Hyphenated Techniques in Supercritical Fluid Chromatography and Extraction

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Publisher : Elsevier
ISBN 13 : 0080858619
Total Pages : 345 pages
Book Rating : 4.0/5 (88 download)

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Book Synopsis Hyphenated Techniques in Supercritical Fluid Chromatography and Extraction by : K. Jinno

Download or read book Hyphenated Techniques in Supercritical Fluid Chromatography and Extraction written by K. Jinno and published by Elsevier. This book was released on 1992-07-21 with total page 345 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the first book to focus on the latest developments in hyphenated techniques using supercritical fluids. The advantages of SFC in hyphenation with various detection modes, such as FTIR, MS, MPD and ICP and others are clearly featured throughout the book. Special attention is paid to coupling of SFE with GC or SFC.In this edited volume, chapters are written by leading experts in the field. The book will be of interest to professionals in academia, as well as to those researchers working in an industrial environment, such as analytical instrumentation, pharmaceuticals, agriculture, food, petrochemicals and environmental.

Analysis with Supercritical Fluids: Extraction and Chromatography

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Publisher : Springer Science & Business Media
ISBN 13 : 3642774741
Total Pages : 225 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Analysis with Supercritical Fluids: Extraction and Chromatography by : Bernd Wenclawiak

Download or read book Analysis with Supercritical Fluids: Extraction and Chromatography written by Bernd Wenclawiak and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 225 pages. Available in PDF, EPUB and Kindle. Book excerpt: The use of supercritical fluids in analytical chemistry is still grow ing. More and more analysts are discovering the favorable advan tages for a number of applications. Especially supercritical fluid extraction (SFE) has attracted a lot of interest in recent years due to its simplicity. Supercritical fluid chromatography (SFC) has become better established and the development of this technique has been accelerated by the many applications with capillary col umns which have been published in the literature. At first SFC equipment was based on instruments commonly used for liquid chromatography, and the first commercial in struments were derived from this technology. However, capillary columns can be much more easily interfaced to gas chromatogra phy equipment especially to the detectors commonly used for Oc. Many stationary phases both for packed micro columns and capillary columns have been designed for SFC purposes extending this technology to LC and OC. The most common fluid applied in SFC and SFE is carbon dioxide. The advantages of supercritical CO , such as having dif 2 fusivity like a gas and solvating power depending on temperature and pressure, are also valid for other fluids and modified fluids. Both properties are valuable for sample extraction and extraction selectivity.

Supercritical Fluids in Chromatography and Extraction

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Author :
Publisher : Elsevier Science Limited
ISBN 13 : 9780444828699
Total Pages : 404 pages
Book Rating : 4.8/5 (286 download)

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Book Synopsis Supercritical Fluids in Chromatography and Extraction by : R. M. Smith

Download or read book Supercritical Fluids in Chromatography and Extraction written by R. M. Smith and published by Elsevier Science Limited. This book was released on 1997 with total page 404 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the mid 1980s supercritical fluid chromatography (SFC) arose with considerable fanfare as the new technique which would shortly "displace HPLC" and become the "universal separation method". After the initial hype had passed, there has still remained a significant group of applications in both chromatography and extraction for which supercritical fluids are the most suitable solvents. These form the basis of this volume, which illustrates the present state of analytical supercritical technology by a collection of review and research papers. Many publications in this field have blurred the boundaries of supercritical fluids, claiming that they filled a gap between gases and liquids and "had the properties of both". This was never true and this book seeks a more rational view of the state of application of supercritical fluids as their position in the analytical laboratory becomes clearer. These papers emphasise that future chromatographers should not be compartmentalised into "gas chromatographers" or "liquid chromatographers" but should view the field as a series of merging separation techniques. The overall emphasis is on extraction methods, usually as a sample preparation method prior to HPLC or GC analysis, but in some cases the extract is examined directly as the analytical step. This bias on extraction methods reflects the impact of supercritical fluids in the working laboratory. It is therefore an area where advances can have the maximum benefit for the user. The papers on chromatography are diverse and adventurous, covering particularly chiral chromatography and metal complex analysis, where SFC offers particular advantages over existing methods. Rather than be a separate branch of chromatography or extractions it is clear that the use of solvents above their normal conditions of temperature and pressure, up to and including the supercritical state, will continue to expand the range of analytical methods as part of an overall spectrum of solubility, polarity and volatility properties of solvents and mobile phases. This volume is an important addition to this movement and will help to redress the lack of education in the theory and practice of sample preparation which has been a great limiting factor for SFC and SFE.

Chromatographie

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Publisher : Encyclopaedia Universalis
ISBN 13 : 234100315X
Total Pages : 78 pages
Book Rating : 4.3/5 (41 download)

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Book Synopsis Chromatographie by : Encyclopaedia Universalis,

Download or read book Chromatographie written by Encyclopaedia Universalis, and published by Encyclopaedia Universalis. This book was released on 2016-09-19 with total page 78 pages. Available in PDF, EPUB and Kindle. Book excerpt: La chromatographie est une méthode d'analyse chimique (cf. chimie analytique ) consistant à séparer les constituants d'un mélange. Elle est utilisée aussi bien dans les services de recherche et développement que dans le domaine du contrôle. Son champ d'activité couvre les organismes d'État et le...

Analysis with Supercritical Fluids

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Publisher :
ISBN 13 : 9783642774751
Total Pages : 232 pages
Book Rating : 4.7/5 (747 download)

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Book Synopsis Analysis with Supercritical Fluids by : Bernd Wenclawiak

Download or read book Analysis with Supercritical Fluids written by Bernd Wenclawiak and published by . This book was released on 1992-11-03 with total page 232 pages. Available in PDF, EPUB and Kindle. Book excerpt: The editor has brought together in a compact and readable form the new methods of analytical chemistry using supercritical fluids. The volume provides comprehensive treatment of supercritical fluid chromatography (SFC) and supercritical fluid extraction (SFE); it discusses both theory and practice. The contributions are written by leading experts in their fields with exhaustive practical experience in SFC and SFE. Special attention is given to the description of applications and thus provides the experienced analyst with invaluable information widely scattered in the literature and helps the novice to adopt these new techniques quickly in his laboratory. An addendum includes brand new literature on SFC and SFE.

Modern Supercritical Fluid Chromatography

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Publisher : John Wiley & Sons
ISBN 13 : 1119625998
Total Pages : 417 pages
Book Rating : 4.1/5 (196 download)

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Book Synopsis Modern Supercritical Fluid Chromatography by : Larry M. Miller

Download or read book Modern Supercritical Fluid Chromatography written by Larry M. Miller and published by John Wiley & Sons. This book was released on 2019-11-05 with total page 417 pages. Available in PDF, EPUB and Kindle. Book excerpt: Explains why modern supercritical fluid chromatography (SFC) is the leading "green" analytical and purification separations technology. Modern supercritical fluid chromatography (SFC) is the leading method used to analyze and purify chiral and achiral chemical compounds, many of which are pharmaceuticals, pharmaceutical candidates, and natural products including cannabis-related compounds. This book covers current SFC instrumentation as it relates to greater robustness, better reproducibility, and increased analytical sensitivity. Modern Supercritical Fluid Chromatography: Carbon Dioxide Containing Mobile Phases covers the history, instrumentation, method development and applications of SFC. The authors provided readers with an overview of analytical and preparative SFC equipment, stationary phases, and mobile phase choices. Topics covered include: Milestones of Supercritical Fluid Chromatography; Physical Properties of Supercritical Fluids; Instrumentation for SFC; Detection in SFC; Achiral SFC Method Development; Chiral SFC Method Development; and Preparative Scale SFC. The book also includes highlights of modern applications of SFC in the final chapters—namely pharmaceuticals, consumer products, foods, polymers, petroleum-related mixtures, and cannabis—and discusses the future of SFC. Provides a clear explanation of the physical and chemical properties of supercritical fluids, which gives the reader a better understanding of the basis for improved performance in SFC compared to HPLC and GC Describes the advantages of SFC as a green alternative to HPLC and GC for the analysis of both polar, water-soluble, and non-polar analytes Details both achiral and chiral SFC method development, including modifiers, additives, the impact of temperature and pressure, and stationary phase choices Details why SFC is the premier modern preparative chromatographic technique used to purify components of mixtures for subsequent uses, both from performance and economic perspectives Covers numerous detectors, with an emphasis on SFC-MS, SFC-UV, and SFC-ELSD (evaporative light scattering detection) Describes the application of SFC to numerous high-value application areas Modern Supercritical Fluid Chromatography: Carbon Dioxide Containing Mobile Phases will be of great interest to professionals, students, and professors involved in analytical, bioanalytical, separations science, medicinal, petroleum, and environmental chemistries. It will also appeal to pharmaceutical scientists, natural-product scientists, food and consumer-products scientists, chemical engineers, and managers in these areas.

Supercritical Fluid Chromatography for the Analysis of Nitroaromatics, Nitramines and Nitrate Esters

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Publisher :
ISBN 13 :
Total Pages : 26 pages
Book Rating : 4.:/5 (319 download)

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Book Synopsis Supercritical Fluid Chromatography for the Analysis of Nitroaromatics, Nitramines and Nitrate Esters by : Paul H. Miyares

Download or read book Supercritical Fluid Chromatography for the Analysis of Nitroaromatics, Nitramines and Nitrate Esters written by Paul H. Miyares and published by . This book was released on 1992 with total page 26 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Element-specific Chromatographic Detection by Atomic Emission Spectroscopy

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Publisher :
ISBN 13 :
Total Pages : 368 pages
Book Rating : 4.:/5 (44 download)

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Book Synopsis Element-specific Chromatographic Detection by Atomic Emission Spectroscopy by : Peter C. Uden

Download or read book Element-specific Chromatographic Detection by Atomic Emission Spectroscopy written by Peter C. Uden and published by . This book was released on 1992 with total page 368 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first book to specifically cover interfaced chromatographic separations and element-specific detection by AES. Offers fundamental research studies and reviews by the most active groups in the field, including those involved in instrument development. Discusses a wide variety of techniques, including LC/GC, SFC, atomic emission spectroscopy, plasma spectroscopy, microwave induced plasmas, inductively coupled plasmas, direct current plasmas, and inductively coupled plasma/mass spectroscopy.

Chromatographic Detectors

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Publisher : CRC Press
ISBN 13 : 148227356X
Total Pages : 533 pages
Book Rating : 4.4/5 (822 download)

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Book Synopsis Chromatographic Detectors by : Raymond P.W. Scott

Download or read book Chromatographic Detectors written by Raymond P.W. Scott and published by CRC Press. This book was released on 1996-07-17 with total page 533 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Comprehensively covers the design, construction, and operation of gas chromatography, liquid chromatography, and thin-layer chromatography detectors--all in one convenient, up-to-date source. Emphasizes the essential use of common specifications to describe all detectors, allowing easy comparison of their attributes."

Supercritical Fluid Extraction and Chromatography

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Publisher :
ISBN 13 :
Total Pages : 272 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Supercritical Fluid Extraction and Chromatography by : Bonnie A. Charpentier

Download or read book Supercritical Fluid Extraction and Chromatography written by Bonnie A. Charpentier and published by . This book was released on 1988 with total page 272 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Diode Array Detection in HPLC

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Publisher : CRC Press
ISBN 13 : 9780824789473
Total Pages : 416 pages
Book Rating : 4.7/5 (894 download)

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Book Synopsis Diode Array Detection in HPLC by : Ludwig Huber

Download or read book Diode Array Detection in HPLC written by Ludwig Huber and published by CRC Press. This book was released on 1993-04-28 with total page 416 pages. Available in PDF, EPUB and Kindle. Book excerpt: This resource discusses the principles and techniques of diode array detectors, compares them to conventional absorbance detectors, and examines their applications in high-performance liquid chromatography.;Providing guidelines on how to optimize diode array detectors for high sensitivity, selectivity, linearity and automation, Diode Array Detection in HPLC presents: early developments in diode array technology; current areas of application; computer techniques for spectral library searching; the mathematical basis of spectral deconvolution; practical uses of ultraviolet spectra for peak purity control and peak confirmation; chromatographic examples for HPLC applications, and more.;Diode Array Detection in HPLC is a practical guide for analytical, food, and pharmaceutical chemists and biochemists; analytical laboratory managers, consultants, and operators; and upper-level undergraduate, graduate, and continuing-education students in these disciplines.

Selective Gas Chromatographic Detectors

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Publisher : Elsevier Publishing Company
ISBN 13 : 9780444424884
Total Pages : 319 pages
Book Rating : 4.4/5 (248 download)

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Book Synopsis Selective Gas Chromatographic Detectors by : M. Dressler

Download or read book Selective Gas Chromatographic Detectors written by M. Dressler and published by Elsevier Publishing Company. This book was released on 1986-01-01 with total page 319 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book gives a comprehensive, up-to-date review of all selective detectors used in combination with gas chromatography. For each detector, the historical background, design and principle are described, and the working parameters affecting the detector performance are analyzed critically and in detail. The analytical possibilities of the detectors and the main characteristics such as sensitivity, noise and minimum detectability are discussed. All the selective detectors that are currently used are discussed in detail. Combinations of GC with other techniques such as plasma emission spectroscopy, atomic absorption spectrometry, ion-selective electrodes, piezoelectric sorption detector, mass spectrometry and infrared spectroscopy are discussed briefly. Chromatographers and users of gas chromatographs, especially in the field of environmental protection, agriculture, clinical chemistry, and toxicology will find the book useful to their work. Institutes and organisations dealing with analytical chemistry will also find it of interest.