Volume 14 Analysis Of Petroleum For Trace Elements

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Oscillometry and Conductometry

Author : E. Pungor
Publisher : Elsevier
ISBN 13 : 1483156893
Total Pages : 256 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Oscillometry and Conductometry by : E. Pungor

Download or read book Oscillometry and Conductometry written by E. Pungor and published by Elsevier. This book was released on 2016-07-29 with total page 256 pages. Available in PDF, EPUB and Kindle. Book excerpt: Oscillometry and Conductometry deals with oscillometry and conductometry and covers topics ranging from the conductivity and dielectric constant of a solution and their determination, to instruments used in carrying out conductometric and oscillometric measurements. Acid-base titrations and titrations based on precipitation, complex formation, and redox reactions are also discussed. A number of applications of conductometry and oscillometry are considered. This volume is comprised of 18 chapters and begins with an overview of the fundamentals of electrical conductivity, its theoretical interpretation, and how it is affected by temperature. The relation between ionic interaction and conductivity of solutions is also described, with emphasis on the Wien effect and the Debye effect. The theoretical fundamentals of the determination of conductivity using direct and alternating currents are then outlined. Subsequent chapters explore the principles and the devices used in determining dielectric constants; conductometric and oscillometric instruments; the titration of acids and bases; and acid-base titrations in aqueous and non-aqueous media. The final section is devoted to applications of conductometry and oscillometry, including kinetic studies and chromatographic analysis. This monograph will be of interest to analytical chemists.

Principles of Field Ionization and Field Desorption Mass Spectrometry

Author : H. D. Beckey
Publisher : Elsevier
ISBN 13 : 1483156915
Total Pages : 355 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Principles of Field Ionization and Field Desorption Mass Spectrometry by : H. D. Beckey

Download or read book Principles of Field Ionization and Field Desorption Mass Spectrometry written by H. D. Beckey and published by Elsevier. This book was released on 2016-07-29 with total page 355 pages. Available in PDF, EPUB and Kindle. Book excerpt: Principles of Field Ionization and Field Desorption Mass Spectrometry delves deeper into field ionization and field desorption. The book covers the five main subareas of field ionization and field desorption mass spectrometry that has grown in importance. Coverage includes the theory of field ionization and field desorption; field ionization and field desorption techniques and sources; high field surface chemistry; kinetics and mechanisms of decompostion of field ions in the gas phase; and qualitative and mixture analysis with field ionization and field desorption mass spectrometry. The text is recommended for students, experts, and researchers in chemistry, especially those who wish to learn more or have an in-depth study about field ionization and field desorption, its principles, and its applications in chemistry.

Photoelectron Spectroscopy

Author : A. D. Baker
Publisher : Elsevier
ISBN 13 : 1483152367
Total Pages : 193 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Photoelectron Spectroscopy by : A. D. Baker

Download or read book Photoelectron Spectroscopy written by A. D. Baker and published by Elsevier. This book was released on 2013-10-22 with total page 193 pages. Available in PDF, EPUB and Kindle. Book excerpt: Photoelectron Spectroscopy provides an introduction to the principles of photoelectron spectroscopy, including its applications in structural and analytical chemistry. It deals with both X-ray and UV-photoelectron spectroscopy. This book begins with the basic principles of electron spectroscopy and describes the UV photoelectron spectrometers and X-ray photoelectron spectrometers. It then lists several factors influencing the appearance of the photoelectron spectra. This book concludes by describing other forms of electron spectroscopy and photoelectron techniques. Students and chemists who are looking for a readable introduction to photoelectron spectroscopy will find this book useful.

Indicators

Author : Edmund Bishop
Publisher : Elsevier
ISBN 13 : 1483151395
Total Pages : 759 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Indicators by : Edmund Bishop

Download or read book Indicators written by Edmund Bishop and published by Elsevier. This book was released on 2013-10-22 with total page 759 pages. Available in PDF, EPUB and Kindle. Book excerpt: Indicators offers a comprehensive account of indicators and their applications in areas such as titrimetric analysis and the analysis of mineral waters. The theory and principles of visual indicators are discussed, along with acid-base indicators, indicators for non-aqueous acid-base titrations, and titrations with non-chelating ligands. Metallochromic indicators, adsorption indicators, oxidation-reduction indicators, and fluorescent and chemiluminescent indicators are also considered. This volume is comprised of 10 chapters and begins with a brief history of indicators, including the contribution of Robert Boyle in the field. The different kinds of indicators are also described, along with developments in indicators in the nineteenth century. The next chapter deals with the theory and principles of visual indicators, followed by a discussion on acid-base indicators such as organic dyes, inorganic substances, compounds capable of fluorescence, and chemiluminescent systems. Subsequent chapters explore other varieties of indicators, including indicators for non-aqueous acid-base titrations, metallochromic indicators, and adsorption indicators, as well as oxidation-reduction indicators and fluorescent and chemiluminescent indicators. This book will be of interest to chemists.

Analytical Chemistry in Space

Author : Richard E. Wainerdi
Publisher : Elsevier
ISBN 13 : 1483157725
Total Pages : 296 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Analytical Chemistry in Space by : Richard E. Wainerdi

Download or read book Analytical Chemistry in Space written by Richard E. Wainerdi and published by Elsevier. This book was released on 2013-10-22 with total page 296 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Chemistry in Space presents an analysis of the chemical constitution of space, particularly the particles in the solar wind, of the planetary atmospheres, and the surfaces of the moon and planets. Topics range from space engineering considerations to solar system atmospheres and recovered extraterrestrial materials. Mass spectroscopy in space exploration is also discussed, along with lunar and planetary surface analysis using neutron inelastic scattering. This book is comprised of seven chapters and opens with a discussion on the possibilities for exploration of the solar system by mass spectroscopy, with particular reference to analysis of compositional data on solar system objects such as the Earth and meteorites, asteroids, comets, and interplanetary dust. The reader is then introduced to the project administration, instrument design, and spacecraft integration problems that must be solved to successfully fly a space experiment. The following chapters focus on the atmospheres of the sun and planets; the use of mass spectroscopy in solar system exploration and of neutron inelastic scattering in lunar and planetary surface analysis; and extraterrestrial in situ 14 MeV neutron activation analysis. The final chapter is devoted to the advantages and applications of thermal neutron activation to the analysis of certain samples of geological interest. This monograph will be a useful resource for analytical chemists and space scientists.

Elemental Analysis of Fuels and Lubricants

Author : R. A. Nadkarni
Publisher : ASTM International
ISBN 13 : 0803134940
Total Pages : 282 pages
Book Rating : 4.8/5 (31 download)

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Book Synopsis Elemental Analysis of Fuels and Lubricants by : R. A. Nadkarni

Download or read book Elemental Analysis of Fuels and Lubricants written by R. A. Nadkarni and published by ASTM International. This book was released on 2005 with total page 282 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Thermometric Titrimetry

Author : L. S. Bark
Publisher : Elsevier
ISBN 13 : 1483157423
Total Pages : 139 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Thermometric Titrimetry by : L. S. Bark

Download or read book Thermometric Titrimetry written by L. S. Bark and published by Elsevier. This book was released on 2016-10-27 with total page 139 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermometric Titrimetry covers the significant progress in the application of thermometric titrimetry to routine analysis and as a research tool in the investigations of the basic phenomena associated with chemical reactions. This book is composed of 10 chapters and starts with a brief presentation of the basic principles of the technique. The succeeding chapters deal with the apparatus and several reactions involved in thermometric titrimetry, including neutralization, oxidation-reduction, and precipitation. A chapter focuses on the advantages of the technique for the determination of important commercial chemical, such as water and various chemical systems. The remaining chapters examine the use of some solvents as indicators, the industrial application of thermometric titrimetry, and an investigation of complex formation. This book will be of great value to analytical and laboratory chemists.

N-Benzoylphenylhydroxylamine and Its Analogues

Author : A. K. Majumdar
Publisher : Elsevier
ISBN 13 : 1483278638
Total Pages : 223 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis N-Benzoylphenylhydroxylamine and Its Analogues by : A. K. Majumdar

Download or read book N-Benzoylphenylhydroxylamine and Its Analogues written by A. K. Majumdar and published by Elsevier. This book was released on 2017-07-19 with total page 223 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series of Monographs in Analytical Chemistry, Volume 50: N-Benzoylphenylhydroxylamine and its Analogues covers the analytical applications of the organic hydroxylamine derivatives. This book is composed of seven chapters, and starts with a brief historical account of the uses of organic reagents in inorganic analysis. The next chapter discusses some basic physico-chemical factors associated with the constitution of a good reagent, including some fundamental ideas about the type and nature of the principal reactive and other groupings in the ligand. A chapter deals with the inclusion of the methods of preparation and properties of N-benzoylphenylhydroxylamine (BPHA) and its analogues and derivatives, and their reactions with different metal ions. These topics are followed by descriptions of the various types of analytical applications of BPHA and its analogues, such as gravimetry, spectrophotometry, and solvent extraction, as well as their applications in titrimetry and paper chromatography. This book is of value to analytical and organic chemists.

Analytical Applications of EDTA and Related Compounds

Author : R. Přibil
Publisher : Elsevier
ISBN 13 : 1483158594
Total Pages : 391 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Analytical Applications of EDTA and Related Compounds by : R. Přibil

Download or read book Analytical Applications of EDTA and Related Compounds written by R. Přibil and published by Elsevier. This book was released on 2013-09-17 with total page 391 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Applications of EDTA and Related Compounds examines the analytical applications of ethylenediaminetetra-acetic acid (EDTA) and related compounds. This book also considers the "passive role of these substances, that is, their screening (masking) properties, which greatly improve the selectivity of the reactions in common use. This text consists of six chapters organized into two sections. The first part deals with the uses of EDTA and its derivatives in some fields of chemical analysis. After providing an overview of the history behind the development of EDTA as an analytical reagent, this book discusses to the nature of equilibria of complexes and the methods used in their investigation. The next chapter is dedicated to the reactions of "classical gravimetric analysis, including the precipitation reactions by means of organic reagents. The chapter on colorimetry includes a section on "colored complexing agents, which can be used also in colorimetric determinations of some elements. This text concludes by evaluating the use of EDTA as a masking agent in colorimetry. This book will be of interest to students and practitioners working in analytical chemistry and related disciplines, including polarography, chromatography, electrophoresis, flame photometry, and qualitative analysis.

The Determination of Impurities in Nuclear Grade Sodium Metal

Author : Louis Silverman
Publisher : Elsevier
ISBN 13 : 1483278719
Total Pages : 156 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis The Determination of Impurities in Nuclear Grade Sodium Metal by : Louis Silverman

Download or read book The Determination of Impurities in Nuclear Grade Sodium Metal written by Louis Silverman and published by Elsevier. This book was released on 2013-10-22 with total page 156 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series of Monographs in Analytical Chemistry, Volume 44: The Determination of Impurities in Nuclear Grade Sodium Metal (and Related Sodium Compounds) provides analytical chemical procedures for the determination of impurities in nuclear grade sodium metal. This book is composed of 25 chapters, and begins with a presentation of the methods for dissolving, bulk separation, sampling, and handling of sodium metal. The rest of the book describes the procedures for impurity determination in nuclear grade sodium metals, including aluminum, bismuth, boron, cadmium, calcium, magnesium, carbon, cesium, and chloride. Other impurities considered include chromium, cobalt, copper, hydrogen, iodine, iron, lead, lithium, manganese, nickel, oxide, oxygen, and phosphorus. The last chapters examine the procedures for determination of potassium, silicon, sulfur, and uranium impurities. This book is of value to analytical and inorganic chemists.

The Analytical Chemistry of the Noble Metals

Author : F. E. Beamish
Publisher : Elsevier
ISBN 13 : 1483225976
Total Pages : 624 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis The Analytical Chemistry of the Noble Metals by : F. E. Beamish

Download or read book The Analytical Chemistry of the Noble Metals written by F. E. Beamish and published by Elsevier. This book was released on 2013-10-22 with total page 624 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Chemistry, Volume 24: The Analytical Chemistry of the Noble Metals describes the procedures for the separation, extraction, and analysis of noble metals. This book is composed of seven chapters, and begins with a survey on the influence of metallurgical factors on the susceptibility of platinum and gold metals to various corrosive agents. The succeeding chapter provides the methods of isolation of osmium and ruthenium from associated platinum metals and from base metals. A chapter examines the application of gravimetric methods for the separation of seven noble metals, including ruthenium, osmium, rhodium, iridium, palladium, platinum, and gold. Other chapters consider the procedures for volumetric, spectrophotometric, and spectrochemical analysis of noble metals. The concluding chapter describes the features and attributes of the equipment for noble metal analysis. This book is of value to analytical chemists and workers and researchers in metallurgy.

Atomic-Absorption Spectrophotometry

Author : W. T. Elwell
Publisher : Elsevier
ISBN 13 : 1483160130
Total Pages : 155 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Atomic-Absorption Spectrophotometry by : W. T. Elwell

Download or read book Atomic-Absorption Spectrophotometry written by W. T. Elwell and published by Elsevier. This book was released on 2013-10-22 with total page 155 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Chemistry, Second Edition, Volume 6: Atomic-Absorption Spectrophotometry focuses on the use of atomic absorption spectrophotometry as an analytical technique. This book discusses the developments in the analytical fields of atomic-absorption spectrophotometry. Organized into seven chapters, this edition starts with an overview of the fundamental principles underlying atomic-absorption spectra. This book then describes the use of high-temperature fuel-rich flames that allow the determination of some elements that were not previously capable of being determined by atomic-absorption spectrophotometry. Other chapters explore the advantages of improved instrumentation and consider the atomic-absorption procedures that have been applied to a wide variety of samples from agricultural and biological materials. This book discusses as well the determination of specified elements by a direct examination of the sample solution. The final chapter provides a list of instruments that are commercially available, with emphasis on their characteristics. This book is a valuable resource for analysts, physicists, and chemists.

Microanalysis by the Ring-Oven Technique

Author : Herbert Weisz
Publisher : Elsevier
ISBN 13 : 1483153304
Total Pages : 183 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Microanalysis by the Ring-Oven Technique by : Herbert Weisz

Download or read book Microanalysis by the Ring-Oven Technique written by Herbert Weisz and published by Elsevier. This book was released on 2013-10-22 with total page 183 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series of Monographs in Analytical Chemistry, Volume 37: Microanalysis by the Ring-Oven Technique, Second Edition focuses on the ring-oven method. The book first offers information on the characteristics and uses of ring-oven, gas generator, pipette, glass holder, and other accessories. The text focuses on qualitative analysis, including the systematic schemes for the analysis of metal ions; separations and reactions for acid radicals; and reactions for metal ions. The selection discusses spot colorimetry with the ring-oven method. Concerns include determination of iron and other metals, amplification reactions, removal of interfering ions, and determination of anions. The radiochemical applications of ring-oven method, including determination of inactive substances, identification of radionucleides, and separation procedures, are explained. The text also discusses the combination of ring-oven method with electrography, thin-layer chromatography, and solvent extraction. The book is a valuable source of information for readers interested in the ring-oven method.

Inorganic Ultramicroanalysis

Author : I. P. Alimarin
Publisher : Elsevier
ISBN 13 : 1483150488
Total Pages : 168 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Inorganic Ultramicroanalysis by : I. P. Alimarin

Download or read book Inorganic Ultramicroanalysis written by I. P. Alimarin and published by Elsevier. This book was released on 2013-10-22 with total page 168 pages. Available in PDF, EPUB and Kindle. Book excerpt: Inorganic Ultramicroanalysis focuses on the techniques and experimental methods used in ultramicroanalysis of inorganic compounds. Topics covered include the general apparatus used in the ultramicromethod of chemical analysis, qualitative and quantitative analysis, and methods of separation. This book consists of six chapters and opens with a review of the special features of the ultramicromethod of chemical analysis, paying particular attention to the use of the law of errors to calculate the limiting quantity of a substance necessary for the performance of chemical operations. The surface area of unit volume in the macro- and ultramicromethods of analysis is also compared. The next chapter deals with the general apparatus used in ultramicroanalysis, including the microscope and micromanipulators, and describes techniques of working with small volumes. The reader is then introduced to qualitative and quantitative analysis and methods of separation such as precipitation and electrolysis. The last chapter discusses future prospects for inorganic ultramicroanalysis. This monograph is written primarily for inorganic and analytical chemists.

Analytical Chemistry of Niobium and Tantalum

Author : Ross W. Moshier
Publisher : Elsevier
ISBN 13 : 1483185192
Total Pages : 285 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Analytical Chemistry of Niobium and Tantalum by : Ross W. Moshier

Download or read book Analytical Chemistry of Niobium and Tantalum written by Ross W. Moshier and published by Elsevier. This book was released on 2013-10-22 with total page 285 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Chemistry of Niobium and Tantalum details the methods in understanding the chemistry of niobium and tantalum, which includes separation, identification, and quantification. The text first discusses the general topics about niobium and tantalum, such as history, metallurgical properties, and applications. Next, the selection covers the properties of niobium and tantalum and their compounds. The subsequent chapters tackle the various analytical chemistry processes that can be applied to niobium and tantalum, such as spectrographic determination; titrimetric methods; and colorimetric determinations. The book will be of great use to chemists, chemical engineers, and metallurgists.

The Destruction of Organic Matter

Author : T. T. Gorsuch
Publisher : Elsevier
ISBN 13 : 1483160882
Total Pages : 161 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis The Destruction of Organic Matter by : T. T. Gorsuch

Download or read book The Destruction of Organic Matter written by T. T. Gorsuch and published by Elsevier. This book was released on 2013-10-22 with total page 161 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series of Monographs in Analytical Chemistry, Volume 39: The Destruction of Organic Matter focuses on the identification of trace elements in organic compounds. The monograph first offers information on the processes involved in the determination of trace elements in organic matters, as well as the methods not involving complete destruction of these elements. The text surveys the sources of errors in the processes responsible in pinpointing elements in organic compounds. These processes include sampling, disruption of the samples, manipulation, and measurements. The book examines the processes of wet and dry oxidation, including their applications to sulfuric, nitric, and perchloric acids and hydrogen peroxide. The methods of dry ashing and oxidation with excited oxygen and oxidative fusion are elaborated. The text also underscores the varying methods in removing trace elements in organic compounds. The elements include zinc, copper, silver, gold, lead, germanium, titanium, arsenic, bismuth, and vanadium. The book also describes wet digestion methods and dry ashing procedures in the removal of trace elements in organic matters. The monograph is a vital source of information for readers interested in the identification of trace elements in organic compounds.

Analytical Chemistry of Zirconium and Hafnium

Author : Anil K. Mukherji
Publisher : Elsevier
ISBN 13 : 1483184307
Total Pages : 296 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Analytical Chemistry of Zirconium and Hafnium by : Anil K. Mukherji

Download or read book Analytical Chemistry of Zirconium and Hafnium written by Anil K. Mukherji and published by Elsevier. This book was released on 2013-10-22 with total page 296 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Chemistry of Zirconium and Hafnium compiles literature on the characterization and analysis of zirconium and hafnium. Various methods in studying the properties of the featured elements are presented in this book. This book also discusses the aqueous solutions of zirconium and hafnium. It then explains the methods such as dissolution of ores and alloys, detection and identification, and gravimetric determinations. This text further examines the titrimetric, electrometric, and absorptiometric methods, as well as methods of separations using ion-exchange and using solvent extraction, along with separation of hafnium from zirconium. The latter part of this text presents methods such as spectrographic analyses, X-ray analyses, and neutron activation analysis and separation of tracers. This book will come in handy for chemists and chemistry students, as well as for others interested in studying zirconium and hafnium.