Fast Scanning Calorimetry

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Fast Scanning Calorimetry

Author : Christoph Schick
Publisher : Springer
ISBN 13 : 3319313290
Total Pages : 801 pages
Book Rating : 4.3/5 (193 download)

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Book Synopsis Fast Scanning Calorimetry by : Christoph Schick

Download or read book Fast Scanning Calorimetry written by Christoph Schick and published by Springer. This book was released on 2016-06-28 with total page 801 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the past decades, the scan rate range of calorimeters has been extended tremendously at the high end, from approximately 10 up to 10 000 000 °C/s and more. The combination of various calorimeters and the newly-developed Fast Scanning Calorimeters (FSC) now span 11 orders of magnitude, by which many processes can be mimicked according to the time scale(s) of chemical and physical transitions occurring during cooling, heating and isothermal stays in case heat is exchanged. This not only opens new areas of research on polymers, metals, pharmaceuticals and all kinds of substances with respect to glass transition, crystallization and melting phenomena, it also enables in-depth study of metastability and reorganization of samples on an 1 to 1000 ng scale. In addition, FSC will become a crucial tool for understanding and optimization of processing methods at high speeds like injection molding. The book resembles the state-of-the art in Thermal Analysis & Calorimetry and is an excellent starting point for both experts and newcomers in the field.

Handbook of Thermal Analysis and Calorimetry

Author :
Publisher : Elsevier
ISBN 13 : 0444640630
Total Pages : 860 pages
Book Rating : 4.4/5 (446 download)

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Book Synopsis Handbook of Thermal Analysis and Calorimetry by :

Download or read book Handbook of Thermal Analysis and Calorimetry written by and published by Elsevier. This book was released on 2018-03-12 with total page 860 pages. Available in PDF, EPUB and Kindle. Book excerpt: Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications

Differential Scanning Calorimetry

Author : G.W.H. Höhne
Publisher : Springer Science & Business Media
ISBN 13 : 366203302X
Total Pages : 233 pages
Book Rating : 4.6/5 (62 download)

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Book Synopsis Differential Scanning Calorimetry by : G.W.H. Höhne

Download or read book Differential Scanning Calorimetry written by G.W.H. Höhne and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 233 pages. Available in PDF, EPUB and Kindle. Book excerpt: Differential Scanning Calorimetry (DSC) is a well established measuring method which is used on a large scale in different areas of research, development, and quality inspection and testing. Over a large temperature range, thermal effects can be quickly identified and the relevant temperature and the characteristic caloric values determined using substance quantities in the mg range. Measurement values obtained by DSC allow heat capacity, heat of transition, kinetic data, purity and glass transition to be determined. DSC curves serve to identify substances, to set up phase diagrams and to determine degrees of crystallinity. This book provides, for the first time, an overall description of the most impor tant applications of Differential Scanning Calorimetry. Prerequisites for reliable measurement results, optimum evaluation of the measurement curves and esti mation of the uncertainties of measurement are, however, the knowledge of the theoretical bases of DSC, a precise calibration of the calorimeter and the correct analysis of the measurement curve. The largest part of this book deals with these basic aspects: The theory of DSC is discussed for both heat flux and power compensated instruments; temperature calibration and caloric calibration are described on the basis of thermodynamic principles. Desmearing of the measurement curve in different ways is presented as a method for evaluating the curves of fast transitions.

Principles and Applications of Thermal Analysis

Author : Paul Gabbott
Publisher : John Wiley & Sons
ISBN 13 : 0470698128
Total Pages : 480 pages
Book Rating : 4.4/5 (76 download)

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Book Synopsis Principles and Applications of Thermal Analysis by : Paul Gabbott

Download or read book Principles and Applications of Thermal Analysis written by Paul Gabbott and published by John Wiley & Sons. This book was released on 2008-04-30 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Handbook of Differential Scanning Calorimetry

Author : Joseph D Menczel
Publisher : Butterworth-Heinemann
ISBN 13 : 0128113480
Total Pages : 876 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Handbook of Differential Scanning Calorimetry by : Joseph D Menczel

Download or read book Handbook of Differential Scanning Calorimetry written by Joseph D Menczel and published by Butterworth-Heinemann. This book was released on 2023-02-22 with total page 876 pages. Available in PDF, EPUB and Kindle. Book excerpt: Differential scanning calorimetry (DSC) is the most important thermal analysis technique used today and the most common thermal analysis instrument found in chemical characterization laboratories. DSC has become an everyday tool in characterization laboratories, but many researchers using this technique have a limited understanding of the true breadth of its capabilities. Up to now, there has been no book that would describe the application of DSC in all the various areas of materials chemistry. The Handbook of Differential Scanning Calorimetry has been written to fill that void. This book is designed to summarize the knowledge of differential scanning calorimetry so that materials researchers and application chemists are given both a better understanding of techniques , as well as a review of the full scope of its capabilities. It also discusses how to properly interpret the DSC thermograms data obtained. Included in this work is the most up-to-date information written by some of the leaders in the field. It is written not only to help users get the most out of their equipment, After reading this book, people in all chemical and biological areas will have a broad overview of this measuring technique, and will be able to utilize this analytical technique more efficiently. Provides a detail description of the theory behind differential scanning while simultaneously providing a wider breadth of understanding of the actual DSC technique Includes a review of the basics of heat flux and power compensation DSC’s, as well as separate chapters on inorganic and organic materials Reviews the most common commercial DSC instruments on the market and their uses, including TA Instruments, Perkin-Elmer, Hitachi, Mettler Toledo, Netzsch, and Setaram

Assignment of the Glass Transition

Author : Rickey J. Seyler
Publisher : ASTM International
ISBN 13 : 080311995X
Total Pages : 310 pages
Book Rating : 4.8/5 (31 download)

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Book Synopsis Assignment of the Glass Transition by : Rickey J. Seyler

Download or read book Assignment of the Glass Transition written by Rickey J. Seyler and published by ASTM International. This book was released on 1994 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Thermal Analysis of Polymers

Author : Joseph D. Menczel
Publisher : John Wiley & Sons
ISBN 13 : 1118995996
Total Pages : 696 pages
Book Rating : 4.1/5 (189 download)

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Book Synopsis Thermal Analysis of Polymers by : Joseph D. Menczel

Download or read book Thermal Analysis of Polymers written by Joseph D. Menczel and published by John Wiley & Sons. This book was released on 2014-07-09 with total page 696 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents a solid introduction to thermal analysis, methods,instrumentation, calibration, and application along with thenecessary theoretical background. Useful to chemists, physicists, materials scientists, andengineers who are new to thermal analysis techniques, and toexisting users of thermal analysis who wish expand their experienceto new techniques and applications Topics covered include Differential Scanning Calorimetry andDifferential Thermal Analysis (DSC/DTA), Thermogravimetry,Thermomechanical Analysis and Dilatometry, Dynamic MechanicalAnalysis, Micro-Thermal Analysis, Hot Stage Microscopy, andInstrumentation. Written by experts in the various areas of thermalanalysis Relevant and detailed experiments and examples follow eachchapter.

Thermal Analysis

Author : El-Zeiny Ebeid
Publisher : Elsevier
ISBN 13 : 0323901921
Total Pages : 324 pages
Book Rating : 4.3/5 (239 download)

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Book Synopsis Thermal Analysis by : El-Zeiny Ebeid

Download or read book Thermal Analysis written by El-Zeiny Ebeid and published by Elsevier. This book was released on 2021-06-23 with total page 324 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry. Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management. Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs Contains chapters that cover the user of TA in materials science and crystal structures

Solid State Development and Processing of Pharmaceutical Molecules

Author : Michael Gruss
Publisher : John Wiley & Sons
ISBN 13 : 352734635X
Total Pages : 578 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Solid State Development and Processing of Pharmaceutical Molecules by : Michael Gruss

Download or read book Solid State Development and Processing of Pharmaceutical Molecules written by Michael Gruss and published by John Wiley & Sons. This book was released on 2021-11-15 with total page 578 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid State Development and Processing of Pharmaceutical Molecules A guide to the lastest industry principles for optimizing the production of solid state active pharmaceutical ingredients Solid State Development and Processing of Pharmaceutical Molecules is an authoritative guide that covers the entire pharmaceutical value chain. The authors—noted experts on the topic—examine the importance of the solid state form of chemical and biological drugs and review the development, production, quality control, formulation, and stability of medicines. The book explores the most recent trends in the digitization and automation of the pharmaceutical production processes that reflect the need for consistent high quality. It also includes information on relevant regulatory and intellectual property considerations. This resource is aimed at professionals in the pharmaceutical industry and offers an in-depth examination of the commercially relevant issues facing developers, producers and distributors of drug substances. This important book: Provides a guide for the effective development of solid drug forms Compares different characterization methods for solid state APIs Offers a resource for understanding efficient production methods for solid state forms of chemical and biological drugs Includes information on automation, process control, and machine learning as an integral part of the development and production workflows Covers in detail the regulatory and quality control aspects of drug development Written for medicinal chemists, pharmaceutical industry professionals, pharma engineers, solid state chemists, chemical engineers, Solid State Development and Processing of Pharmaceutical Molecules reviews information on the solid state of active pharmaceutical ingredients for their efficient development and production.

TMS 2019 148th Annual Meeting & Exhibition Supplemental Proceedings

Author : & The Minerals, Metals Materials Society
Publisher : Springer
ISBN 13 : 3030058611
Total Pages : 1731 pages
Book Rating : 4.0/5 (3 download)

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Book Synopsis TMS 2019 148th Annual Meeting & Exhibition Supplemental Proceedings by : & The Minerals, Metals Materials Society

Download or read book TMS 2019 148th Annual Meeting & Exhibition Supplemental Proceedings written by & The Minerals, Metals Materials Society and published by Springer. This book was released on 2019-02-26 with total page 1731 pages. Available in PDF, EPUB and Kindle. Book excerpt: This collection features papers presented at the 148th Annual Meeting & Exhibition of The Minerals, Metals & Materials Society.

Thermal Analysis of Polymeric Materials

Author : Krzysztof Pielichowski
Publisher : John Wiley & Sons
ISBN 13 : 3527828702
Total Pages : 878 pages
Book Rating : 4.5/5 (278 download)

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Book Synopsis Thermal Analysis of Polymeric Materials by : Krzysztof Pielichowski

Download or read book Thermal Analysis of Polymeric Materials written by Krzysztof Pielichowski and published by John Wiley & Sons. This book was released on 2022-06-01 with total page 878 pages. Available in PDF, EPUB and Kindle. Book excerpt: An all-in-one reference work covering the essential principles and techniques on thermal behavior and response of polymeric materials This book delivers a detailed understanding of the thermal behavior of polymeric materials evaluated by thermal analysis methods. It covers the most widely applied principles which are used in method development to substantiate what happens upon heating of polymers. It also reviews the key application areas of polymers in materials science. Edited by two experts in the field, the book covers a wide range of specific topics within the aforementioned categories of discussion, such as: Crucial thermal phenomena - glass transition, crystallization behavior and curing kinetics Polymeric materials that have gained considerable interest over the last decade The latest advancements in techniques related to the field, such as modulated temperature DSC and fast scanning calorimetry The recent advances in hyphenated techniques and their applications Polymer chemists, chemical engineers, materials scientists, and process engineers can use this comprehensive reference work to gain clarity on the topics discussed within and learn how to harness them in practical applications across a wide range of disciplines.

Glass

Author : Jürn W. P. Schmelzer
Publisher : Walter de Gruyter
ISBN 13 : 3110298589
Total Pages : 610 pages
Book Rating : 4.1/5 (12 download)

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Book Synopsis Glass by : Jürn W. P. Schmelzer

Download or read book Glass written by Jürn W. P. Schmelzer and published by Walter de Gruyter. This book was released on 2014-05-08 with total page 610 pages. Available in PDF, EPUB and Kindle. Book excerpt: “This book contains overviews on technologically important classes of glasses, their treatment to achieve desired properties, theoretical approaches for the description of structure-property relationships, and new concepts in the theoretical treatment of crystallization in glass-forming systems. It contains overviews about the state of the art and about specific features for the analysis and application of important classes of glass-forming systems, and describes new developments in theoretical interpretation by well-known glass scientists. Thus, the book offers comprehensive and abundant information that is difficult to come by or has not yet been made public.” Edgar Dutra Zanotto (Center for Research, Technology and Education in Vitreous Materials, Brazil) Glass, written by a team of renowned researchers and experienced book authors in the field, presents general features of glasses and glass transitions. Different classes of glassforming systems, such as silicate glasses, metallic glasses, and polymers, are exemplified. In addition, the wide field of phase formation processes and their effect on glasses and their properties is studied both from a theoretical and experimental point of view.

Principles of Thermal Analysis and Calorimetry

Author : Peter J. Haines
Publisher : Royal Society of Chemistry
ISBN 13 : 9780854046102
Total Pages : 244 pages
Book Rating : 4.0/5 (461 download)

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Book Synopsis Principles of Thermal Analysis and Calorimetry by : Peter J. Haines

Download or read book Principles of Thermal Analysis and Calorimetry written by Peter J. Haines and published by Royal Society of Chemistry. This book was released on 2002 with total page 244 pages. Available in PDF, EPUB and Kindle. Book excerpt: The use of thermal and calorimetric methods has shown rapid growth over the last two decades, in an increasingly wide range of applications. In addition, a number of powerful new techniques have been developed. This book supplies a concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Brief accounts of the basic theory are reinforced with detailed applications of the methods and contemporary developments. Also included is information on standard test methods and manufacturers. Written by acknowledged experts, Principles of Thermal Analysis and Calorimetry is up-to-date, wide-ranging and practical. It will be an important source of information for many levels of readership in a variety of areas, from students and lecturers through to industrial and laboratory staff and consultants.

Who is Who in Thermal Analysis and Calorimetry

Author : Imre Miklós Szilágyi
Publisher : Springer
ISBN 13 : 3319094866
Total Pages : 363 pages
Book Rating : 4.3/5 (19 download)

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Book Synopsis Who is Who in Thermal Analysis and Calorimetry by : Imre Miklós Szilágyi

Download or read book Who is Who in Thermal Analysis and Calorimetry written by Imre Miklós Szilágyi and published by Springer. This book was released on 2014-11-18 with total page 363 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is an expanded and revised second edition, presenting accurate and comprehensive information about our leading thermal scientists to current and future generations. In our globalized world, most researchers in thermal analysis do not know each other in person and are not familiar with each other’s achievements. This volume provides the reader with an up-to-date list of the prominent members in this community. The publication contains only living scientists. The selection is based partly on several decades of the editors' personal professional experience and also partly on the opinion of the Regional Editors of the Journal of Thermal Analysis and Calorimetry.

Applications of Calorimetry in a Wide Context

Author : Amal Ali Elkordy
Publisher : BoD – Books on Demand
ISBN 13 : 9535109472
Total Pages : 488 pages
Book Rating : 4.5/5 (351 download)

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Book Synopsis Applications of Calorimetry in a Wide Context by : Amal Ali Elkordy

Download or read book Applications of Calorimetry in a Wide Context written by Amal Ali Elkordy and published by BoD – Books on Demand. This book was released on 2013-01-23 with total page 488 pages. Available in PDF, EPUB and Kindle. Book excerpt: Calorimetry, as a technique for thermal analysis, has a wide range of applications which are not only limited to studying the thermal characterisation (e.g. melting temperature, denaturation temperature and enthalpy change) of small and large drug molecules, but are also extended to characterisation of fuel, metals and oils. Differential Scanning Calorimetry is used to study the thermal behaviours of drug molecules and excipients by measuring the differential heat flow needed to maintain the temperature difference between the sample and reference cells equal to zero upon heating at a controlled programmed rate. Microcalorimetry is used to study the thermal transition and folding of biological macromolecules in dilute solutions. Microcalorimetry is applied in formulation and stabilisation of therapeutic proteins. This book presents research from all over the world on the applications of calorimetry on both solid and liquid states of materials.

Thermal Analysis and Thermodynamic Properties of Solids

Author : Jaroslav Sestak
Publisher : Elsevier
ISBN 13 : 0323858112
Total Pages : 646 pages
Book Rating : 4.3/5 (238 download)

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Book Synopsis Thermal Analysis and Thermodynamic Properties of Solids by : Jaroslav Sestak

Download or read book Thermal Analysis and Thermodynamic Properties of Solids written by Jaroslav Sestak and published by Elsevier. This book was released on 2021-08-09 with total page 646 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis and Thermodynamic Properties of Solids, Second Edition covers foundational principles and recent updates in the field, presenting an authoritative overview of theoretical knowledge and practical applications across several fields. Since the first edition of this book was published, large developments have occurred in the theoretical understanding of—and subsequent ability to assess and apply—principles of thermal analysis. Drawing on the knowledge of its expert author, this second edition provides fascinating insight for both new and experienced students, researchers, and industry professionals whose work is influenced or impacted by thermo analysis principles and tools. Part 1 provides a detailed introduction and guide to theoretical aspects of thermal analysis and the related impact of thermodynamics. Key terminology and concepts, the fundamentals of thermophysical examinations, thermostatics, equilibrium background, thermotics, reaction kinetics and models, thermokinetics and the exploitation of fractals are all discussed. Part 2 then goes on to discuss practical applications of this theoretical information to topics such as crystallization kinetics and glass states, thermodynamics in superconductor models, and climate change. Includes fully updated as well as new chapters on kinetic phase diagrams, thermokinetics in DTA experiments, and crystallization kinetics Discusses the influence of key derivatives such as thermostatics, thermodynamics, thermotics, and thermokinetics Helps readers understand and describe reaction kinetics in solids, both in terms of simplified descriptions of the reaction mechanism models and averaged descriptions using fractals

Modulated Temperature Differential Scanning Calorimetry

Author : Mike Reading
Publisher : Springer Science & Business Media
ISBN 13 : 1402037503
Total Pages : 340 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Modulated Temperature Differential Scanning Calorimetry by : Mike Reading

Download or read book Modulated Temperature Differential Scanning Calorimetry written by Mike Reading and published by Springer Science & Business Media. This book was released on 2006-10-12 with total page 340 pages. Available in PDF, EPUB and Kindle. Book excerpt: MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.