Problems In Organic Structure Determination

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Problems in Organic Structure Determination

Author : Roger G. Linington
Publisher : CRC Press
ISBN 13 : 1498719635
Total Pages : 755 pages
Book Rating : 4.4/5 (987 download)

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Book Synopsis Problems in Organic Structure Determination by : Roger G. Linington

Download or read book Problems in Organic Structure Determination written by Roger G. Linington and published by CRC Press. This book was released on 2015-10-14 with total page 755 pages. Available in PDF, EPUB and Kindle. Book excerpt: At a point where most introductory organic chemistry texts end, this problems-based workbook picks up the thread to lead students through a graduated set of 120 problems. With extensive detailed spectral data, it contains a variety of problems designed by renowned authors to develop proficiency in organic structure determination. This workbook leads you from basic problems encountered in introductory organic chemistry textbooks to highly complex natural product-based problems. It presents a concept-based learning platform, introducing key concepts sequentially and reinforcing them with problems that exemplify the complexities and underlying principles that govern each concept. The book is organized in such a way that allows you to work through the problems in order or in selections according to your experience and desired area of mastery. It also provides access to raw data files online that can be downloaded and used for data manipulation using freeware or commercial software. With its problem-centered approach, integrated use of online and digital resources, and appendices that include notes and hints, Problems in Organic Structure Determination: A Practical Approach to NMR Spectroscopy is an outstanding resource for training students and professionals in structure determination.

Organic Structure Determination Using 2-D NMR Spectroscopy

Author : Jeffrey H. Simpson
Publisher : Academic Press
ISBN 13 : 0123849705
Total Pages : 591 pages
Book Rating : 4.1/5 (238 download)

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Book Synopsis Organic Structure Determination Using 2-D NMR Spectroscopy by : Jeffrey H. Simpson

Download or read book Organic Structure Determination Using 2-D NMR Spectroscopy written by Jeffrey H. Simpson and published by Academic Press. This book was released on 2011-12-30 with total page 591 pages. Available in PDF, EPUB and Kindle. Book excerpt: "The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner in which the material contained in this book is presented both reflects and validates this belief"--

Problems in Spectroscopy

Author : Barry M. Trost
Publisher :
ISBN 13 :
Total Pages : 42 pages
Book Rating : 4.4/5 (91 download)

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Book Synopsis Problems in Spectroscopy by : Barry M. Trost

Download or read book Problems in Spectroscopy written by Barry M. Trost and published by . This book was released on 1967 with total page 42 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Organic Structure Determination Using 2-D NMR Spectroscopy

Author : Jeffrey H. Simpson
Publisher : Academic Press
ISBN 13 : 0123849713
Total Pages : 540 pages
Book Rating : 4.1/5 (238 download)

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Book Synopsis Organic Structure Determination Using 2-D NMR Spectroscopy by : Jeffrey H. Simpson

Download or read book Organic Structure Determination Using 2-D NMR Spectroscopy written by Jeffrey H. Simpson and published by Academic Press. This book was released on 2011-12-03 with total page 540 pages. Available in PDF, EPUB and Kindle. Book excerpt: Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, is a primary text for a course in two-dimensional (2-D) nuclear magnetic resonance (NMR) techniques, with the goal to learn to identify organic molecular structure. It presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra. The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed. The book contains 30 known and 30 unknown structure determination problems. It also features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing. This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty. Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra Contains 30 known and 30 unknown structure determination problems Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing

Challenges in Molecular Structure Determination

Author : Manfred Reichenbächer
Publisher : Springer Science & Business Media
ISBN 13 : 3642243894
Total Pages : 500 pages
Book Rating : 4.6/5 (422 download)

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Book Synopsis Challenges in Molecular Structure Determination by : Manfred Reichenbächer

Download or read book Challenges in Molecular Structure Determination written by Manfred Reichenbächer and published by Springer Science & Business Media. This book was released on 2012-03-23 with total page 500 pages. Available in PDF, EPUB and Kindle. Book excerpt: Taking a problem-based approach, the authors provide a practice-oriented and systematic introduction to both organic and inorganic structure determination by spectroscopic methods. This includes mass spectrometry, vibrational spectroscopies, UV/VIS spectroscopy and NMR as well as applying combinations of these methods. The authors show how to elucidate chemical structures with a minimal number of spectroscopic techniques. Readers can train their skills by more than 400 problems with varying degree of sophistication. Interactive Powerpoint-Charts are available as Extra Materials to support self-study.

Tables of Spectral Data for Structure Determination of Organic Compounds

Author : Ernö Pretsch
Publisher : Springer Science & Business Media
ISBN 13 : 3662224550
Total Pages : 325 pages
Book Rating : 4.6/5 (622 download)

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Book Synopsis Tables of Spectral Data for Structure Determination of Organic Compounds by : Ernö Pretsch

Download or read book Tables of Spectral Data for Structure Determination of Organic Compounds written by Ernö Pretsch and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 325 pages. Available in PDF, EPUB and Kindle. Book excerpt: Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.

Determination of Organic Structures by Physical Methods

Author : E. A. Braude
Publisher : Elsevier
ISBN 13 : 1483275728
Total Pages : 824 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis Determination of Organic Structures by Physical Methods by : E. A. Braude

Download or read book Determination of Organic Structures by Physical Methods written by E. A. Braude and published by Elsevier. This book was released on 2013-10-22 with total page 824 pages. Available in PDF, EPUB and Kindle. Book excerpt: Determination of Organic Structures by Physical Methods, Volume 1 focuses on the processes, methodologies, principles, and approaches involved in the determination of organic structures by physical methods, including infrared light absorption, thermodynamic properties, Raman spectra, and kinetics. The selection first elaborates on the phase properties of small molecules, equilibrium and dynamic properties of large molecules, and optical rotation. Discussions focus on simple acyclic compounds, carbohydrates, steroids, diffusion, viscosity, osmotic pressure, sedimentation velocity, melting and boiling points, and molar volume. The book then examines ultraviolet and visible light absorption, infrared light absorption, Raman spectra, and the theory of magnetic susceptibility. Concerns cover applications to the study of organic compounds, applications to the determination of structure, determination of thermodynamic properties, and experimental methods and evaluation of data. The text ponders on wave-mechanical theory, reaction kinetics, and dissociation constants, including dissociation of molecular addition compounds, principles of reaction kinetics, and valence-bond treatment of aromatic systems. The selection is a valuable source of data for researchers interested in the determination of organic structures by physical methods.

Organic Structures from Spectra

Author : L. D. Field
Publisher :
ISBN 13 :
Total Pages : 304 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Organic Structures from Spectra by : L. D. Field

Download or read book Organic Structures from Spectra written by L. D. Field and published by . This book was released on 1995-12-26 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: Offers a realistic approach to solving problems used by organic chemists. Covering all the major spectroscopic techniques, it provides a graded set of problems that develop and consolidate students' understanding of organic spectroscopy. This edition contains more elementary problems and a modern approach to NMR spectra.

Organic Structures from Spectra

Author : L. D. Field
Publisher : John Wiley & Sons
ISBN 13 : 1118325451
Total Pages : 512 pages
Book Rating : 4.1/5 (183 download)

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Book Synopsis Organic Structures from Spectra by : L. D. Field

Download or read book Organic Structures from Spectra written by L. D. Field and published by John Wiley & Sons. This book was released on 2013-02-18 with total page 512 pages. Available in PDF, EPUB and Kindle. Book excerpt: The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra. Organic Structures from Spectra, Fifth Edition is a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 27 problems using 2D-NMR spectroscopy, more than 20 problems specifically dealing with the interpretation of spin-spin coupling in proton NMR spectra and 8 problems based on the quantitative analysis of mixtures using proton and carbon NMR spectroscopy. All of the problems are graded to develop and consolidate the student’s understanding of organic spectroscopy. The accompanying text is descriptive and only explains the underlying theory at a level which is sufficient to tackle the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups. The examples themselves have been selected to include all important common structural features found in organic compounds and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems, to build confidence and demonstrate basic principles, than in other collections. The fifth edition of this popular textbook: • includes more than 250 new spectra and more than 25 completely new problems; • now incorporates an expanded suite of new problems dealing with the analysis of 2D NMR spectra (COSY, C H Correlation spectroscopy, HMBC, NOESY and TOCSY); • has been expanded and updated to reflect the new developments in NMR and to retire older techniques that are no longer in common use; • provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy; • features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra include DEPT experiments as well as proton-coupled experiments; • contains 6 problems in the style of the experimental section of a research paper and two examples of fully worked solutions. Organic Structures from Spectra, Fifth Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry. Contents Preface Introduction Ultraviolet Spectroscopy Infrared Spectroscopy Mass Spectrometry Nuclear Magnetic Resonance Spectroscopy 2DNMR Problems Index Reviews from earlier editions “Your book is becoming one of the “go to” books for teaching structure determination here in the States. Great work!” “…I would definitely state that this book is the most useful aid to basic organic spectroscopy teaching in existence and I would strongly recommend every instructor in this area to use it either as a source of examples or as a class textbook”. Magnetic Resonance in Chemistry “Over the past year I have trained many students using problems in your book - they initially find it as a task. But after doing 3-4 problems with all their brains activities... working out the rest of the problems become a mania. They get addicted to the problem solving and every time they solve a problem by themselves, their confident level also increases.” “I am teaching the fundamentals of Molecular Spectroscopy and your books represent excellent sources of spectroscopic problems for students.”

Organic Structure Analysis

Author : Phillip Crews
Publisher : Oxford University Press, USA
ISBN 13 :
Total Pages : 664 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Organic Structure Analysis by : Phillip Crews

Download or read book Organic Structure Analysis written by Phillip Crews and published by Oxford University Press, USA. This book was released on 2010 with total page 664 pages. Available in PDF, EPUB and Kindle. Book excerpt: The most up-to-date integrated spectroscopy text available, Organic Structure Analysis, Second Edition, is the only text that teaches students how to solve structures as they are solved in actual practice. Ideal for advanced undergraduate and graduate courses in organic structure analysis, organic structure identification, and organic spectroscopy, it emphasizes real applications--integrating theory as needed--and introduces students to the latest spectroscopic methods. FEATURES * Focus on Structure: Opens with structural elements and then considers the characteristics, advantages, and disadvantages of spectroscopic methods. Includes coverage of the steps used in determining a molecular structure, the limitations to organic structure determination by spectroscopic methods, and an "Organic Structure Analyses Gone Bad" table (all unique to this text) * Practical Organization: Presents the most commonly used methods first, beginning with an overview of strategies, followed by the use of NMR, and then moving on to mass spectrometry, infrared, and ultraviolet * Innovative Real-World Problem-Solving Approach: Follows the actual information flow used by chemists to solve molecular structures, as opposed to the standard methods-based approach of other texts * Unique Chapter (12) Featuring 51 Structure-Solving Problems: Each problem emphasizes a different method; the problems increase in difficulty throughout the chapter, successively building on students' knowledge and requiring them to integrate multiple methods to identify molecules. NEW TO THE SECOND EDITION * Coverage of the Latest Instrumental and Computational Advances: Examines the use of modern instruments, data processing, and computer-assisted structure elucidation techniques * Updated and Expanded Treatment of NMR (Chapters 2-5): An extensively revised Chapter 5 discusses multi-pulse 1D and 2D NMR methods, 1D TOCSY and 1D NOESY sequences, and using NOESY and ROESY in determining relative stereochemistry and solution conformation. * Additional Coverage of Mass Spectrometry: A new chapter (7) expands the discussion of mass spectrometry to three chapters (6-8). Topics include cutting-edge MS instrumentation and new information on tandem MS techniques, combining NMR with MS, large-molecule MS, chemo-informatics, and more. * More Exercises and Improved Spectra: The second edition includes 25% more problems than the previous edition (279 total). In addition, many of the spectra, including all of those presented in Chapters 11 and 12, have been reprocessed or reacquired for greater clarity.

Structure Elucidation by NMR in Organic Chemistry

Author : Eberhard Breitmaier
Publisher : John Wiley & Sons
ISBN 13 : 0470850078
Total Pages : 279 pages
Book Rating : 4.4/5 (78 download)

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Book Synopsis Structure Elucidation by NMR in Organic Chemistry by : Eberhard Breitmaier

Download or read book Structure Elucidation by NMR in Organic Chemistry written by Eberhard Breitmaier and published by John Wiley & Sons. This book was released on 2002-11-22 with total page 279 pages. Available in PDF, EPUB and Kindle. Book excerpt: This text provides the graduate student with a systematic guide to unravelling structural information from the NMR spectra of unknown synthetic and natural compounds. A brief introduction gives an overview of the basic principles and elementary instrumental methods of NMR. This is followed by instructional strategy and tactical advice on how to translate spectra into meaningful structural information. The book provides the student with 55 sets of spectra of graduated complexity. These are designed to challenge the student's problem-solving abilities by the introduction of new concepts with each group of problems, followed by possible solutions and full explanations. A formula index of solutions is provided at the end of the text. This third edition, following on from the second (a reprint of the first edition with corrections), presents significant new material. Thus, actual methods of two-dimensional NMR such as some inverse techniques of heteronuclear shift correlation, as well as the detection of proton-proton connectivities and nuclear Overhauser effects are included. To demonstrate the applications of these methods, new problems have replaced those of previous editions.

Determination Of Organic Structures By Physical Methods

Author : F.C. Nachod
Publisher : Elsevier
ISBN 13 : 0323149200
Total Pages : 468 pages
Book Rating : 4.3/5 (231 download)

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Book Synopsis Determination Of Organic Structures By Physical Methods by : F.C. Nachod

Download or read book Determination Of Organic Structures By Physical Methods written by F.C. Nachod and published by Elsevier. This book was released on 2012-12-02 with total page 468 pages. Available in PDF, EPUB and Kindle. Book excerpt: Determination of Organic Structures by Physical Methods, Volume 6 is a six-chapter text that describes the refinements of some established physical methods for organic structure determination. The opening chapters examine the application of mass spectroscopy to amino acid sequencing of oligopeptides and the computerized organic structure retrieval. The following chapters discuss the historical developments, principles, instrumentation, and application of flash photolysis and 29Si nuclear magnetic resonance to structure determination. A chapter considers the relevant theory from which information on internuclear distances can be obtained and the steady-state measurements, transient methods, as well as the use of Fourier transform technique. This chapter also explores the application of nuclear overhauser effect measurements to structural and stereochemical problems. The concluding chapter deals with the liquid crystal structure determination using NMR spectroscopy. This work will be of value to organic and analytical chemists and researchers.

Organic Structures from 2D NMR Spectra

Author : L. D. Field
Publisher : John Wiley & Sons
ISBN 13 : 1118868943
Total Pages : 328 pages
Book Rating : 4.1/5 (188 download)

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Book Synopsis Organic Structures from 2D NMR Spectra by : L. D. Field

Download or read book Organic Structures from 2D NMR Spectra written by L. D. Field and published by John Wiley & Sons. This book was released on 2015-06-15 with total page 328 pages. Available in PDF, EPUB and Kindle. Book excerpt: The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two-dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes automatically) acquired during the identification and characterisation of organic compounds. Organic Structures from 2D NMR Spectra is a carefully chosen set of more than 60 structural problems employing 2D-NMR spectroscopy. The problems are graded to develop and consolidate a student’s understanding of 2D NMR spectroscopy. There are many easy problems at the beginning of the collection, to build confidence and demonstrate the basic principles from which structural information can be extracted using 2D NMR. The accompanying text is very descriptive and focussed on explaining the underlying theory at the most appropriate level to sufficiently tackle the problems. Organic Structures from 2D NMR Spectra Is a graded series of about 60 problems in 2D NMR spectroscopy that assumes a basic knowledge of organic chemistry and a basic knowledge of one-dimensional NMR spectroscopy Incorporates the basic theory behind 2D NMR and those common 2D NMR experiments that have proved most useful in solving structural problems in organic chemistry Focuses on the most common 2D NMR techniques – including COSY, NOESY, HMBC, TOCSY, CH-Correlation and multiplicity-edited C-H Correlation. Incorporates several examples containing the heteronuclei 31P, 15N and 19F Organic Structures from 2D NMR Spectra is a logical follow-on from the highly successful “Organic Structures from Spectra” which is now in its fifth edition. The book will be invaluable for students of Chemistry, Pharmacy, Biochemistry and those taking courses in Organic Chemistry. Also available: Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra

Problems in Organic Structure Determination

Author : Addison Ault
Publisher :
ISBN 13 :
Total Pages : 204 pages
Book Rating : 4.:/5 (38 download)

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Book Synopsis Problems in Organic Structure Determination by : Addison Ault

Download or read book Problems in Organic Structure Determination written by Addison Ault and published by . This book was released on 1967 with total page 204 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Organic Structure Determination

Author : Daniel J. Pasto
Publisher : Prentice Hall
ISBN 13 : 9780136408543
Total Pages : 536 pages
Book Rating : 4.4/5 (85 download)

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Book Synopsis Organic Structure Determination by : Daniel J. Pasto

Download or read book Organic Structure Determination written by Daniel J. Pasto and published by Prentice Hall. This book was released on 1969 with total page 536 pages. Available in PDF, EPUB and Kindle. Book excerpt: Part 1 : Physical methods of separation, purification, and characterization -- Separation and purification -- Physical characterization -- Part 2 : Adsorption spectroscopy -- Ultraviolet spectroscopy -- Infrared spectroscopy -- Nuclear magnetic resonance -- Electron paramagnetic resonance -- Determination of absolute stereochemistry -- Mass spectrometry -- Part 3 : Identification of organic compounds -- Characterization of an unknown compound -- Classification by solubility and acid-base properties -- Qualitative and quantitative elemental analyses -- Functional group classification and characterization -- Searching the literature -- Problems.

Determination of Organic Structures by Physical Methods

Author : F.C. Nachod
Publisher : Elsevier
ISBN 13 : 0323152848
Total Pages : 384 pages
Book Rating : 4.3/5 (231 download)

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Book Synopsis Determination of Organic Structures by Physical Methods by : F.C. Nachod

Download or read book Determination of Organic Structures by Physical Methods written by F.C. Nachod and published by Elsevier. This book was released on 2012-12-02 with total page 384 pages. Available in PDF, EPUB and Kindle. Book excerpt: Determination of Organic Structures by Physical Methods, Volume 5 is a seven-chapter text that discusses the improvements of some established physical methods for organic structure determination. Each chapter of this book examines specific physical method, including electron diffraction, spin saturation labeling, chemically and electro-magnetically induced dynamic nuclear polarization, ion cyclotron resonance spectroscopy, nuclear quadrupole resonance, Mössbauer spectroscopy, and automated analysis systems. The historical developments, principles, instrumentation, and applications to organic chemistry of these methods are discussed. This work will be of value to organic and analytical chemists and researchers.

Solving Problems with NMR Spectroscopy

Author : Atta-ur Rahman
Publisher : Academic Press
ISBN 13 : 0124116132
Total Pages : 535 pages
Book Rating : 4.1/5 (241 download)

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Book Synopsis Solving Problems with NMR Spectroscopy by : Atta-ur Rahman

Download or read book Solving Problems with NMR Spectroscopy written by Atta-ur Rahman and published by Academic Press. This book was released on 2015-08-18 with total page 535 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solving Problems with NMR Spectroscopy, Second Edition, is a fully updated and revised version of the best-selling book. This new edition still clearly presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving many new, clear examples for readers to understand and try, with new solutions provided in the text. It also explains new developments and concepts in NMR spectroscopy, including sensitivity problems (hardware and software solutions) and an extension of the multidimensional coverage to 3D NMR. The book also includes a series of applications showing how NMR is used in real life to solve advanced problems beyond simple small-molecule chemical analysis. This new text enables organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems provided by the authors help readers understand the discussion more clearly and the solution and interpretation of spectra help readers become proficient in the application of important, modern 1D, 2D, and 3D NMR techniques to structural studies. Explains and presents the most important NMR techniques used for structural determinations Offers a unique problem-solving approach for readers to understand how to solve structure problems Uses questions and problems, including discussions of their solutions and interpretations, to help readers understand the fundamentals and applications of NMR Avoids use of extensive mathematical formulas and clearly explains how to implement NMR structure analysis Foreword by Nobel Prize winner Richard R. Ernst New to This Edition Key developments in the field of NMR spectroscopy since the First Edition in 1996 New chapter on sensitivity enhancement, a key driver of development in NMR spectroscopy New concepts such as Pulse Field Gradients, shaped pulses, and DOSY (Diffusion Order Spectroscopy) in relevant chapters More emphasis on practical aspects of NMR spectroscopy, such as the use of Shigemi tubes and various types of cryogenic probes Over 100 new problems and questions addressing the key concepts in NMR spectroscopy Improved figures and diagrams More than 180 example problems to solve, with detailed solutions provided at the end of each chapter