Organic Structure Analysis

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Organic Structure Analysis

Author : Phillip Crews
Publisher : Oxford University Press, USA
ISBN 13 :
Total Pages : 664 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Organic Structure Analysis by : Phillip Crews

Download or read book Organic Structure Analysis written by Phillip Crews and published by Oxford University Press, USA. This book was released on 2010 with total page 664 pages. Available in PDF, EPUB and Kindle. Book excerpt: The most up-to-date integrated spectroscopy text available, Organic Structure Analysis, Second Edition, is the only text that teaches students how to solve structures as they are solved in actual practice. Ideal for advanced undergraduate and graduate courses in organic structure analysis, organic structure identification, and organic spectroscopy, it emphasizes real applications--integrating theory as needed--and introduces students to the latest spectroscopic methods. FEATURES * Focus on Structure: Opens with structural elements and then considers the characteristics, advantages, and disadvantages of spectroscopic methods. Includes coverage of the steps used in determining a molecular structure, the limitations to organic structure determination by spectroscopic methods, and an "Organic Structure Analyses Gone Bad" table (all unique to this text) * Practical Organization: Presents the most commonly used methods first, beginning with an overview of strategies, followed by the use of NMR, and then moving on to mass spectrometry, infrared, and ultraviolet * Innovative Real-World Problem-Solving Approach: Follows the actual information flow used by chemists to solve molecular structures, as opposed to the standard methods-based approach of other texts * Unique Chapter (12) Featuring 51 Structure-Solving Problems: Each problem emphasizes a different method; the problems increase in difficulty throughout the chapter, successively building on students' knowledge and requiring them to integrate multiple methods to identify molecules. NEW TO THE SECOND EDITION * Coverage of the Latest Instrumental and Computational Advances: Examines the use of modern instruments, data processing, and computer-assisted structure elucidation techniques * Updated and Expanded Treatment of NMR (Chapters 2-5): An extensively revised Chapter 5 discusses multi-pulse 1D and 2D NMR methods, 1D TOCSY and 1D NOESY sequences, and using NOESY and ROESY in determining relative stereochemistry and solution conformation. * Additional Coverage of Mass Spectrometry: A new chapter (7) expands the discussion of mass spectrometry to three chapters (6-8). Topics include cutting-edge MS instrumentation and new information on tandem MS techniques, combining NMR with MS, large-molecule MS, chemo-informatics, and more. * More Exercises and Improved Spectra: The second edition includes 25% more problems than the previous edition (279 total). In addition, many of the spectra, including all of those presented in Chapters 11 and 12, have been reprocessed or reacquired for greater clarity.

Organic Structure Analysis

Author : Phillip Crews
Publisher : OUP USA
ISBN 13 : 9780199733224
Total Pages : 576 pages
Book Rating : 4.7/5 (332 download)

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Book Synopsis Organic Structure Analysis by : Phillip Crews

Download or read book Organic Structure Analysis written by Phillip Crews and published by OUP USA. This book was released on 2010-10-28 with total page 576 pages. Available in PDF, EPUB and Kindle. Book excerpt: Organic Spectroscopy is a standard chemistry course offered each year to large numbers of seniors and beginning graduate students. They learn to efficiently solve problems of molecular structure determination by an integrated use of four primary spectroscopic methods; NMR; mass spectrometry; infrared and ultraviolet. The problem solving approach used in the second edition follows the actual information flow used by practitioners solving molecular strustures and not the standard methods-based aooroach used in other texts. In the ten years since the last edition published there have been significant changes in spectroscopic instrumentation and these are reflected throughout this text. New sections have been included where the first edition omitted coverage, and all chapters are updated with the most recent developments in the field. Major changes have been made in the pivotal chapters covering multipulse 1D and 2D nuclear magnetic resonance methods and the chapters covering mass spectrometric methods have been split from two into three to increase content on modern MS methodology. As examples in NMR, selective pulses and their uses, 15N 2D methods and computer assisted structure elucidation has been included and there is now a section on NOESY and ROESY. For MS the three chapters cover: core techniques and ionization processes; small and large molecule analysis and fragmentation processes. A hallmark of this text is the focus on chemical structure and the text revolves around how relevant information regarding skeleton, functional groups and stereochemistry can be derived and the benefits/disadvantages of particular approaches. The straightforward writing style and use of illustrative examples, clearly reproduced spectra and a large number of problems make this text more accessible than ever.

Organic Structure Analysis

Author : Phillip Crews
Publisher : Oxford University Press, USA
ISBN 13 : 9780195101027
Total Pages : 552 pages
Book Rating : 4.1/5 (1 download)

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Book Synopsis Organic Structure Analysis by : Phillip Crews

Download or read book Organic Structure Analysis written by Phillip Crews and published by Oxford University Press, USA. This book was released on 1998 with total page 552 pages. Available in PDF, EPUB and Kindle. Book excerpt: The text's major aim is to show how spectra can be efficiently examined in order to identify a molecule's major structural elements.

Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods

Author : J.T. Clerc
Publisher : Elsevier
ISBN 13 : 0444597549
Total Pages : 288 pages
Book Rating : 4.4/5 (445 download)

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Book Synopsis Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods by : J.T. Clerc

Download or read book Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods written by J.T. Clerc and published by Elsevier. This book was released on 2012-12-02 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Structural Analysis of Organic Compounds covers some practical analytical aspects of organic structural analysis by combined application of spectroscopic methods. This book is composed of three parts encompassing 35 chapters that specifically describe infrared-, ultraviolet-, proton and carbon-13 nuclear magnetic resonance and mass spectroscopy. Considerable chapters discuss the problems intended to cover a wide variety of chemical structure and spectroscopic argument, thereby exemplifying interpretations and comment on specific practical aspects of the problem solving procedure. The remaining chapters provide short supplementing research concerning various aspects of structural analysis. This book will prove useful to organic and analytical chemists.

Structure Elucidation in Organic Chemistry

Author : Maria-Magdalena Cid
Publisher : John Wiley & Sons
ISBN 13 : 3527664637
Total Pages : 552 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Structure Elucidation in Organic Chemistry by : Maria-Magdalena Cid

Download or read book Structure Elucidation in Organic Chemistry written by Maria-Magdalena Cid and published by John Wiley & Sons. This book was released on 2015-01-05 with total page 552 pages. Available in PDF, EPUB and Kindle. Book excerpt: Intended for advanced readers, this is a review of all relevant techniques for structure analysis in one handy volume. As such, it provides the latest knowledge on spectroscopic and related techniques for chemical structure analysis, such as NMR, optical spectroscopy, mass spectrometry and X-ray crystallography, including the scope and limitation of each method. As a result, readers not only become acquainted with the techniques, but also the advantages of the synergy between them. This enables them to choose the correct analytical method for each problem, saving both time and resources. Special emphasis is placed on NMR and its application to absolute configuration determination and the analysis of molecular interactions. Adopting a practical point of view, the author team from academia and industry guarantees both solid methodology and applications essential for structure determination, equipping experts as well as newcomers with the tools to solve any structural problem.

Tables of Spectral Data for Structure Determination of Organic Compounds

Author : Ernö Pretsch
Publisher : Springer Science & Business Media
ISBN 13 : 3662224550
Total Pages : 325 pages
Book Rating : 4.6/5 (622 download)

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Book Synopsis Tables of Spectral Data for Structure Determination of Organic Compounds by : Ernö Pretsch

Download or read book Tables of Spectral Data for Structure Determination of Organic Compounds written by Ernö Pretsch and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 325 pages. Available in PDF, EPUB and Kindle. Book excerpt: Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.

X-ray Analysis and the Structure of Organic Molecules

Author : Jack D. Dunitz
Publisher : Wiley-VCH
ISBN 13 :
Total Pages : 520 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis X-ray Analysis and the Structure of Organic Molecules by : Jack D. Dunitz

Download or read book X-ray Analysis and the Structure of Organic Molecules written by Jack D. Dunitz and published by Wiley-VCH. This book was released on 1995 with total page 520 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is the second corrected reprint of â2X-Ray Analysisâ2, published in 1979 and consists of two parts. Part one is about Crystal Structure Analysis, part two deals with Molecular Structure. All the information in this volume is of considerable value especially to those engaged in, or about to embark upon, X-ray crystal structure analysis.

Organic Structures from Spectra

Author : L. D. Field
Publisher :
ISBN 13 :
Total Pages : 304 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Organic Structures from Spectra by : L. D. Field

Download or read book Organic Structures from Spectra written by L. D. Field and published by . This book was released on 1995-12-26 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: Offers a realistic approach to solving problems used by organic chemists. Covering all the major spectroscopic techniques, it provides a graded set of problems that develop and consolidate students' understanding of organic spectroscopy. This edition contains more elementary problems and a modern approach to NMR spectra.

Structure Determination of Organic Compounds

Author : Ernö Pretsch
Publisher : Springer Science & Business Media
ISBN 13 : 9783540678151
Total Pages : 444 pages
Book Rating : 4.6/5 (781 download)

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Book Synopsis Structure Determination of Organic Compounds by : Ernö Pretsch

Download or read book Structure Determination of Organic Compounds written by Ernö Pretsch and published by Springer Science & Business Media. This book was released on 2000 with total page 444 pages. Available in PDF, EPUB and Kindle. Book excerpt: Table -- Combination tables -- 13C NMR spectroscopy -- 1H NMR specroscopy -- IR spectroscopy -- Mass spectrometry -- UV/Vis spectroscopy.

Organic Structures from Spectra

Author : L. D. Field
Publisher : John Wiley & Sons
ISBN 13 : 1118325451
Total Pages : 512 pages
Book Rating : 4.1/5 (183 download)

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Book Synopsis Organic Structures from Spectra by : L. D. Field

Download or read book Organic Structures from Spectra written by L. D. Field and published by John Wiley & Sons. This book was released on 2013-02-18 with total page 512 pages. Available in PDF, EPUB and Kindle. Book excerpt: The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra. Organic Structures from Spectra, Fifth Edition is a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 27 problems using 2D-NMR spectroscopy, more than 20 problems specifically dealing with the interpretation of spin-spin coupling in proton NMR spectra and 8 problems based on the quantitative analysis of mixtures using proton and carbon NMR spectroscopy. All of the problems are graded to develop and consolidate the student’s understanding of organic spectroscopy. The accompanying text is descriptive and only explains the underlying theory at a level which is sufficient to tackle the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups. The examples themselves have been selected to include all important common structural features found in organic compounds and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems, to build confidence and demonstrate basic principles, than in other collections. The fifth edition of this popular textbook: • includes more than 250 new spectra and more than 25 completely new problems; • now incorporates an expanded suite of new problems dealing with the analysis of 2D NMR spectra (COSY, C H Correlation spectroscopy, HMBC, NOESY and TOCSY); • has been expanded and updated to reflect the new developments in NMR and to retire older techniques that are no longer in common use; • provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy; • features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra include DEPT experiments as well as proton-coupled experiments; • contains 6 problems in the style of the experimental section of a research paper and two examples of fully worked solutions. Organic Structures from Spectra, Fifth Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry. Contents Preface Introduction Ultraviolet Spectroscopy Infrared Spectroscopy Mass Spectrometry Nuclear Magnetic Resonance Spectroscopy 2DNMR Problems Index Reviews from earlier editions “Your book is becoming one of the “go to” books for teaching structure determination here in the States. Great work!” “…I would definitely state that this book is the most useful aid to basic organic spectroscopy teaching in existence and I would strongly recommend every instructor in this area to use it either as a source of examples or as a class textbook”. Magnetic Resonance in Chemistry “Over the past year I have trained many students using problems in your book - they initially find it as a task. But after doing 3-4 problems with all their brains activities... working out the rest of the problems become a mania. They get addicted to the problem solving and every time they solve a problem by themselves, their confident level also increases.” “I am teaching the fundamentals of Molecular Spectroscopy and your books represent excellent sources of spectroscopic problems for students.”

Organic Structure Determination Using 2-D NMR Spectroscopy

Author : Jeffrey H. Simpson
Publisher : Academic Press
ISBN 13 : 0123849705
Total Pages : 591 pages
Book Rating : 4.1/5 (238 download)

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Book Synopsis Organic Structure Determination Using 2-D NMR Spectroscopy by : Jeffrey H. Simpson

Download or read book Organic Structure Determination Using 2-D NMR Spectroscopy written by Jeffrey H. Simpson and published by Academic Press. This book was released on 2011-12-30 with total page 591 pages. Available in PDF, EPUB and Kindle. Book excerpt: "The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner in which the material contained in this book is presented both reflects and validates this belief"--

Determination of Organic Structures by Physical Methods

Author : E. A. Braude
Publisher : Elsevier
ISBN 13 : 1483275728
Total Pages : 824 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis Determination of Organic Structures by Physical Methods by : E. A. Braude

Download or read book Determination of Organic Structures by Physical Methods written by E. A. Braude and published by Elsevier. This book was released on 2013-10-22 with total page 824 pages. Available in PDF, EPUB and Kindle. Book excerpt: Determination of Organic Structures by Physical Methods, Volume 1 focuses on the processes, methodologies, principles, and approaches involved in the determination of organic structures by physical methods, including infrared light absorption, thermodynamic properties, Raman spectra, and kinetics. The selection first elaborates on the phase properties of small molecules, equilibrium and dynamic properties of large molecules, and optical rotation. Discussions focus on simple acyclic compounds, carbohydrates, steroids, diffusion, viscosity, osmotic pressure, sedimentation velocity, melting and boiling points, and molar volume. The book then examines ultraviolet and visible light absorption, infrared light absorption, Raman spectra, and the theory of magnetic susceptibility. Concerns cover applications to the study of organic compounds, applications to the determination of structure, determination of thermodynamic properties, and experimental methods and evaluation of data. The text ponders on wave-mechanical theory, reaction kinetics, and dissociation constants, including dissociation of molecular addition compounds, principles of reaction kinetics, and valence-bond treatment of aromatic systems. The selection is a valuable source of data for researchers interested in the determination of organic structures by physical methods.

Fourier Technique in X-ray Organic Structure Analysis

Author : Andrew Donald Booth
Publisher : CUP Archive
ISBN 13 :
Total Pages : 134 pages
Book Rating : 4./5 ( download)

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Book Synopsis Fourier Technique in X-ray Organic Structure Analysis by : Andrew Donald Booth

Download or read book Fourier Technique in X-ray Organic Structure Analysis written by Andrew Donald Booth and published by CUP Archive. This book was released on 1948 with total page 134 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Problems and Problem Solving in Chemistry Education

Author : Georgios Tsaparlis
Publisher : Royal Society of Chemistry
ISBN 13 : 1839163593
Total Pages : 503 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Problems and Problem Solving in Chemistry Education by : Georgios Tsaparlis

Download or read book Problems and Problem Solving in Chemistry Education written by Georgios Tsaparlis and published by Royal Society of Chemistry. This book was released on 2021-05-17 with total page 503 pages. Available in PDF, EPUB and Kindle. Book excerpt: Problem solving is central to the teaching and learning of chemistry at secondary, tertiary and post-tertiary levels of education, opening to students and professional chemists alike a whole new world for analysing data, looking for patterns and making deductions. As an important higher-order thinking skill, problem solving also constitutes a major research field in science education. Relevant education research is an ongoing process, with recent developments occurring not only in the area of quantitative/computational problems, but also in qualitative problem solving. The following situations are considered, some general, others with a focus on specific areas of chemistry: quantitative problems, qualitative reasoning, metacognition and resource activation, deconstructing the problem-solving process, an overview of the working memory hypothesis, reasoning with the electron-pushing formalism, scaffolding organic synthesis skills, spectroscopy for structural characterization in organic chemistry, enzyme kinetics, problem solving in the academic chemistry laboratory, chemistry problem-solving in context, team-based/active learning, technology for molecular representations, IR spectra simulation, and computational quantum chemistry tools. The book concludes with methodological and epistemological issues in problem solving research and other perspectives in problem solving in chemistry. With a foreword by George Bodner.

Organic Spectroscopic Structure Determination

Author : Douglass F. Taber
Publisher : Oxford University Press, USA
ISBN 13 :
Total Pages : 276 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Organic Spectroscopic Structure Determination by : Douglass F. Taber

Download or read book Organic Spectroscopic Structure Determination written by Douglass F. Taber and published by Oxford University Press, USA. This book was released on 2007 with total page 276 pages. Available in PDF, EPUB and Kindle. Book excerpt: Organic Spectroscopic Structure Determination is designed as a first introduction to the elucidation of molecular structures. It consists of four sections that engage the imagination of the student. Taber has arranged the material in such a way that the students can work the problems and learn the procedures on their own, minimizing the time taken in lecture. The first section includes three chapters of instruction on the methods of organic spectroscopy. The second consists of fifty problems with just data sets of spectroscopic data. The third includes fifty problems that show starting materials and reaction conditions, with spectroscopic data for the product. The final section features tables of spectroscopic data.

Organic Spectroscopic Analysis

Author : Rosaleen J. Anderson
Publisher : Royal Society of Chemistry
ISBN 13 : 9780854044764
Total Pages : 190 pages
Book Rating : 4.0/5 (447 download)

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Book Synopsis Organic Spectroscopic Analysis by : Rosaleen J. Anderson

Download or read book Organic Spectroscopic Analysis written by Rosaleen J. Anderson and published by Royal Society of Chemistry. This book was released on 2004 with total page 190 pages. Available in PDF, EPUB and Kindle. Book excerpt: A unique textbook, aimed at undergraduate students, containing large numbers of spectra, problems and marginal notes, specifically chosen to highlight the points being discussed.

Organic Structures from 2D NMR Spectra

Author : L. D. Field
Publisher : John Wiley & Sons
ISBN 13 : 1118868943
Total Pages : 328 pages
Book Rating : 4.1/5 (188 download)

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Book Synopsis Organic Structures from 2D NMR Spectra by : L. D. Field

Download or read book Organic Structures from 2D NMR Spectra written by L. D. Field and published by John Wiley & Sons. This book was released on 2015-06-15 with total page 328 pages. Available in PDF, EPUB and Kindle. Book excerpt: The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two-dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes automatically) acquired during the identification and characterisation of organic compounds. Organic Structures from 2D NMR Spectra is a carefully chosen set of more than 60 structural problems employing 2D-NMR spectroscopy. The problems are graded to develop and consolidate a student’s understanding of 2D NMR spectroscopy. There are many easy problems at the beginning of the collection, to build confidence and demonstrate the basic principles from which structural information can be extracted using 2D NMR. The accompanying text is very descriptive and focussed on explaining the underlying theory at the most appropriate level to sufficiently tackle the problems. Organic Structures from 2D NMR Spectra Is a graded series of about 60 problems in 2D NMR spectroscopy that assumes a basic knowledge of organic chemistry and a basic knowledge of one-dimensional NMR spectroscopy Incorporates the basic theory behind 2D NMR and those common 2D NMR experiments that have proved most useful in solving structural problems in organic chemistry Focuses on the most common 2D NMR techniques – including COSY, NOESY, HMBC, TOCSY, CH-Correlation and multiplicity-edited C-H Correlation. Incorporates several examples containing the heteronuclei 31P, 15N and 19F Organic Structures from 2D NMR Spectra is a logical follow-on from the highly successful “Organic Structures from Spectra” which is now in its fifth edition. The book will be invaluable for students of Chemistry, Pharmacy, Biochemistry and those taking courses in Organic Chemistry. Also available: Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra