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Nanoindentation Of Soft Films On Hard Substrates
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Book Synopsis Nanoindentation of Soft Films on Hard Substrates by :
Download or read book Nanoindentation of Soft Films on Hard Substrates written by and published by . This book was released on 1996 with total page 6 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanoindentation is used for measuring mechanical properties of thin films. This paper addresses potential measurement errors caused by pile-up when soft films deposited on hard substrates are tested this way. Pile-up is exacerbated in soft film/hard substrate systems because of the constraint the substrate exerts on plastic deformation of the film. To examine pile-up effects, Al films 240 and 1700 nm thick were deposited on hard glass and tested by standard nanoindentation. In Al/glass, the film and substrate have similar elastic moduli; thus, any unusual behavior in nanoindentation results may be attributed to differences in plastic flow alone. SEM examination of nanoindentation hardness impressions in the film revealed that common methods for analyzing nanoindentation data underestimate the true contact areas by as much as 80%, which results in overestimations of the hardness and modulus by as much as 80 and 35%, respectively. Sources of these errors and their effect on measurement of hardness and elastic modulus are discussed, and a simple model for the composite hardness of the film/substrate system is developed. This model could prove useful when it is not possible to make indentations shallow enough to avoid substrate effects.
Book Synopsis Nanoindentation Hardness of Soft Films on Hard Substrates by :
Download or read book Nanoindentation Hardness of Soft Films on Hard Substrates written by and published by . This book was released on 1997 with total page 7 pages. Available in PDF, EPUB and Kindle. Book excerpt: The ability to accurately measure the mechanical properties of thin metallic films is important in the semiconductor industry as it relates to device reliability issues. One popular technique for measuring thin film mechanical properties is nanoindentation. This technique has the advantage of being able to measure properties such as hardness and elastic modulus without removing a film from its substrate. However, according to a widely-held rule of thumb, intrinsic film properties can be measured in a manner which is not influenced by the substrate only if the indentation depth is kept to less than 10% of the film thickness, which is often not practical. In this work, a method for making substrate independent hardness measurements of soft metallic films on hard substrates is proposed. The primary issue to be addressed is the substrate-induced enhancement of indentation pile-up and the ways in which this pile-up influences the contact area determined from analyses of nanoindentation load- displacement data. Based on experimental observations of soft aluminum films on silicon, glass, and sapphire substrates, a simple empirical relationship is derived which relates the amount of pile-up to the contact depth. From this relationship, a simple method is developed which allows the intrinsic hardness of the film to be measured by nanoindentation methods even when the indenter penetrates through the film into the substrate.
Book Synopsis Nanoindentation of Soft Films on Hard Substrates by :
Download or read book Nanoindentation of Soft Films on Hard Substrates written by and published by . This book was released on 1997 with total page 12 pages. Available in PDF, EPUB and Kindle. Book excerpt: Experiments and finite element simulations have been performed to examine error measurement of hardness and elastic modulus caused by pile-up when soft films deposited on hard substrates are tested by nanoindentation methods. Pile-up is exacerbated in soft-film/hard-substrate systems by the constraint imposed on plastic deformation in the film by the relatively non-deformable substrate. To experimentally examine pile-up effects, soft aluminum films with thicknesses of 240, 650, and 1700 nm were deposited on hard soda-lime glass substrates and tested by nanoindentation techniques. This system is attractive because the elastic modulus of the film and the substrate are approximately the same, but the substrate is harder than the film by a factor of about ten. Consequently, substrate influences on the indentation load-displacement behavior are manifested primarily by differences in the plastic flow characteristics alone. The elastic modulus of the film/substrate system, as measured by nanoindentation techniques, exhibits an increase with indenter penetration depth which peaks at a value approximately 30% greater than the true film modulus at a penetration depth close to the film thickness. Finite element simulation shows that this unusual behavior is caused by substrate-induced enhancement of pile-up. Finite element simulation also shows that the amount of pile-up increases with increasing penetration depth, and that the pile-up geometry depends on the work-hardening characteristics of the film. Because of these effects, nanoindentation techniques overestimate the true film hardness and elastic modulus by as much as 68% and 35%, respectively, depending on the work-hardening behavior of the film and the indenter penetration depth. The largest errors occur in non-work-hardening materials at penetration depths close to the film thickness, for which substrate-induced enhancement of pile-up is greatest.
Download or read book Old Glasgow written by and published by . This book was released on with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Applied Nanoindentation in Advanced Materials by : Atul Tiwari
Download or read book Applied Nanoindentation in Advanced Materials written by Atul Tiwari and published by John Wiley & Sons. This book was released on 2017-08-18 with total page 935 pages. Available in PDF, EPUB and Kindle. Book excerpt: Research in the area of nanoindentation has gained significant momentum in recent years, but there are very few books currently available which can educate researchers on the application aspects of this technique in various areas of materials science. Applied Nanoindentation in Advanced Materials addresses this need and is a comprehensive, self-contained reference covering applied aspects of nanoindentation in advanced materials. With contributions from leading researchers in the field, this book is divided into three parts. Part one covers innovations and analysis, and parts two and three examine the application and evaluation of soft and ceramic-like materials respectively. Key features: A one stop solution for scholars and researchers to learn applied aspects of nanoindentation Contains contributions from leading researchers in the field Includes the analysis of key properties that can be studied using the nanoindentation technique Covers recent innovations Includes worked examples Applied Nanoindentation in Advanced Materials is an ideal reference for researchers and practitioners working in the areas of nanotechnology and nanomechanics, and is also a useful source of information for graduate students in mechanical and materials engineering, and chemistry. This book also contains a wealth of information for scientists and engineers interested in mathematical modelling and simulations related to nanoindentation testing and analysis.
Book Synopsis Residual Stresses and Nanoindentation Testing of Films and Coatings by : Haidou Wang
Download or read book Residual Stresses and Nanoindentation Testing of Films and Coatings written by Haidou Wang and published by Springer. This book was released on 2018-03-12 with total page 215 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers the basic principles and application of nanoindentation technology to determine residual stresses in films and coatings. It briefly introduces various detection technologies for measuring residual stresses, while mainly focusing on nanoindentation. Subsequently, nanoindentation is used to determine residual stresses in different types of films and coatings, and to describe them in detail. This book is intended for specialists, engineers and graduate students in mechanical design, manufacturing, maintenance and remanufacturing, and as a guide to the practice of production with social and economic benefits.
Author :Anthony C. Fischer-Cripps Publisher :Springer Science & Business Media ISBN 13 :1475759436 Total Pages :283 pages Book Rating :4.4/5 (757 download)
Book Synopsis Nanoindentation by : Anthony C. Fischer-Cripps
Download or read book Nanoindentation written by Anthony C. Fischer-Cripps and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 283 pages. Available in PDF, EPUB and Kindle. Book excerpt: This new edition of Nanoindentation includes a dedicated chapter on thin films, new material on dynamic analysis and creep, accounts of recent research, and three new appendices on nonlinear least squares fitting, frequently asked questions, and specifications for a nanoindentation instrument. Nanoindentation Second Edition is intended for those who are entering the field for the first time and to act as a reference for those already conversant with the technique.
Author :Anthony C. Fischer-Cripps Publisher :Springer Science & Business Media ISBN 13 :0387224629 Total Pages :216 pages Book Rating :4.3/5 (872 download)
Book Synopsis Nanoindentation by : Anthony C. Fischer-Cripps
Download or read book Nanoindentation written by Anthony C. Fischer-Cripps and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 216 pages. Available in PDF, EPUB and Kindle. Book excerpt: Mechanical engineering, an engineering discipline borne of the needs of the industrial revolution, is once again asked to do its substantial share in the call for industrial renewal. The general call is urgent as we face profound issues of productivity and competitiveness that require engineering solutions, among others. The Mechanical Engineering Series features graduate texts and research monographs intended to address the need for information in contemporary areas of mechanical engineering. The series is conceived as a comprehensive one that covers a broad range of concentrations important to mechanical engineering graduate education and research. We are fortunate to have a distinguished roster of consulting editors on the advisory board, each an expert in one of the areas of concentration. The names of the consulting editors are listed on the facing page of this volume. The areas of concentration are: applied mechanics; biomechanics; computational mechanics; dynamic systems and control; energetics; mechanics of materials; processing; thermal science; and tribology.
Book Synopsis Nanoindentation of Brittle Solids by : Arjun Dey
Download or read book Nanoindentation of Brittle Solids written by Arjun Dey and published by CRC Press. This book was released on 2014-06-25 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Understanding the Basics of Nanoindentation and Why It Is Important Contact damage induced brittle fracture is a common problem in the field of brittle solids. In the case of both glass and ceramics—and as it relates to both natural and artificial bio-materials—it has triggered the need for improved fabrication technology and new product development in the industry. The Nanoindentation Technique Is Especially Dedicated to Brittle Materials Nanoindentation of Brittle Solids highlights the science and technology of nanoindentation related to brittle materials, and considers the applicability of the nanoindentation technique. This book provides a thorough understanding of basic contact induced deformation mechanisms, damage initiation, and growth mechanisms. Starting from the basics of contact mechanics and nanoindentation, it considers contact mechanics, addresses contact issues in brittle solids, and explores the concepts of hardness and elastic modulus of a material. It examines a variety of brittle solids and deciphers the physics of deformation and fracture at scale lengths compatible with the microstructural unit block. Discusses nanoindentation data analysis methods and various nanoindentation techniques Includes nanoindentation results from the authors’ recent research on natural biomaterials like tooth, bone, and fish scale materials Considers the nanoindentation response if contact is made too quickly in glass Explores energy issues related to the nanoindentation of glass Describes the nanoindentation response of a coarse grain alumina Examines nanoindentation on microplasma sprayed hydroxyapatite coatings Nanoindentation of Brittle Solids provides a brief history of indentation, and explores the science and technology of nanoindentation related to brittle materials. It also offers an in-depth discussion of indentation size effect; the evolution of shear induced deformation during indentation and scratches, and includes a collection of related research works.
Book Synopsis Mechanical Characterization of Thin Films Using Nanoindentation Techniques by : Angela Strojny
Download or read book Mechanical Characterization of Thin Films Using Nanoindentation Techniques written by Angela Strojny and published by . This book was released on 1999 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Fracture of Hard Thin Films Using Nanoindentation and Nanoscratch Techniques by :
Download or read book Fracture of Hard Thin Films Using Nanoindentation and Nanoscratch Techniques written by and published by . This book was released on 1998 with total page 6 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thin films are used in many applications where special properties are needed to insure performance and reliability. Of particular interest are thin tantalum nitride films. They are used extensively in microelectronic applications because of their long term stability and low thermal coefficient of resistance. They are sputter deposited which produces films with a high structural defect content and high compressive residual stresses both of which can alter the physical and mechanical properties of microelectronic thin films. Although these films are strong heat generators, they exhibit no changes in structure or composition of the interface with aluminum oxide substrates that degrade performance or reliability. However, the use of high power density components is driving a move to replace aluminum oxide with aluminum nitride for greater heat transfer. 6 This replacement substrate creates concern as residual stresses and long-term operation could induce detrimental changes along the thin film interface not observed in aluminum oxide devices. As a result, the authors employed nanoindentation and continuous nanoscratch testing to determine the effects of the intrinsic compressive residual stresses on the properties and fracture resistance of the thin tantalum nitride films. These techniques sample small volumes of material while preserving the production configuration of a free surface. Although nanoscratch tests lack a rigorous derivation of stress distributions and strain energy release rates, good approximations for strain energy release rates can be obtained using mechanics-based models for blister formation where residual stresses dominate interfacial fracture behavior. When combined with scanning and transmission electron microscopy, the results define structure-property relationships and resistance to fracture of these hard films.
Book Synopsis Effects of Adhesion on the Measurement of Thin Film Mechanical Properties by Nanoindentation by :
Download or read book Effects of Adhesion on the Measurement of Thin Film Mechanical Properties by Nanoindentation written by and published by . This book was released on 1997 with total page 7 pages. Available in PDF, EPUB and Kindle. Book excerpt: Experiments have been performed on soft aluminum films deposited on hard ceramic substrates to explore the influences of interfacial adhesion on mechanical property measurement by nanoindentation. The substrate materials included soda-lime silicate glass, aluminum oxynitride (ALON), and (100) sapphire. Thin films of high purity aluminum were sputtered onto each substrate to a thickness of 500 nm. Because the films were deposited simultaneously, the only major difference in the specimens was the nature of the substrate, which exerts an important influence on film adhesion through interfacial chemistry. Of the substrates examined, aluminum adheres strongly to glass and sapphire, but poorly to ALON. In addition, two different types of aluminum films on sapphire were examined - one with and the other without a 10 nm interlayer of amorphous carbon which significantly reduces film adhesion. Testing revealed important differences in the hardness of the specimens when measured by standard nanoindentation methods. Characterization of the residual hardness impressions by high resolution scanning electron microscopy showed that the hardness differences arise from an influence of interfacial debonding and film delamination on pile-up in the film. Furthermore, when the pile-up is accounted for in contact area determinations, the film hardness is actually independent of the substrate, thus indicating that the hardness differences observed in nanoindentation testing are an artifact of the testing analysis procedure. Results of the experiments are documented and discussed. 8 refs., 6 figs., 1 tab.
Book Synopsis Finite-element Modeling of Nanoindentation for Determining the Mechanical Properties of Implanted Layers and Thin Films by :
Download or read book Finite-element Modeling of Nanoindentation for Determining the Mechanical Properties of Implanted Layers and Thin Films written by and published by . This book was released on 1996 with total page 13 pages. Available in PDF, EPUB and Kindle. Book excerpt: The mechanical properties of implanted layers and thin films on dissimilar substrates are difficult to accurately determine. Nanoindentation of the layer provides information, but detailed numerical modeling is required in order to separate the properties of the layer from those of the substrate. We describe here the procedures we have developed to accomplish this modeling with the commercially available finite-element code ABAQUS. Using these techniques, we are able to extract from nanoindentation testing the yield stress, Young's modulus, and hardness of the layer material, with an absolute accuracy of at least 20%. The procedure is applicable to layers as thin as 50 nm on essentially any substrate, hard or soft. We have used it for materials ranging from ion-implanted layers to thin films of metals and dielectrics formed using plasma-deposition methods. An example is given of 0-implanted Al, a thin, hard layer on a soft substrate.
Book Synopsis Nanoindentation of Natural Materials by : Arjun Dey
Download or read book Nanoindentation of Natural Materials written by Arjun Dey and published by CRC Press. This book was released on 2018-09-03 with total page 235 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanoindentation of Natural Materials: Hierarchical and Functionally Graded Microstructures provides a systematic introduction and review of state-of-the-art statistical hierarchical and functionally graded structures found in bone, teeth, hair, and scales, from a nanoindentation perspective, including detailed microstructure and composition. It covers the basics of hierarchical and functionally graded structures and nanoindentation techniques and detailed discussion with correlation micro/nano mechanical-structures The book includes practical issues backed with experimental data
Book Synopsis Nanocomposite Thin Films and Coatings by : Sam Zhang
Download or read book Nanocomposite Thin Films and Coatings written by Sam Zhang and published by Imperial College Press. This book was released on 2007 with total page 628 pages. Available in PDF, EPUB and Kindle. Book excerpt: Materials development has reached a point where it is difficult for a single material to satisfy the needs of sophisticated applications in the modern world. Nanocomposite films and coatings achieve much more than the simple addition of the constitutents OCo the law of summation fails to work in the nano-world. This book encompasses three major parts of the development of nanocomposite films and coatings: the first focuses on processing and properties, the second concentrates on mechanical performance, and the third deals with functional performance, including wide application areas ranging from mechanical cutting to solar energy and from electronics to medicine. Sample Chapter(s). Chapter 1: Magnetron Sputtered Hard and Yet Tough Nanocomposite Coatings With Case Studies: Nanocrystalline Tin Embedded in Amorphous SiNx (187 KB). Contents: Magnetron Sputtered Hard and Yet Tough Nanocomposite Coatings with Case Studies: Nanocrystalline TiN Embedded in Amorphous SiN x (S Zhang et al.); Magnetron Sputtered Hard and Yet Tough Nanocomposite Coatings with Case Studies: Nanocrystalline TiC Embedded in Amorphous Carbon (S Zhang et al.); Properties of Chemical Vapor Deposited Nanocrystalline Diamond and Nanodiamond/Amorphous Carbon Composite Films (S C Tjong); Synthesis, Characterization and Applications of Nanocrystalline Diamond Films (Z-Q Xu & A Kumar); Properties of Hard Nanocomposite Thin Films (J Musil); Nanostructured, Multifunctional Tribological Coatings (J J Moore et al.); Nanocomposite Thin Films for Solar Energy Conversion (Y-B Yin); Application of Silicon Nanocrystal in Non-Volatile Memory Devices (T P Chen); Nanocrystalline Silicon Films for Thin Film Transistor and Optoelectronic Applications (Y-J Choi et al.); Amorphous and Nanocomposite Diamond-Like Carbon Coatings for Biomedical Applications (T I T Okpalugo et al.); Nanocoatings for Orthopaedic and Dental Application (W-Q Yan). Readership: Undergraduates, postgraduates, researchers, scientists, college and university professors, research professionals, technology investors and developers, research enterprises, R&D research laboratories, academic and research libraries."
Book Synopsis Factors Limiting the Accuracy of Mechanical Property Measurement by Nanoindentation by : Ting Yiu Tsui
Download or read book Factors Limiting the Accuracy of Mechanical Property Measurement by Nanoindentation written by Ting Yiu Tsui and published by . This book was released on 1996 with total page 664 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Nanotribology and Nanomechanics by : Bharat Bhushan
Download or read book Nanotribology and Nanomechanics written by Bharat Bhushan and published by Springer Science & Business Media. This book was released on 2008-05-10 with total page 1530 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume serves as a timely, practical introduction to the principles of nanotribology and nanomechanics and applications to magnetic storage systems and MEMS/NEMS. Assuming some familiarity with macrotribology/mechanics, the book comprises chapters by internationally recognized experts, who integrate knowledge of the field from the mechanics and materials-science perspectives. Graduate students, research workers, and practicing engineers will find the book of value.
