Multinuclear Nmr

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Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials

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Author : Kenneth J.D. MacKenzie
Publisher : Elsevier
ISBN 13 : 0080537103
Total Pages : 748 pages
Book Rating : 4.0/5 (85 download)

Book Synopsis Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials by : Kenneth J.D. MacKenzie

Download or read book Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials written by Kenneth J.D. MacKenzie and published by Elsevier. This book was released on 2002-04-26 with total page 748 pages. Available in PDF, EPUB and Kindle. Book excerpt: Techniques of solid state nuclear magnetic resonance (NMR) spectroscopy are constantly being extended to a more diverse range of materials, pressing into service an ever-expanding range of nuclides including some previously considered too intractable to provide usable results. At the same time, new developments in both hardware and software are being introduced and refined. This book covers the most important of these new developments. With sections addressed to non-specialist researchers (providing accessible answers to the most common questions about the theory and practice of NMR asked by novices) as well as a more specialised and up-to-date treatment of the most important areas of inorganic materials research to which NMR has application, this book should be useful to NMR users whatever their level of expertise and whatever inorganic materials they wish to study.

Multinuclear NMR

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Author : J. Mason
Publisher : Springer Science & Business Media
ISBN 13 : 1461317835
Total Pages : 642 pages
Book Rating : 4.4/5 (613 download)

Book Synopsis Multinuclear NMR by : J. Mason

Download or read book Multinuclear NMR written by J. Mason and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 642 pages. Available in PDF, EPUB and Kindle. Book excerpt: With the power and range of modern pulse spectrometers the compass of NMR spec troscopy is now very large for a single book-but we have undertaken this. Our book covers the Periodic Table as multinuclear spectrometers do, and introductory chapters are devoted to the essentials of the NMR experiment and its products. Primary products are chemical shifts (including anisotropies), spin-spin coupling constants, and relaxation times; the ultimate product is a knowledge of content and constitution, dynamic as well as static. Our province is chemical and biochemical rather than physical or technical; only passing reference is made to metallic solids or unstable species, or to practical NMR spectroscopy. Our aim is depth as well as breadth, to explain the fundamental processes, whether of nuclear magnetic shielding, spin-spin coupling, relaxation, or the multiple pulse sequences that have allowed the development of high-resolution studies of solids, multidimensional NMR spectroscopy, techniques for sensitivity enhancement, and so on. This book therefore combines the functions of advanced textbook and reference book. For reasonably comprehensive coverage in a single volume we have sum marized the information in tables and charts, and included all leading references.

Handbook of High Resolution Multinuclear NMR

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Author : C. Brevard
Publisher : John Wiley & Sons
ISBN 13 :
Total Pages : 264 pages
Book Rating : 4.3/5 (91 download)

Book Synopsis Handbook of High Resolution Multinuclear NMR by : C. Brevard

Download or read book Handbook of High Resolution Multinuclear NMR written by C. Brevard and published by John Wiley & Sons. This book was released on 1981 with total page 264 pages. Available in PDF, EPUB and Kindle. Book excerpt:

The Multinuclear Approach to NMR Spectroscopy

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Author : J.B. Lambert
Publisher : Springer Science & Business Media
ISBN 13 : 9400971303
Total Pages : 552 pages
Book Rating : 4.4/5 (9 download)

Book Synopsis The Multinuclear Approach to NMR Spectroscopy by : J.B. Lambert

Download or read book The Multinuclear Approach to NMR Spectroscopy written by J.B. Lambert and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 552 pages. Available in PDF, EPUB and Kindle. Book excerpt: The field of nuclear magnetic resonance has experienced a number of spectacular developments during the last decade. Fourier transform methodology revolutionized signal acquisition capabilities. Superconducting magnets enhanced sensitivity and produced considerable improvement in spectral dispersion. In areas of new applicat ions, the life sciences particularly bene fited from these developments and probably saw the largest increase in usage. NMR imaging promises to offer a noninvasive alternative to X rays. High resolution is now achievable with solids, through magic angle spinning and cross polarization, so that the powers of NMR are applicable to previously intractable materials such as polymers, coal, and other geochemicals. The ease of obtaining relaxation times brought an important fourth variable, after the chemical shift, the coupling constant, and the rate constant, to the examination of structural and kinetic problems i~ all fields. Software development, particularly in the area of pulse sequences, created a host of useful tech niques, including difference decoupling and difference nuclear Overhauser effect spectra, multidimensional displays, signal enhancement (INEPT), coupling constant analysis for connectivity (INADEQUATE), and observation of specific structural classes such as only quaternary carbons. Finally, hardware development gave us access to the entire Periodic Table, to the particular advan tage of the inorganic and organometallic chemist. At the NATO Advanced Study Institute at Stirling, Scotland, the participants endeavored to examine all these advances, except imaging, from a multidisciplinary point of view.

Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications

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Author : P. Granger
Publisher : Springer Science & Business Media
ISBN 13 : 9400921497
Total Pages : 473 pages
Book Rating : 4.4/5 (9 download)

Book Synopsis Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications by : P. Granger

Download or read book Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications written by P. Granger and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 473 pages. Available in PDF, EPUB and Kindle. Book excerpt: The idea of this NATO school was born during philosophical discussions with Dr Brevard on the present and future of NMR during a night walk under the palm trees in Biskra during a seminar held in this oasis. It was clear for us that the recent progress in the field of NMR, especially inverse spectroscopy and the development of MAS, was opening new perspectives for chemists. We realised also that organometallic and inorganic chemists were not clearly informed about the potentialities of all the new methods. NA TO, with its summer schools, was offering a good opportunity to propose to the chemical community a session where those problems would be largely developped. This School is then the prolongation of the two previous ones: Palermo in 1976 on "the less receptive nuclei" and Stirling in 1982 on "the multinuclear approach to NMR spectroscopy" . It was divided into two sub-sessions: NMR in the liquid state and NMR in the solid state. This is reflected in the book organization. As indicated by the title of this School, we were mainly concerned with the methodological aspects of multinuclear NMR. If many examples are given, they appear only as a support for the understanding of the theory or in explanation of some practical aspects of the different experiments. Each domain is introduced by a lecture which presents selected examples.

Introduction to Multinuclear NMR

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Author : Claude H. Yoder
Publisher : Benjamin-Cummings Publishing Company
ISBN 13 : 9780805397512
Total Pages : 335 pages
Book Rating : 4.3/5 (975 download)

Book Synopsis Introduction to Multinuclear NMR by : Claude H. Yoder

Download or read book Introduction to Multinuclear NMR written by Claude H. Yoder and published by Benjamin-Cummings Publishing Company. This book was released on 1987-01-01 with total page 335 pages. Available in PDF, EPUB and Kindle. Book excerpt:

NMR in Chemistry

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Author : William Kemp
Publisher : Free Press
ISBN 13 : 9780029494011
Total Pages : 240 pages
Book Rating : 4.4/5 (94 download)

Book Synopsis NMR in Chemistry by : William Kemp

Download or read book NMR in Chemistry written by William Kemp and published by Free Press. This book was released on 1988 with total page 240 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Multinuclear NMR of Ionomers and Polymer Blends

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Author : Ellen Margaret O'Connell
Publisher :
ISBN 13 :
Total Pages : 586 pages
Book Rating : 4.:/5 (89 download)

Book Synopsis Multinuclear NMR of Ionomers and Polymer Blends by : Ellen Margaret O'Connell

Download or read book Multinuclear NMR of Ionomers and Polymer Blends written by Ellen Margaret O'Connell and published by . This book was released on 1995 with total page 586 pages. Available in PDF, EPUB and Kindle. Book excerpt: Many factors are known to affect the morphology and properties of ionomers, and the role that the cation local environment plays is not well understood. To better understand ionomer morphology, the cation environment in sulfonated and carboxylated ionomers was investigated using 23Na NMR. As many as three environments were seen in polydisperse sulfonated polystyrene (NaSPS): isolated sodium ions at 7 ppm, hydrated ions at 0 ppm, and aggregated ions at -12 to -23 ppm. In monodisperse NaSPS, a fourth peak at -2.7 ppm appeared at ionization levels above 1.2% and molecular weights of at least 35,000. The fraction of sodium ions held in isolated ion pairs decreased to zero while the fraction of ionic species in aggregates increased with increasing sulfonation. As the neutralization level increased, the aggregate peak shifted to higher frequency with incorporation of neutralizing NaOH. These peak positions and trends are explainable in terms of the magnetic and electric field properties of each Na+ environment.

The Multinuclear Approach to NMR Spectroscopy

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Author : J.B. Lambert
Publisher : Springer
ISBN 13 : 9789027715821
Total Pages : 548 pages
Book Rating : 4.7/5 (158 download)

Book Synopsis The Multinuclear Approach to NMR Spectroscopy by : J.B. Lambert

Download or read book The Multinuclear Approach to NMR Spectroscopy written by J.B. Lambert and published by Springer. This book was released on 1983-05-31 with total page 548 pages. Available in PDF, EPUB and Kindle. Book excerpt: The field of nuclear magnetic resonance has experienced a number of spectacular developments during the last decade. Fourier transform methodology revolutionized signal acquisition capabilities. Superconducting magnets enhanced sensitivity and produced considerable improvement in spectral dispersion. In areas of new applicat ions, the life sciences particularly bene fited from these developments and probably saw the largest increase in usage. NMR imaging promises to offer a noninvasive alternative to X rays. High resolution is now achievable with solids, through magic angle spinning and cross polarization, so that the powers of NMR are applicable to previously intractable materials such as polymers, coal, and other geochemicals. The ease of obtaining relaxation times brought an important fourth variable, after the chemical shift, the coupling constant, and the rate constant, to the examination of structural and kinetic problems i~ all fields. Software development, particularly in the area of pulse sequences, created a host of useful tech niques, including difference decoupling and difference nuclear Overhauser effect spectra, multidimensional displays, signal enhancement (INEPT), coupling constant analysis for connectivity (INADEQUATE), and observation of specific structural classes such as only quaternary carbons. Finally, hardware development gave us access to the entire Periodic Table, to the particular advan tage of the inorganic and organometallic chemist. At the NATO Advanced Study Institute at Stirling, Scotland, the participants endeavored to examine all these advances, except imaging, from a multidisciplinary point of view.

Biological Applications of Magnetic Resonance

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Author : Robert Gerson Shulman
Publisher :
ISBN 13 :
Total Pages : 616 pages
Book Rating : 4.3/5 (91 download)

Book Synopsis Biological Applications of Magnetic Resonance by : Robert Gerson Shulman

Download or read book Biological Applications of Magnetic Resonance written by Robert Gerson Shulman and published by . This book was released on 1979 with total page 616 pages. Available in PDF, EPUB and Kindle. Book excerpt: Biological Applications of Magnetic Resonance ...

Fundamentals of Protein NMR Spectroscopy

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Author : Gordon S. Rule
Publisher : Springer Science & Business Media
ISBN 13 : 1402035004
Total Pages : 543 pages
Book Rating : 4.4/5 (2 download)

Book Synopsis Fundamentals of Protein NMR Spectroscopy by : Gordon S. Rule

Download or read book Fundamentals of Protein NMR Spectroscopy written by Gordon S. Rule and published by Springer Science & Business Media. This book was released on 2006-02-16 with total page 543 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR spectroscopy has proven to be a powerful technique to study the structure and dynamics of biological macromolecules. Fundamentals of Protein NMR Spectroscopy is a comprehensive textbook that guides the reader from a basic understanding of the phenomenological properties of magnetic resonance to the application and interpretation of modern multi-dimensional NMR experiments on 15N/13C-labeled proteins. Beginning with elementary quantum mechanics, a set of practical rules is presented and used to describe many commonly employed multi-dimensional, multi-nuclear NMR pulse sequences. A modular analysis of NMR pulse sequence building blocks also provides a basis for understanding and developing novel pulse programs. This text not only covers topics from chemical shift assignment to protein structure refinement, as well as the analysis of protein dynamics and chemical kinetics, but also provides a practical guide to many aspects of modern spectrometer hardware, sample preparation, experimental set-up, and data processing. End of chapter exercises are included to emphasize important concepts. Fundamentals of Protein NMR Spectroscopy not only offer students a systematic, in-depth, understanding of modern NMR spectroscopy and its application to biomolecular systems, but will also be a useful reference for the experienced investigator.

NMR and Chemistry

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Author : J. W. Akitt
Publisher : Springer
ISBN 13 :
Total Pages : 288 pages
Book Rating : 4.3/5 (91 download)

Book Synopsis NMR and Chemistry by : J. W. Akitt

Download or read book NMR and Chemistry written by J. W. Akitt and published by Springer. This book was released on 1983 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: The theory of nuclear magnetization. The magnetic field at the nucleus. Internuclear spin-spin coupling. Nuclear magnetic relaxation and related phenomena. Modern spectrometer systems. The sample. Multiple resonance experiments. Some and exciting techniques in NMR. Some examples of the use of NMR in chemistry.

Solid-State NMR in Materials Science

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Author : Vladimir I. Bakhmutov
Publisher : CRC Press
ISBN 13 : 1439869634
Total Pages : 283 pages
Book Rating : 4.4/5 (398 download)

Book Synopsis Solid-State NMR in Materials Science by : Vladimir I. Bakhmutov

Download or read book Solid-State NMR in Materials Science written by Vladimir I. Bakhmutov and published by CRC Press. This book was released on 2011-12-19 with total page 283 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-state NMR is a powerful physical method widely applied in modern fundamental and applied science, medicine, and industry. Its role is particularly valuable in materials chemistry due to the capability of solid-state NMR to rapidly solve tasks connected with structural descriptions of complex systems on macro and/or molecular levels, and the identification of the dynamics often responsible for complex systems mechanical properties. Written for non-specialists, Solid-State NMR in Materials Science: Principles and Applications introduces the general physical principles of pulsed NMR, by including elements of the theory and practice in the registration of NMR signals, and by explaining different NMR equipment. After the preliminaries, the book covers: The theory and features of solid-state NMR and nuclear relaxation in solids, including dynamics of materials Different materials, diamagnetic and paramagnetic, from metals and metal clusters to amorphous composites The methodology of collection and interpretations of solid-state NMR data, including strategies and criteria for structural characterizations of different materials Practical examples of multinuclear NMR and relaxation experiments as well as interpretations of data obtained Numerous solid-state NMR experiments performed for various materials to evaluate their structure and dynamics Written in clear and simple language, this book includes clear illustrations, numerous examples, and detailed bibliographies. It an excellent reference not only for young and experienced researchers, but also for students interested in a future in materials science.

Gas Phase NMR

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Author : Karol Jackowski
Publisher : Royal Society of Chemistry
ISBN 13 : 1782623817
Total Pages : 400 pages
Book Rating : 4.7/5 (826 download)

Book Synopsis Gas Phase NMR by : Karol Jackowski

Download or read book Gas Phase NMR written by Karol Jackowski and published by Royal Society of Chemistry. This book was released on 2016-02-09 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers the recent NMR studies with the application of gaseous molecules. Among the comprehensively discussed aspects of the area it includes in particular: new multinuclear experiments that deliver spectral parameters of isolated molecules and provide the most accurate values of nuclear magnetic shielding, isotropic spin–spin coupling and relaxation times; advanced, precise and correct theoretical descriptions of spectral parameters of molecules as well as the application of gas-phase NMR measurements to chemical analysis and medicine. The progress of research in these fields is enormous and has rapidly changed our knowledge and understanding of molecular parameters in NMR spectroscopy. For example, accurate studies of the shielding for isolated molecules allow the exact determination of nuclear magnetic dipole moments, the calculated values of spectral parameters can be verified by precise gas-phase NMR measurements, and the application of hyperpolarized noble gases provides excellent MRI pictures of lungs. Aimed at graduates and researchers in spectroscopy, analytical chemistry and those researching the applications of NMR in medicine, this book presents the connections between sophisticated experiments, the theory of magnetic parameters and the exploration of new methods in practice.

NMR and MRI of Gels

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Author : Yves De Deene
Publisher : Royal Society of Chemistry
ISBN 13 : 1788019202
Total Pages : 409 pages
Book Rating : 4.7/5 (88 download)

Book Synopsis NMR and MRI of Gels by : Yves De Deene

Download or read book NMR and MRI of Gels written by Yves De Deene and published by Royal Society of Chemistry. This book was released on 2020-07-07 with total page 409 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gels are used in a large variety of commercial and scientific products from drug delivery systems and food science to biomedical sensors. They also are invaluable in MRI physics research where they mimic biological tissue and in radiotherapy quality assurance where they are used to capture the three dimensional radiation dose distribution. This unique book discusses the state-of-the-art of NMR and MRI techniques in studying the physics and chemistry of gel systems, in their application as MRI phantoms and as three dimensional radiation dosimeters. The first part of the book will cover the fundamental physical concepts of gels and the NMR techniques to study gel systems. The second part is dedicated to the application of gels in the life sciences and in the medical practice to validate radiotherapy and new MRI techniques. Filling the gap in literature, this volume provides the scientific reader with an extensive overview of possible techniques and methods to study the interesting properties and applications of gels. For the MRI researcher and medical physicist, the book will be a valuable resource in using gel phantoms for validating contemporary MRI techniques and radiotherapy treatments.

Nuclear Magnetic Resonance Volume 47

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Author : Paul Hodgkinson
Publisher : Royal Society of Chemistry
ISBN 13 : 1839163917
Total Pages : 299 pages
Book Rating : 4.8/5 (391 download)

Book Synopsis Nuclear Magnetic Resonance Volume 47 by : Paul Hodgkinson

Download or read book Nuclear Magnetic Resonance Volume 47 written by Paul Hodgkinson and published by Royal Society of Chemistry. This book was released on 2021-11-29 with total page 299 pages. Available in PDF, EPUB and Kindle. Book excerpt: Applications of nuclear magnetic resonance span a wide range of scientific disciplines, from physics to medicine. For those wanting to become acquainted with NMR or seasoned practitioners, this is a valuable source of current methods and applications.

Multinuclear NMR Studies of Macrocyclic Complexes

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Author : Roger Donald Boss
Publisher :
ISBN 13 :
Total Pages : 482 pages
Book Rating : 4.3/5 (129 download)

Book Synopsis Multinuclear NMR Studies of Macrocyclic Complexes by : Roger Donald Boss

Download or read book Multinuclear NMR Studies of Macrocyclic Complexes written by Roger Donald Boss and published by . This book was released on 1985 with total page 482 pages. Available in PDF, EPUB and Kindle. Book excerpt: