of NMR are applicable to previously intractable materials such as polymers, coal, and other geochemicals. The ease of obtaining relaxation times brought an important fourth variable, after the chemical shift, the coupling constant, and the rate constant, to the examination of structural and kinetic problems i~ all fields. Software development, particularly in the area of pulse sequences, created a host of useful tech niques, including difference decoupling and difference nuclear Overhauser effect spectra, multidimensional displays, signal enhancement (INEPT), coupling constant analysis for connectivity (INADEQUATE), and observation of specific structural classes such as only quaternary carbons. Finally, hardware development gave us access to the entire Periodic Table, to the particular advan tage of the inorganic and organometallic chemist. At the NATO Advanced Study Institute at Stirling, Scotland, the participants endeavored to examine all these advances, except imaging, from a multidisciplinary point of view.

The Multinuclear Approach to NMR Spectroscopy

Author : J.B. Lambert
Publisher : Springer
ISBN 13 : 9789027715821
Total Pages : 548 pages
Book Rating : 4.7/5 (158 download)

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Book Synopsis The Multinuclear Approach to NMR Spectroscopy by : J.B. Lambert

Download or read book The Multinuclear Approach to NMR Spectroscopy written by J.B. Lambert and published by Springer. This book was released on 1983-05-31 with total page 548 pages. Available in PDF, EPUB and Kindle. Book excerpt: The field of nuclear magnetic resonance has experienced a number of spectacular developments during the last decade. Fourier transform methodology revolutionized signal acquisition capabilities. Superconducting magnets enhanced sensitivity and produced considerable improvement in spectral dispersion. In areas of new applicat ions, the life sciences particularly bene fited from these developments and probably saw the largest increase in usage. NMR imaging promises to offer a noninvasive alternative to X rays. High resolution is now achievable with solids, through magic angle spinning and cross polarization, so that the powers of NMR are applicable to previously intractable materials such as polymers, coal, and other geochemicals. The ease of obtaining relaxation times brought an important fourth variable, after the chemical shift, the coupling constant, and the rate constant, to the examination of structural and kinetic problems i~ all fields. Software development, particularly in the area of pulse sequences, created a host of useful tech niques, including difference decoupling and difference nuclear Overhauser effect spectra, multidimensional displays, signal enhancement (INEPT), coupling constant analysis for connectivity (INADEQUATE), and observation of specific structural classes such as only quaternary carbons. Finally, hardware development gave us access to the entire Periodic Table, to the particular advan tage of the inorganic and organometallic chemist. At the NATO Advanced Study Institute at Stirling, Scotland, the participants endeavored to examine all these advances, except imaging, from a multidisciplinary point of view.

Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications

Author : P. Granger
Publisher : Springer Science & Business Media
ISBN 13 : 9400921497
Total Pages : 473 pages
Book Rating : 4.4/5 (9 download)

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Book Synopsis Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications by : P. Granger

Download or read book Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications written by P. Granger and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 473 pages. Available in PDF, EPUB and Kindle. Book excerpt: The idea of this NATO school was born during philosophical discussions with Dr Brevard on the present and future of NMR during a night walk under the palm trees in Biskra during a seminar held in this oasis. It was clear for us that the recent progress in the field of NMR, especially inverse spectroscopy and the development of MAS, was opening new perspectives for chemists. We realised also that organometallic and inorganic chemists were not clearly informed about the potentialities of all the new methods. NA TO, with its summer schools, was offering a good opportunity to propose to the chemical community a session where those problems would be largely developped. This School is then the prolongation of the two previous ones: Palermo in 1976 on "the less receptive nuclei" and Stirling in 1982 on "the multinuclear approach to NMR spectroscopy" . It was divided into two sub-sessions: NMR in the liquid state and NMR in the solid state. This is reflected in the book organization. As indicated by the title of this School, we were mainly concerned with the methodological aspects of multinuclear NMR. If many examples are given, they appear only as a support for the understanding of the theory or in explanation of some practical aspects of the different experiments. Each domain is introduced by a lecture which presents selected examples.

Handbook of High Resolution Multinuclear NMR

Author : C. Brevard
Publisher : John Wiley & Sons
ISBN 13 :
Total Pages : 264 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Handbook of High Resolution Multinuclear NMR by : C. Brevard

Download or read book Handbook of High Resolution Multinuclear NMR written by C. Brevard and published by John Wiley & Sons. This book was released on 1981 with total page 264 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Multinuclear NMR

Author : J. Mason
Publisher : Springer Science & Business Media
ISBN 13 : 1461317835
Total Pages : 642 pages
Book Rating : 4.4/5 (613 download)

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Book Synopsis Multinuclear NMR by : J. Mason

Download or read book Multinuclear NMR written by J. Mason and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 642 pages. Available in PDF, EPUB and Kindle. Book excerpt: With the power and range of modern pulse spectrometers the compass of NMR spec troscopy is now very large for a single book-but we have undertaken this. Our book covers the Periodic Table as multinuclear spectrometers do, and introductory chapters are devoted to the essentials of the NMR experiment and its products. Primary products are chemical shifts (including anisotropies), spin-spin coupling constants, and relaxation times; the ultimate product is a knowledge of content and constitution, dynamic as well as static. Our province is chemical and biochemical rather than physical or technical; only passing reference is made to metallic solids or unstable species, or to practical NMR spectroscopy. Our aim is depth as well as breadth, to explain the fundamental processes, whether of nuclear magnetic shielding, spin-spin coupling, relaxation, or the multiple pulse sequences that have allowed the development of high-resolution studies of solids, multidimensional NMR spectroscopy, techniques for sensitivity enhancement, and so on. This book therefore combines the functions of advanced textbook and reference book. For reasonably comprehensive coverage in a single volume we have sum marized the information in tables and charts, and included all leading references.

NMR and Chemistry

Author : J. W. Akitt
Publisher : Springer
ISBN 13 :
Total Pages : 288 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis NMR and Chemistry by : J. W. Akitt

Download or read book NMR and Chemistry written by J. W. Akitt and published by Springer. This book was released on 1983 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: The theory of nuclear magnetization. The magnetic field at the nucleus. Internuclear spin-spin coupling. Nuclear magnetic relaxation and related phenomena. Modern spectrometer systems. The sample. Multiple resonance experiments. Some and exciting techniques in NMR. Some examples of the use of NMR in chemistry.

Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials

Author : Kenneth J.D. MacKenzie
Publisher : Elsevier
ISBN 13 : 0080537103
Total Pages : 748 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials by : Kenneth J.D. MacKenzie

Download or read book Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials written by Kenneth J.D. MacKenzie and published by Elsevier. This book was released on 2002-04-26 with total page 748 pages. Available in PDF, EPUB and Kindle. Book excerpt: Techniques of solid state nuclear magnetic resonance (NMR) spectroscopy are constantly being extended to a more diverse range of materials, pressing into service an ever-expanding range of nuclides including some previously considered too intractable to provide usable results. At the same time, new developments in both hardware and software are being introduced and refined. This book covers the most important of these new developments. With sections addressed to non-specialist researchers (providing accessible answers to the most common questions about the theory and practice of NMR asked by novices) as well as a more specialised and up-to-date treatment of the most important areas of inorganic materials research to which NMR has application, this book should be useful to NMR users whatever their level of expertise and whatever inorganic materials they wish to study.

Nuclear Magnetic Resonance Spectroscopy

Author : Joseph B. Lambert
Publisher : John Wiley & Sons
ISBN 13 : 1119295238
Total Pages : 485 pages
Book Rating : 4.1/5 (192 download)

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Book Synopsis Nuclear Magnetic Resonance Spectroscopy by : Joseph B. Lambert

Download or read book Nuclear Magnetic Resonance Spectroscopy written by Joseph B. Lambert and published by John Wiley & Sons. This book was released on 2019-01-04 with total page 485 pages. Available in PDF, EPUB and Kindle. Book excerpt: Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

NMR — From Spectra to Structures

Author : Terence N. Mitchell
Publisher : Springer Science & Business Media
ISBN 13 : 3662054345
Total Pages : 144 pages
Book Rating : 4.6/5 (62 download)

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Book Synopsis NMR — From Spectra to Structures by : Terence N. Mitchell

Download or read book NMR — From Spectra to Structures written by Terence N. Mitchell and published by Springer Science & Business Media. This book was released on 2013-04-17 with total page 144 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR spectroscopy is one of the most important analytical methods available today. This practice-oriented textbook shows how NMR spectra is used in the education of organic structures. The emphasis is on practical rather than on theoretical aspects, which are treated only briefly. NMR- From Spectra to Strucures is a textbook providing an ideal practical guide to today ́s standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only the 1D NMR spectra (proton, carbon, DEPT/APT) but, for the first time in a textbook, also the most important 2D spectra (H,H and C,H correlation).

Introduction to Multinuclear NMR

Author : Claude H. Yoder
Publisher : Benjamin-Cummings Publishing Company
ISBN 13 : 9780805397512
Total Pages : 335 pages
Book Rating : 4.3/5 (975 download)

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Book Synopsis Introduction to Multinuclear NMR by : Claude H. Yoder

Download or read book Introduction to Multinuclear NMR written by Claude H. Yoder and published by Benjamin-Cummings Publishing Company. This book was released on 1987-01-01 with total page 335 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Fourier Transform NMR Techniques

Author : K. Müllen
Publisher :
ISBN 13 :
Total Pages : 170 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Fourier Transform NMR Techniques by : K. Müllen

Download or read book Fourier Transform NMR Techniques written by K. Müllen and published by . This book was released on 1976 with total page 170 pages. Available in PDF, EPUB and Kindle. Book excerpt:

17 0 NMR Spectroscopy in Organic Chemistry

Author : David W. Boykin
Publisher : CRC Press
ISBN 13 : 1000103099
Total Pages : 332 pages
Book Rating : 4.0/5 (1 download)

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Book Synopsis 17 0 NMR Spectroscopy in Organic Chemistry by : David W. Boykin

Download or read book 17 0 NMR Spectroscopy in Organic Chemistry written by David W. Boykin and published by CRC Press. This book was released on 2020-08-26 with total page 332 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a comprehensive review of the application of 17O NMR spectroscopy to organic chemistry. Topics include the theoretical aspects of chemical shift, quadrupolar and J coupling; 17O enrichment; the effect of steric interactions on 17O chemical shifts of functional groups in flexible and rigid systems; the application of 17O NMR spectroscopy to hydrogen bonding investigations; mechanistic problems in organic and bioorganic chemistry; and 17O NMR spectroscopy of oxygen monocoordinated to carbon in alcohols, ethers, and derivatives. Recent results that show correlations between molecular geometry, determined by X-ray studies and estimated by molecular mechanics calculations, and 17O chemical shifts are also covered. 17O Spectroscopy in Organic Chemistry provides important reference information for organic chemists and other scientists interested in 17O NMR spectroscopy as a tool for obtaining new structural and chemical data about organic molecules.

Annual Reports on NMR Spectroscopy

Author :
Publisher : Academic Press
ISBN 13 : 9780080584003
Total Pages : 356 pages
Book Rating : 4.5/5 (84 download)

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Book Synopsis Annual Reports on NMR Spectroscopy by :

Download or read book Annual Reports on NMR Spectroscopy written by and published by Academic Press. This book was released on 1986-07-10 with total page 356 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR spectroscopy has grown to be a vitally important technique with applications in many areas of science. Annual Reports on NMR Spectroscopy is quickly becoming the source for the latest information on current progress, both experimental and theoretical. Chemists in a variety of disciplines will be interested in this up-to-date, comprehensive series.

Annual Reports on NMR Spectroscopy

Author : Graham A. Webb
Publisher : Academic Press
ISBN 13 : 9780123810427
Total Pages : 233 pages
Book Rating : 4.8/5 (14 download)

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Book Synopsis Annual Reports on NMR Spectroscopy by : Graham A. Webb

Download or read book Annual Reports on NMR Spectroscopy written by Graham A. Webb and published by Academic Press. This book was released on 2009-10-12 with total page 233 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. * Provides updates on the latest developments in NMR spectroscopy * Includes comprehensive review articles * Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

Nuclear Magnetic Resonance

Author : William W. Paudler
Publisher : Wiley-Interscience
ISBN 13 :
Total Pages : 310 pages
Book Rating : 4.:/5 (319 download)

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Book Synopsis Nuclear Magnetic Resonance by : William W. Paudler

Download or read book Nuclear Magnetic Resonance written by William W. Paudler and published by Wiley-Interscience. This book was released on 1987-05-11 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt: Describes the use of NMR for structural and mechanistic studies in organic and inorganic chemistry and biochemistry. Theory is presented in semi-empirical fashion, and only a minimal mathematical approach applied. Describes the original NMR experiment done using the low resolution technique and advances to the modern Fourier transform technique. In addition to chemical shifts, coupling constants, and double resonance, this book covers magic angle and treats inorganic and biological systems. Presentations include appropriate examples and problems.

Fast NMR Data Acquisition

Author : Mehdi Mobli
Publisher : Royal Society of Chemistry
ISBN 13 : 1849736197
Total Pages : 325 pages
Book Rating : 4.8/5 (497 download)

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Book Synopsis Fast NMR Data Acquisition by : Mehdi Mobli

Download or read book Fast NMR Data Acquisition written by Mehdi Mobli and published by Royal Society of Chemistry. This book was released on 2017-05-23 with total page 325 pages. Available in PDF, EPUB and Kindle. Book excerpt: Providing a definitive reference source on novel methods in NMR acquisition and processing, this book will highlight similarities and differences between emerging approaches and focus on identifying which methods are best suited for different applications. The highly qualified editors have conducted extensive research into the fundamentals of fast methods of data acquisition in NMR, including applications of non-Fourier methods of spectrum analysis. With contributions from additional distinguished experts in allied fields, clear explanations are provided on methods that speed up NMR experiments using different ways to manipulate the nuclei in the sample, modern methods for estimating the spectrum from the time domain response recorded during an NMR experiment, and finally how the data is sampled. Starting with a historical overview of Fourier Transformation and its role in modern NMR spectroscopy, this volume will clarify and demystify this important emerging field for spectroscopists and analytical chemists in industry and academia.

Perspectives in Modern Chemical Spectroscopy

Author : David L. Andrews
Publisher : Springer Science & Business Media
ISBN 13 : 3642754562
Total Pages : 333 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Perspectives in Modern Chemical Spectroscopy by : David L. Andrews

Download or read book Perspectives in Modern Chemical Spectroscopy written by David L. Andrews and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 333 pages. Available in PDF, EPUB and Kindle. Book excerpt: "An interesting and enlightening book well worth the time for someone who is grounded in the basics of spectroscopy, yet interested in newer techniques and applications... particularly useful in providing breadth for those whose work has caused them to narrow their appreciation of spectroscopy to one area." (Spectroscopy) "This book should be on the bookshelves of all chemists whose daily work involves the practical application of spectroscopy to chemical analysis." (Fresenius' J. of Analytical Chem.) "...stands in style between an introduction to the various topics covered and near monographic treatments...meets a real need." (Faraday Transactions) "It covers an enormous amount of spectral theory and methodology in a condensed and readable format." (SIM News)