Quantitative Analysis By Gas Chromatography

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Quantitative Gas Chromatography for Laboratory Analyses and On-Line Process Control

Author : G. Guiochon
Publisher : Elsevier
ISBN 13 : 9780080858470
Total Pages : 796 pages
Book Rating : 4.8/5 (584 download)

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Book Synopsis Quantitative Gas Chromatography for Laboratory Analyses and On-Line Process Control by : G. Guiochon

Download or read book Quantitative Gas Chromatography for Laboratory Analyses and On-Line Process Control written by G. Guiochon and published by Elsevier. This book was released on 1988-06-01 with total page 796 pages. Available in PDF, EPUB and Kindle. Book excerpt: Here is an invaluable new book on quantitative gas chromatography which explains how the method can - or should - be used for accurate and precise analysis. Gas chromatography is firmly established as one of the few major methods for the quantitative analysis of complex mixtures. It is fast, accurate and inexpensive, with a broad range of applications. It has however become very complex and involved: over 200 stationary phases, more than 10 detector principles and several very different column types are available from among the catalogs of over 100 manufacturers and major retailers. The progressive changes in the nature of gas chromatography have created new needs for information which are not satisfied by the literature presently available. This book provides a complete discussion of all the problems involved in the achievement of quantitative analysis by gas chromatography, whether in the research laboratory, in the routine analysis laboratory or in process control. For this reason the presentation of theoretical concepts has been limited to the essential, while extensive explanations have been devoted to the various steps involved in the derivation of precise and accurate data. This starts with the selection of the instrumentation and column, continues with the choice of optimum experimental conditions, then calibration and ends with the use of correct procedures for data acquisition and calculations. Finally, there is almost always a way to reduce errors and an entire chapter deals with this single issue. Numerous relevant examples are presented. The first part of the book presents the theoretical background, simple enough to be understood by all analytical chemists, but still complete and up-to-date. It discusses the problems of flow dynamics, retention and band broadening. The changes in band profile associated with column overloading are explained without much recourse to mathematics. The second part describes the gas chromatograph and discusses the properties of each of its parts: gas flow and pressure controller sampling system, oven, column switching valves, detectors. The different implementations, their advantages and drawbacks are discussed and compared. In addition, three chapters present packed column technology, open tubular column technology and some sophisticated new phase systems, respectively. The new phase systems described use adsorbents, modified by coating or grafting organic phase, and carrier gases containing vapors which are sorbed by the stationary phase and modify it, such as steam. The third part discusses the applications in qualitative and quantitative analysis. Calibration, peak integration, sources of errors arising from the various parts of the instrument as well as from the measurement process itself are carefully described in four detailed chapters. Methods to carry out accurate and precise analysis are presented. A last chapter is devoted to process control analysis and gives a number of detailed examples of applications. A lexicon explaining the most important chromatographic terms and a detailed index complete the book. This is a book which no chemical analyst should be without. It should be on the library shelf of all universities, instrument companies and any laboratory and plant where gas chromatography is used.

Basic Gas Chromatography

Author : Harold M. McNair
Publisher : John Wiley & Sons
ISBN 13 : 1118211200
Total Pages : 195 pages
Book Rating : 4.1/5 (182 download)

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Book Synopsis Basic Gas Chromatography by : Harold M. McNair

Download or read book Basic Gas Chromatography written by Harold M. McNair and published by John Wiley & Sons. This book was released on 2011-09-20 with total page 195 pages. Available in PDF, EPUB and Kindle. Book excerpt: The New Edition of the Well-Regarded Handbook on Gas Chromatography Since the publication of the highly successful first edition of Basic Gas Chromatography, the practice of chromatography has undergone several notable developments. Basic Gas Chromatography, Second Edition covers the latest in the field, giving readers the most up-to-date guide available, while maintaining the first edition's practical, applied approach to the subject and its accessibility to a wide range of readers. The text provides comprehensive coverage of basic topics in the field, such as stationary phases, packed columns and inlets, capillary columns and inlets, detectors, and qualitative and quantitative analysis. At the same time, the coverage also features key additions and updated topics including: Gas chromatography-mass spectrometry (GC-MS) Sampling methods Multidimensional gas chromatography Fast gas chromatography Gas chromatography analysis of nonvolatile compounds Inverse gas chromatography and pyrolysis gas chromatography Along with these new and updated topics, the references, resources, and Web sites in Basic Gas Chromatography have been revised to reflect the state of the field. Concise and fundamental in its coverage, Basic Gas Chromatography, Second Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists.

Quantitative Analysis by Gas Chromatography, Second Edition,

Author : Josef P Novák
Publisher : CRC Press
ISBN 13 : 9780824778187
Total Pages : 360 pages
Book Rating : 4.7/5 (781 download)

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Book Synopsis Quantitative Analysis by Gas Chromatography, Second Edition, by : Josef P Novák

Download or read book Quantitative Analysis by Gas Chromatography, Second Edition, written by Josef P Novák and published by CRC Press. This book was released on 1987-12-18 with total page 360 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Quantitative Analysis by Gas Chromatography

Author : Josef Novak
Publisher :
ISBN 13 :
Total Pages : 277 pages
Book Rating : 4.:/5 (945 download)

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Book Synopsis Quantitative Analysis by Gas Chromatography by : Josef Novak

Download or read book Quantitative Analysis by Gas Chromatography written by Josef Novak and published by . This book was released on 1988 with total page 277 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Advanced Gas Chromatography in Food Analysis

Author : Peter Q Tranchida
Publisher : Royal Society of Chemistry
ISBN 13 : 1788011279
Total Pages : 492 pages
Book Rating : 4.7/5 (88 download)

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Book Synopsis Advanced Gas Chromatography in Food Analysis by : Peter Q Tranchida

Download or read book Advanced Gas Chromatography in Food Analysis written by Peter Q Tranchida and published by Royal Society of Chemistry. This book was released on 2019-10-30 with total page 492 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography is widely used in applications involving food analysis. Typical applications pertain to the quantitative and/or qualitative analysis of food composition, natural products, food additives, and flavour and aroma components. Providing an up-to-date look at the significant advances in the technology, this book includes details on novel sample preparation processes; conventional, high-speed multidimensional gas chromatography systems, including preparative instrumentation; gas chromatography–olfactometry principles; and, finally, chemometrics principles and applications in food analysis. Aimed at providing the food researcher or analyst with detailed analytical information related to advanced gas chromatography technologies, this book is suitable for professionals and postgraduate students learning about the technique in the food industry and research.

Quantitative Chromatographic Analysis

Author : Thomas Beesley
Publisher : CRC Press
ISBN 13 : 9780203910788
Total Pages : 398 pages
Book Rating : 4.9/5 (17 download)

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Book Synopsis Quantitative Chromatographic Analysis by : Thomas Beesley

Download or read book Quantitative Chromatographic Analysis written by Thomas Beesley and published by CRC Press. This book was released on 2000-12-06 with total page 398 pages. Available in PDF, EPUB and Kindle. Book excerpt: Highlights critical factors involved in successful chromatographic analysis. Details analytical procedures; outlining sample preparation, collection, transportation, and storage. Provides step-by-step guidelines for producing analytical reports.

Advances in Gas Chromatography

Author : Xinghua Guo
Publisher : BoD – Books on Demand
ISBN 13 : 9535112279
Total Pages : 226 pages
Book Rating : 4.5/5 (351 download)

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Book Synopsis Advances in Gas Chromatography by : Xinghua Guo

Download or read book Advances in Gas Chromatography written by Xinghua Guo and published by BoD – Books on Demand. This book was released on 2014-02-26 with total page 226 pages. Available in PDF, EPUB and Kindle. Book excerpt: For decades gas chromatography has been and will remain an irreplaceable analytical technique in many research areas for both quantitative analysis and qualitative characterization/identification, which is still supplementary with HPLC. This book highlights a few areas where significant advances have been reported recently and/or a revisit of basic concepts is deserved. It provides an overview of instrumental developments, frontline and modern research as well as practical industrial applications. The topics include GC-based metabolomics in biomedical, plant and microbial research, natural products as well as characterization of aging of synthetic materials and industrial monitoring, which are contributions of several experts from different disciplines. It also contains best hand-on practices of sample preparation (derivatization) and data processing in daily research. This book is recommended to both basic and experienced researchers in gas chromatography.

Basic Gas Chromatography

Author : Harold M. McNair
Publisher : John Wiley & Sons
ISBN 13 : 1119450756
Total Pages : 293 pages
Book Rating : 4.1/5 (194 download)

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Book Synopsis Basic Gas Chromatography by : Harold M. McNair

Download or read book Basic Gas Chromatography written by Harold M. McNair and published by John Wiley & Sons. This book was released on 2019-09-11 with total page 293 pages. Available in PDF, EPUB and Kindle. Book excerpt: Basic Gas Chromatography, Third Edition provides a brief introduction to GC following the objectives for titles in this series. It should appeal to readers with varying levels of education and emphasizes a practical, applied approach to the subject. : This book provides a quick need-to-know introduction to gas chromatography; still the most widely used instrumental analysis technique, and is intended to assist new users in gaining understanding quickly and as a quick reference for experienced users. The new edition provides updated chapters that reflect changes in technology and methodology, especially sample preparation, detectors and multidimensional chromatography. The book also covers new detectors recently introduced and sample preparation methods that have become much more easily accessible since the previous edition.

Modern Practice of Gas Chromatography

Author : Robert L. Grob, PhD
Publisher : John Wiley & Sons
ISBN 13 : 047165115X
Total Pages : 1059 pages
Book Rating : 4.4/5 (716 download)

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Book Synopsis Modern Practice of Gas Chromatography by : Robert L. Grob, PhD

Download or read book Modern Practice of Gas Chromatography written by Robert L. Grob, PhD and published by John Wiley & Sons. This book was released on 2004-08-04 with total page 1059 pages. Available in PDF, EPUB and Kindle. Book excerpt: The bible of gas chromatography-offering everything the professional and the novice need to know about running, maintaining, and interpreting the results from GC Analytical chemists, technicians, and scientists in allied disciplines have come to regard Modern Practice of Gas Chomatography as the standard reference in gas chromatography. In addition to serving as an invaluable reference for the experienced practitioner, this bestselling work provides the beginner with a solid understanding of gas chromatographic theory and basic techniques. This new Fourth Edition incorporates the most recent developments in the field, including entirely new chapters on gas chromatography/mass spectrometry (GC/MS); optimization of separations and computer assistance; high speed or fast gas chromatography; mobile phase requirements: gas system requirements and sample preparation techniques; qualitative and quantitative analysis by GC; updated information on detectors; validation and QA/QC of chromatographic methods; and useful hints for good gas chromatography. As in previous editions, contributing authors have been chosen for their expertise and active participation in their respective areas. Modern Practice of Gas Chromatography, Fourth Edition presents a well-rounded and comprehensive overview of the current state of this important technology, providing a practical reference that will greatly appeal to both experienced chomatographers and novices.

Quantitative Analysis by Gas Chromatography

Author :
Publisher :
ISBN 13 : 9780824763114
Total Pages : 218 pages
Book Rating : 4.7/5 (631 download)

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Book Synopsis Quantitative Analysis by Gas Chromatography by :

Download or read book Quantitative Analysis by Gas Chromatography written by and published by . This book was released on 1975 with total page 218 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Quantitative Analysis Using Chromatographic Techniques

Author : Elena Katz
Publisher :
ISBN 13 :
Total Pages : 456 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Quantitative Analysis Using Chromatographic Techniques by : Elena Katz

Download or read book Quantitative Analysis Using Chromatographic Techniques written by Elena Katz and published by . This book was released on 1987-02-27 with total page 456 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the only book that covers only quantitative techniques of all chromatography methods. Contributors, experts in the field, present general concepts applicable to all types of analyses performed by chromatographic techniques, and treat in detail principles of quantitative detection and sources of error in data processing procedures. Chapters cover liquid chromatography, gas chromatography, thin-layer chromatography, detection methods, detector performance, data handling procedures, and automation procedures. Included is discussion of chromatographic applications in physical chemistry and in pharmaceutical analysis.

Practical Gas Chromatography

Author : Katja Dettmer-Wilde
Publisher : Springer
ISBN 13 : 3642546404
Total Pages : 904 pages
Book Rating : 4.6/5 (425 download)

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Book Synopsis Practical Gas Chromatography by : Katja Dettmer-Wilde

Download or read book Practical Gas Chromatography written by Katja Dettmer-Wilde and published by Springer. This book was released on 2014-11-05 with total page 904 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.

Comprehensive Two Dimensional Gas Chromatography

Author : Lourdes Ramos
Publisher : Elsevier
ISBN 13 : 9780080932699
Total Pages : 328 pages
Book Rating : 4.9/5 (326 download)

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Book Synopsis Comprehensive Two Dimensional Gas Chromatography by : Lourdes Ramos

Download or read book Comprehensive Two Dimensional Gas Chromatography written by Lourdes Ramos and published by Elsevier. This book was released on 2009-07-22 with total page 328 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book reviews the basic concepts and highlights the most relevant advances and developments that have taken place in the field of comprehensive two dimensional gas chromatography (GC x GC) since its introduction in 1991. The several instrumental and technical approaches assayed and developed during these seventeen years and that have contributed to the development of this powerful separation technique and to its increasing application in many areas is explained and comprehensively illustrated through a number of chapters devoted these specific topics. More specialized aspects of the technique, including theoretical aspects, modelization of the chromatographic process, software developments, and alternative couplings is also covered. Finally, special attention is paid to data treatment, for both qualitative and quantitative analysis. This book will be a practical resource that will explain from basic to specialized concepts of GC x GC and will show the current state-of-the-art and discuss future trends of this technique. Outlines basic concepts and principles of GCxGC technique for non-specialists to apply the technique to their research Provides detailed descriptions of recent technical advances and serves as an instructional guide in latest applications in GCxGC Sets the scene for possible future development and alternative new applications of technique

Static Headspace-Gas Chromatography

Author : Bruno Kolb
Publisher : John Wiley & Sons
ISBN 13 : 0471749443
Total Pages : 386 pages
Book Rating : 4.4/5 (717 download)

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Book Synopsis Static Headspace-Gas Chromatography by : Bruno Kolb

Download or read book Static Headspace-Gas Chromatography written by Bruno Kolb and published by John Wiley & Sons. This book was released on 2006-05-05 with total page 386 pages. Available in PDF, EPUB and Kindle. Book excerpt: STATIC HEADSPACE-GAS CHROMATOGRAPHY THE ONLY REFERENCE TO PROVIDE BOTH CURRENT AND THOROUGH COVERAGE OF THIS IMPORTANT ANALYTICAL TECHNIQUE Static headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC. Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent developments and practices, and also includes coverage of solid-phase microextraction (SPME) and the purge-and-trap technique. Chapters cover: Principles of static and dynamic headspace analysis, including the evolution of HS-GC methods and regulatory methods using static HS-GC Basic theory of headspace analysis—physicochemical relationships, sensitivity, and the principles of multiple headspace extraction HS-GC techniques—vials, cleaning, caps, sample volume, enrichment, and cryogenic techniques Sample handling Cryogenic HS-GC Method development in HS-GC Nonequilibrium static headspace analysis Determination of physicochemical functions such as vapor pressures, activity coefficients, and more Comprehensive and focused, Static Headspace-Gas Chromatography, Second Edition provides an excellent resource to help the reader achieve optimal chromatographic results. Practical examples with original data help readers to master determinations in a wide variety of areas, such as forensic, environmental, pharmaceutical, and industrial applications.

Analytical Reaction Gas Chromatography

Author : Viktor G. Berezkin
Publisher : Springer Science & Business Media
ISBN 13 : 1468407090
Total Pages : 199 pages
Book Rating : 4.4/5 (684 download)

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Book Synopsis Analytical Reaction Gas Chromatography by : Viktor G. Berezkin

Download or read book Analytical Reaction Gas Chromatography written by Viktor G. Berezkin and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 199 pages. Available in PDF, EPUB and Kindle. Book excerpt: The most universal and effective method for the analysis of complex multicomponent mixtures of volatile substances is gas chromatography. However, there are a number of limitations asso ciated with the classical variation of this technique which retard its development and the further expansion of its application: 1) the identification of the components of a complex mix ture of unknown composition is in itself a complex and difficult problem, unless the homologous series of the component to be identified is known; 2) the overlapping of chromatographic peaks for several compounds makes it difficult, and in a number of cases impossible, to carry out qualitative and quantitative analysis of these components, and leads to the necessity of using several columns of different polarities or to the use of columns with very high efficiency; 3) the direct analysis of unstable and nonvolatile compounds is impossible; 4) the difficulty of quantitative chromatographic analysis using thermal conductivity detectors increases with the necessity of determining individual response (calibration) factors; the insensitivity of the flame ionization detector to a number of substances (inorganic gases) leads to the necessity of introducing additional operations (prelimi nary concentration of trace components) in connection with thermal conductivity detectors. vii viii FOREWORD The directed use of chemical conversion of the compounds analyzed usually makes it possible to remove the limitations cited above.

Split and Splitless Injection for Quantitative Gas Chromatography

Author : Konrad Grob
Publisher : John Wiley & Sons
ISBN 13 : 3527612882
Total Pages : 480 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Split and Splitless Injection for Quantitative Gas Chromatography by : Konrad Grob

Download or read book Split and Splitless Injection for Quantitative Gas Chromatography written by Konrad Grob and published by John Wiley & Sons. This book was released on 2008-11-21 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated. This new edition offers: - New insights concerning sample evaporation in the injector - Information about matrix effects - A new chapter on injector design The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book. Furthermore the reader will understand the concepts of injection techniques and get a knowledge of the sources of error. The handbook also includes many practical guidelines. From reviews of former editions: "This substantial book is on injection techniques alone, which ... demonstrates this can have many pitfalls ... no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book ..." The Analyst "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day-to-day world of the working gas chromatographer. It will be useful ... for anyone who must work hands-on with GC." Journal of High Resolution Chromatography

Introduction to Analytical Gas Chromatography, Revised and Expanded

Author : Raymond P.W. Scott
Publisher : CRC Press
ISBN 13 : 1351990985
Total Pages : 401 pages
Book Rating : 4.3/5 (519 download)

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Book Synopsis Introduction to Analytical Gas Chromatography, Revised and Expanded by : Raymond P.W. Scott

Download or read book Introduction to Analytical Gas Chromatography, Revised and Expanded written by Raymond P.W. Scott and published by CRC Press. This book was released on 2017-12-19 with total page 401 pages. Available in PDF, EPUB and Kindle. Book excerpt: Covering the principles of chromatographic separation, the chromatographic process from a physical chemical perspective, instrumentation for performing analyses, and operational procedures, this second edition offers information needed for the successful practice of gas chromatography. It contains examples of available apparatus, detectors, columns, stationary phases and operating conditions.