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Microreactors In Organic Chemistry And Catalysis
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Book Synopsis Microreactors in Organic Chemistry and Catalysis by : Thomas Wirth
Download or read book Microreactors in Organic Chemistry and Catalysis written by Thomas Wirth and published by John Wiley & Sons. This book was released on 2013-02-22 with total page 493 pages. Available in PDF, EPUB and Kindle. Book excerpt: For the second edition of 'Microreactors in Organic Chemistry and Catalysis' all chapters have been revised and updated to reflect the latest developments in this rapidly developing field. This new edition has 60% more content, and it remains a comprehensive publication covering most aspects of the topic. The use of microreactors in homogeneous, heterogeneous as well as biphasic reactions is covered in the main part of the book, together with catalytic, bioorganic and automation approaches. The initial chapters also provide a solid physical chemistry background on fluidics in microdevices. Finally, a chapter on industrial applications and developments covers recent progress in process chemistry. An excellent reference for beginners and experts alike.
Book Synopsis Microreactors in Organic Synthesis and Catalysis by : Thomas Wirth
Download or read book Microreactors in Organic Synthesis and Catalysis written by Thomas Wirth and published by John Wiley & Sons. This book was released on 2008-05-05 with total page 308 pages. Available in PDF, EPUB and Kindle. Book excerpt: This one-stop reference is the first book on this emerging and rapid developing field with a focus on synthesis and catalysis. As such, it covers all aspects from academia and industry in a clearly structured way. Leading experts provide the background information as an initial aid for newcomers to the field, while chapters on different reaction types and industrial applications make this an equally vital resource for specialists. From the contents: - Introduction and background - Fabrication of microractors - Properties and use of microreactors - Organic chemistry in microreactors - Homogeneous reactions (including photochemical and electrochemical reactions) - Heterogeneous reactions - Biphasic reactions (liquid/liquid, liquid/gas) - Bioorganic reactions - Industrial applications Thomas Wirth is Professor of Organic Chemistry at Cardiff University in Wales. After a postdoctoral stay with Kaoru Fuji at Kyoto University as a JSPS fellow, he started his independent research in the group of Bernd Giese in Basel, Switzerland. He was invited as a visiting professor to various places: University of Toronto, Canada (1999), Chuo University in Tokyo, Japan (2000), Osaka University, Japan (2004). He was awarded the Werner-Prize from the New Swiss Chemical Society in 2000. He is the author of about 80 publications and has written or edited 4 books.
Book Synopsis Microreactors in Preparative Chemistry by : Wladimir Reschetilowski
Download or read book Microreactors in Preparative Chemistry written by Wladimir Reschetilowski and published by John Wiley & Sons. This book was released on 2013-09-13 with total page 351 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the first book in the field to focus on these aspects, providing extremely valuable information unavailable elsewhere for anyone seeking the practical application of microreactor technology in preparative chemistry. The topics covered branch out in three different directions. To begin with, the knowledge necessary for the preparative chemistry concerning the influence of the so-called microeffects on the reaction procedure and on mass and heat transfer as well as the surface phenomena are provided in detail. Next, practical aspects of the synthesis of various basic chemicals and fine chemicals, polymers, bioproducts and nanoparticles are discussed, including important advice for both the researcher and industrial chemist. Finally, reaction examples in microreactors whose reaction guidance are best understood are given together with universally applicable correlations as well as modeling approaches and transfer potential on related reaction systems. With its specific instructions, tips and experimental procedures for product syntheses as well as the inclusion of both the technical and theoretical background this is a must-have for beginners and experts alike working in this emerging field.
Book Synopsis Novel Concepts in Catalysis and Chemical Reactors by : Andrzej Cybulski
Download or read book Novel Concepts in Catalysis and Chemical Reactors written by Andrzej Cybulski and published by John Wiley & Sons. This book was released on 2011-08-04 with total page 399 pages. Available in PDF, EPUB and Kindle. Book excerpt: The chemical process industry faces a tremendous challenge of supplying a growing and ever more demanding global population with the products we need. The average efficiency at which resources are converted into the final products is however still dramatically low. The most obvious solution is to carry out chemical conversions at much higher yields and selectivity and this is where active and selective catalysts and efficient chemical reactors play a crucial role. Written by an international team of highly experienced editors and authors from academia and industry, this ready reference focuses on how to enhance the efficiency of catalysts and reactors. It treats key topics such as molecular modeling, zeolites, MOFs, catalysis at room temperature, biocatalysis, catalysis for sustainability, structured reactors including membrane and microchannel reactors, switching from batch to continuous reactors, application of alternative energies and process intensification. By including recent achievements and trends, the book provides an up-to-date insight into the most important developments in the field of industrial catalysis and chemical reactor engineering. In addition, several ways of improving efficiency, selectivity, activity and improved methods for scale-up, modeling and design are presented in a compact manner.
Book Synopsis Microreactor Technology and Process Intensification by : Yong Wang
Download or read book Microreactor Technology and Process Intensification written by Yong Wang and published by . This book was released on 2005 with total page 468 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microreaction technology, with its unprecedented heat and mass transfer advantages as well as uniform residence time and flow pattern, is one of the few technologies with potential to develop efficient, environmentally benign, and compact processes. Novel fabrication and processing techniques, equipment, and operational methods are resulting in spectacular developments that go beyond "traditional" chemical engineering. These new developments promise improvements in process plants, and lead to the transformation of our concept of chemical plants into compact, safe, energy-efficient, and environmentally sustainable processes. Microsystems are now available in many devices for commercial applications including: micromixers and microreactors as alternative to batch production in pharmaceutical and fine chemical industry, lab-on-chip devices, microsensors, advanced rapid throughput chemical and catalyst screening tools (e.g. combi), distributed or portable power and chemical production, distributed heating and cooling, and even out of this world applications with NASA. A wide diversity of subjects are discussed in this book ranging from catalysis to fuel processing to combinatorial techniques to separations to novel reactors all of which are enabled by microtechnology principles. World renowned pioneers (Klavs Jensen, Volker Hessel, Jennifer Holmgren, and Galip Akay) provide accounts on both historical developments and the current state of the art as well as insights into future research and development in microreactor and process intensification. Research and developments are presented by industry, universities, U.S. National Laboratories, and other laboratories located in the United States and throughout the world. It is composed of peer-reviewed chapters from both contributing and invited authors. The review and original research topics include (1) introductory and general overviews, (2) microreactors- including catalysts for microreactors, fuel processors, milli-second contact time catalysis, gas to liquid technology, and biomass conversion; and (3) process intensification such as micro mixers, reactive membranes, and intensification of separation operations.
Book Synopsis Chemical Micro Process Engineering by : Volker Hessel
Download or read book Chemical Micro Process Engineering written by Volker Hessel and published by John Wiley & Sons. This book was released on 2006-03-06 with total page 712 pages. Available in PDF, EPUB and Kindle. Book excerpt: Micro process engineering is approaching both academia and industry. With the provision of micro devices and systems by commercial suppliers, one main barrier for using these units has been eliminated. More and more they become familiar, thereby being one facet of the upheaval in chemical industry. This book focuses on processes rather than on devices: what is 'before' and 'behind' micro device fabrication. A comprehensive and detailed overview is given on: - A multi-faceted, hierarchic analysis of chemical micro process technology - Modelling and simulation of micro reactors - Liquid- and liquid/liquid-phase reactions - Gas/liquid reactions - Gas-phase reactions (heterogeneous catalysis)
Book Synopsis Catalytic Reactors by : Basudeb Saha
Download or read book Catalytic Reactors written by Basudeb Saha and published by Walter de Gruyter GmbH & Co KG. This book was released on 2015-12-18 with total page 356 pages. Available in PDF, EPUB and Kindle. Book excerpt: Catalytic Reactors presents several key aspects of reactor design in Chemical and Process Engineering. Starting with the fundamental science across a broad interdisciplinary field, this graduate level textbook offers a concise overview on reactor and process design for students, scientists and practitioners new to the field. This book aims to collate into a comprehensive and well-informed work of leading researchers from north America, western Europe and south-east Asia. The editor and international experts discuss state-of-the-art applications of multifunctional reactors, biocatalytic membrane reactors, micro-flow reactors, industrial catalytic reactors, micro trickle bed reactors and multiphase catalytic reactors. The use of catalytic reactor technology is essential for the economic viability of the chemical manufacturing industry. The importance of Chemical and Process Engineering and efficient design of reactors are another focus of the book. Especially the combination of advantages from both catalysis and chemical reaction technology for optimization and intensification as essential factors in the future development of reactors and processes are discussed. Furthermore, options that can drastically influence reaction processes, e.g. choice of catalysts, alternative reaction pathways, mass and heat transfer effects, flow regimes and inherent design of catalytic reactors are reviewed in detail. Focuses on the state-of-the-art applications of catalytic reactors and optimization in the design and operation of industrial catalytic reactors Insights into transfer of knowledge from laboratory science to industry For students and researchers in Chemical and Mechanical Engineering, Chemistry, Industrial Catalysis and practising Engineers
Book Synopsis Chemical Reactor Development by : D. Thoenes
Download or read book Chemical Reactor Development written by D. Thoenes and published by Springer Science & Business Media. This book was released on 2013-12-14 with total page 358 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemical Reactor Development is written primarily for chemists and chemical engineers who are concerned with the development of a chemical synthesis from the laboratory bench scale, where the first successful experiments are performed, to the design desk, where the first commercial reactor is conceived. It is also written for those chemists and chemical engineers who are concerned with the further development of a chemical process with the objective of enhancing the performance of an existing industrial plant, as well as for students of chemistry and chemical engineering. In Part I, the `how' and the `why' of chemical reaction engineering are explained, particularly for those who are not familiar with this area. Part II deals with the effects of a number of physical phenomena on the outcome of chemical reactions, such as micro and meso-mixing and residence time distribution, mass transfer between two phases, and the formation of another phase, such as in precipitations. These scale-dependent effects are not only important in view of the conversion of chemical reactions, but also with regard to the selectivity, and in the case of solid products, to their morphology. In Part III, some applications are treated in a general way, including organic syntheses, the conversion and formation of inorganic solids, catalytic processes and polymerizations. The last chapter gives a review of the importance of the selectivity for product quality and for the purity of waste streams. For research chemists and chemical engineers whose work involves chemical reaction engineering. The book is also suitable as a supplementary graduate text.
Book Synopsis High-Throughput Screening in Chemical Catalysis by : Alfred Hagemeyer
Download or read book High-Throughput Screening in Chemical Catalysis written by Alfred Hagemeyer and published by John Wiley & Sons. This book was released on 2006-03-06 with total page 339 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this first book to present every important aspect of this fascinating and developing field, the three editors A. Hagemeyer, P. Strasser and A. F. Volpe Jr. from Symyx Technologies have chosen a perfect mixture of distinguished, international authors from both academia and industry. Each chapter is devoted to a major topic - high-throughput experimentation methodologies, integrated combinatorial synthesis and screening workflow, and applications to chemical catalysts with an emphasis on heterogeneous catalysis, olefin polymerization and electrocatalysis for fuel cells. An indispensable source for everyone working in the field.
Book Synopsis Multiphase Catalytic Reactors by : Zeynep Ilsen Önsan
Download or read book Multiphase Catalytic Reactors written by Zeynep Ilsen Önsan and published by John Wiley & Sons. This book was released on 2016-07-05 with total page 395 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides a holistic approach to multiphase catalytic reactors from their modeling and design to their applications in industrial manufacturing of chemicals Covers theoretical aspects and examples of fixed-bed, fluidized-bed, trickle-bed, slurry, monolith and microchannel reactors Includes chapters covering experimental techniques and practical guidelines for lab-scale testing of multiphase reactors Includes mathematical content focused on design equations and empirical relationships characterizing different multiphase reactor types together with an assortment of computational tools Involves detailed coverage of multiphase reactor applications such as Fischer-Tropsch synthesis, fuel processing for fuel cells, hydrotreating of oil fractions and biofuels processing
Book Synopsis Micro Reaction Technology in Organic Synthesis by : Charlotte Wiles
Download or read book Micro Reaction Technology in Organic Synthesis written by Charlotte Wiles and published by CRC Press. This book was released on 2016-04-19 with total page 453 pages. Available in PDF, EPUB and Kindle. Book excerpt: While continuous processes have found widespread application within chemical production, members of the research and development communities have historically favored the centuries old technique of iterative batch reactions. With the exception of combinatorial and microwave chemistry, little had been done to change the way that synthetic chemists c
Book Synopsis Catalytic Microreactors for Portable Power Generation by : Symeon Karagiannidis
Download or read book Catalytic Microreactors for Portable Power Generation written by Symeon Karagiannidis and published by Springer Science & Business Media. This book was released on 2011-03-28 with total page 112 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Catalytic Microreactors for Portable Power Generation” addresses a problem of high relevance and increased complexity in energy technology. This thesis outlines an investigation into catalytic and gas-phase combustion characteristics in channel-flow, platinum-coated microreactors. The emphasis of the study is on microreactor/microturbine concepts for portable power generation and the fuels of interest are methane and propane. The author carefully describes numerical and experimental techniques, providing a new insight into the complex interactions between chemical kinetics and molecular transport processes, as well as giving the first detailed report of hetero-/homogeneous chemical reaction mechanisms for catalytic propane combustion. The outcome of this work will be widely applied to the industrial design of micro- and mesoscale combustors.
Book Synopsis Chemical Reactions and Processes under Flow Conditions by : Santiago V Luis
Download or read book Chemical Reactions and Processes under Flow Conditions written by Santiago V Luis and published by Royal Society of Chemistry. This book was released on 2009-11-20 with total page 213 pages. Available in PDF, EPUB and Kindle. Book excerpt: Pharmaceutical and fine chemical products are typically synthesised batchwise which is an anomaly since batch processes have a series of practical and economical disadvantages. On the contrary, flow continuous processes present a series of advantages leading to new ways to synthesise chemical products. Flow processes - * enable control reaction parameters more precisely (temperature, residence time, amount of reagents and solvent etc.), leading to better reproducibility, safer and more reliable processes * can be performed more advantageously using immobilized reagents or catalysts * improve the selectivity and productivity of the process and possibly even the stability of the catalyst * offer opportunities for heat exchange and energy conservation as well as an easy separation and recycling of the reactants and products by adequate process design * achieve multistep syntheses by assembling a line of reactors with minimum or no purification in between two reaction steps * can be assured by facile automation * scale-up can be easily conducted by number-up With all the new research activity in manufacturing chemical products, this comprehensive book is very timely, as it summarises the latest trends in organic synthesis. It gives an insight into flow continuous processes, outlining the basic concepts and explaining the terminology of, and systems approach to, process design dealing with both homogeneous and heterogeneous catalysis and mini- or micro-reactors. The book contains case studies, extensive bibliographies and reference lists in each chapter to enable the reader to grasp the contents and to go on to more detailed texts on specific subjects if desired. The book is written by both organic chemists and engineers giving a multidisciplinary vision of the new tools and methodologies in this field. It is essential reading for organic chemists (in industry or academia) working alongside chemical engineers or who want to undertake chemical engineering projects. It will also be of interest for chemical engineers to see how basic engineering concepts are applied in modern organic chemistry.
Book Synopsis Flow and Microreactor Technology in Medicinal Chemistry by : Esther Alza
Download or read book Flow and Microreactor Technology in Medicinal Chemistry written by Esther Alza and published by John Wiley & Sons. This book was released on 2022-06-13 with total page 372 pages. Available in PDF, EPUB and Kindle. Book excerpt: Learn to master a powerful technology to enable a faster drug discovery workflow The ultimate dream for medicinal chemists is the ability to synthesize new drug-like compounds with the push of a button. The key to synthesizing chemical compounds more quickly and accurately lies in computer-controlled technologies that can be optimized by machine learning. Recent developments in computer-controlled automated syntheses that rely on miniature flow reactors—with integrated analysis of the resulting products—provide a workable technology for synthesizing new chemical substances very quickly and with minimal effort. In Flow and Microreactor Technology in Medicinal Chemistry, early adopters of this ground-breaking technology describe its current and potential uses in medicinal chemistry. Based on successful examples of the use of flow and microreactor synthesis for drug-like compounds, the book introduces current as well as emerging uses for automated synthesis in a drug discovery context. Flow and Microreactor Technology in Medicinal Chemistry readers will also find: Numerous case studies that address the most common applications of this technology in the day-to-day work of medicinal chemists How to integrate flow synthesis with drug discovery How to perform enantioselective reactions under continuous flow conditions Flow and Microreactor Technology in Medicinal Chemistry is a valuable practical reference for medicinal chemists, organic chemists, and natural products chemists, whether they are working in academia or in the pharmaceutical industry.
Book Synopsis Green Techniques for Organic Synthesis and Medicinal Chemistry by : Wei Zhang
Download or read book Green Techniques for Organic Synthesis and Medicinal Chemistry written by Wei Zhang and published by John Wiley & Sons. This book was released on 2012-07-23 with total page 769 pages. Available in PDF, EPUB and Kindle. Book excerpt: Green chemistry is a new way of looking at organic synthesis and the design of drug molecules, offering important environmental and economic advantages over traditional synthetic processes. Pharmaceutical companies are increasingly turning to the principles of green chemistry in an effort to reduce waste, reduce costs and develop environmentally benign processes. Green Techniques for Organic Synthesis and Medicinal Chemistry presents an overview of the established and emerging techniques in green organic chemistry, highlighting their applications in medicinal chemistry. The book is divided into four parts: Introduction: Introduces the reader to the toxicology of organic chemicals,their environmental impact, and the concept of green chemistry. Green Catalysis: Covers a variety of green catalytic techniques including organocatalysis, supported catalysis, biocatalysis, fluorous catalysis, and catalytic direct C-H bond activation reactions. Green Synthetic Techniques: Presents a series of new techniques, assessing the green chemistry aspects and limitations (i.e. cost, equipment, expertise). Techniques include reactions in alternative solvents, atom economic multicomponent reactions, microwave and ultrasonic reactions, solid-supported synthesis, fluorous and ionic liquid-based recycling techniques, and flow reactors. Green Techniques in Pharmaceutical Industry: Covers applications of green chemistry concepts and special techniques for medicinal chemistry, including synthesis, analysis, separation, formulation, , and drug delivery. Process and business case studies are included to illustrate the applications in the pharmaceutical industry. Green Techniques for Organic Synthesis and Medicinal Chemistry is an essential resource on green chemistry technologies for academic researchers, R&D professionals and students working in organic chemistry and medicinal chemistry.
Book Synopsis Enabling Tools and Techniques for Organic Synthesis by : Stephen G. Newman
Download or read book Enabling Tools and Techniques for Organic Synthesis written by Stephen G. Newman and published by John Wiley & Sons. This book was released on 2023-09-26 with total page 500 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides the practical knowledge of how new technologies impact organic synthesis, enabling the reader to understand literature, evaluate different techniques, and solve synthetic challenges In recent years, new technologies have impacted organic chemistry to the point that they are no longer the sole domain of dedicated specialists. Computational chemistry, for example, can now be used by organic chemists to help predict outcomes, understand selectivity, and decipher mechanisms. To be prepared to solve various synthetic problems, it is increasingly important for chemists to familiarize themselves with a range of current and emerging tools and techniques. Enabling Tools and Techniques for Organic Synthesis A Practical Guide to Experimentation, Automation, and Computation provides a broad overview of contemporary research and new technologies applied to organic synthesis. Detailed chapters, written by a team of experts from academia and industry, describe different state-of-the-art techniques such as computer-assisted retrosynthesis, spectroscopy prediction with computational chemistry, high throughput experimentation for reaction screening, and robotic and automated data collection methods. Emphasizing real-world practicality, the book includes chapters on programming for synthetic chemists, Machine Learning (ML) in chemical synthesis, concepts and applications of computational chemistry, and more. Highlights the most recent methods in organic synthesis and describes how to employ these techniques in a reader’s own research Familiarize readers with the application of computational chemistry and automation technology in organic synthesis Introduces synthetic chemists to electrochemistry, photochemistry, and flow chemistry Helps readers comprehend the literature, assess the strengths and limitations of each technique, and apply those tools to solve synthetic challenges Provides case studies and guided examples with graphical illustrations in each chapter Enabling Tools and Techniques for Organic Synthesis: A Practical Guide to Experimentation, Automation, and Computation is an invaluable reference for scientists needing an up-to-date introduction to new tools, graduate students wanting to expand their organic chemistry skills, and instructors teaching courses in advanced techniques for organic synthesis.
Book Synopsis Microreaction Technology by : M. Matlosz
Download or read book Microreaction Technology written by M. Matlosz and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 584 pages. Available in PDF, EPUB and Kindle. Book excerpt: IMRET 5 featured more than 80 oral and poster communications, covering the entire interdisciplinary field from design, production, modeling and characterization of microreactor devices to application of microstructured systems for production, energy and transportation, including many analytical and biological applications. A particularly strong topic was the investigation of the potential of microstructuring of reactors and systems components for process intensification. Perspectives of combining local, in situ, data acquisition with appropriate microstructuring of actuators and components within chemical and biological devices were explored in order to enhance process performance and facilitate process control.
