Micro Mesoporous Metallosilicates

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Micro-Mesoporous Metallosilicates

Author : Peng Wu
Publisher : John Wiley & Sons
ISBN 13 : 3527350942
Total Pages : 501 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Micro-Mesoporous Metallosilicates by : Peng Wu

Download or read book Micro-Mesoporous Metallosilicates written by Peng Wu and published by John Wiley & Sons. This book was released on 2024-05-28 with total page 501 pages. Available in PDF, EPUB and Kindle. Book excerpt: Micro-Mesoporous Metallosilicates Up-to-date and in-depth text bridging the technology gap between fundamental research and industry-scale applications of porous materials for catalysis Micro-Mesoporous Metallosilicates: Synthesis, Characterization, and Catalytic Applications comprehensively introduces the chemistry and catalytic technologies of metallosilicates, an important family of microporous crystalline zeolite and heteroatom-containing mesoporous materials, with a primary focus on design synthesis, characterization, theoretical studies, and catalytic applications of titanosilicates, tin-silicates, germanosilicates and Ti-mesosilica, and more. The text covers recent advances in the synthesis of titanosilicates, including hydrothermal synthesis, dry-gel conversion, fluoride-assisted synthesis, and post-synthesis methods, along with the synthesis of metallosilicates with two-dimensional lamellar structures and their structural modifications as well as applications in selective oxidation reactions. The text also discusses synthesis of germanosilicates with specially designed organic structure-directing agents, synthesis and catalytic applications of heteroatom-containing mesoporous silica, and dendritic mesoporous silica nanoparticles with unique wrinkled center-radial structures. Overall, every important porous metallosilicate and its synthesis, characterization, pore engineering, catalytic application, and industrial technique and process are covered. Specific sample topics discussed in Micro-Mesoporous Metallosilicates include: Chemical post-modifications of titanosilicates, in terms of the effects on transfer, adsorption/desorption, and surface reactions X-Ray based techniques, ultraviolet-visible-near infrared spectroscopy, Raman spectroscopy, and solid-state NMR spectroscopy Theoretical calculation as an effective tool and supplement to understand the catalytic active center, structural character, and Brønsted/Lewis acidity Titanosilicates in the liquid-phase epoxidation reaction of propylene and propylene chloride to corresponding epoxides Effects of particle sizes, oxidation state, and location sites of Au nanoparticles, and epoxidation performance of Ti-containing materials Delivering cutting-edge research and bridging the technology gap between fundamental research and industrial applications, Micro-Mesoporous Metallosilicates is a valuable resource for chemists, materials scientists, chemical engineers, and experienced researchers in related fields.

Chemical Catalysts for Biomass Upgrading

Author : Mark Crocker
Publisher : John Wiley & Sons
ISBN 13 : 3527344667
Total Pages : 634 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Chemical Catalysts for Biomass Upgrading by : Mark Crocker

Download or read book Chemical Catalysts for Biomass Upgrading written by Mark Crocker and published by John Wiley & Sons. This book was released on 2020-03-09 with total page 634 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive reference to the use of innovative catalysts and processes to turn biomass into value-added chemicals Chemical Catalysts for Biomass Upgrading offers detailed descriptions of catalysts and catalytic processes employed in the synthesis of chemicals and fuels from the most abundant and important biomass types. The contributors?noted experts on the topic?focus on the application of catalysts to the pyrolysis of whole biomass and to the upgrading of bio-oils. The authors discuss catalytic approaches to the processing of biomass-derived oxygenates, as exemplified by sugars, via reactions such as reforming, hydrogenation, oxidation, and condensation reactions. Additionally, the book provides an overview of catalysts for lignin valorization via oxidative and reductive methods and considers the conversion of fats and oils to fuels and terminal olefins by means of esterification/transesterification, hydrodeoxygenation, and decarboxylation/decarbonylation processes. The authors also provide an overview of conversion processes based on terpenes and chitin, two emerging feedstocks with a rich chemistry, and summarize some of the emerging trends in the field. This important book: -Provides a comprehensive review of innovative catalysts, catalytic processes, and catalyst design -Offers a guide to one of the most promising ways to find useful alternatives for fossil fuel resources -Includes information on the most abundant and important types of biomass feedstocks -Examines fields such as catalytic cracking, pyrolysis, depolymerization, and many more Written for catalytic chemists, process engineers, environmental chemists, bioengineers, organic chemists, and polymer chemists, Chemical Catalysts for Biomass Upgrading presents deep insights on the most important aspects of biomass upgrading and their various types.

Microporous Framework Solids

Author : Paul A. Wright
Publisher : Royal Society of Chemistry
ISBN 13 : 085404812X
Total Pages : 445 pages
Book Rating : 4.8/5 (54 download)

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Book Synopsis Microporous Framework Solids by : Paul A. Wright

Download or read book Microporous Framework Solids written by Paul A. Wright and published by Royal Society of Chemistry. This book was released on 2008 with total page 445 pages. Available in PDF, EPUB and Kindle. Book excerpt: The field of microporous solids in solid state chemistry has seen a huge expansion over the last decades with new developments in a diverse range of directions and applications. Drawing upon nature as an inspiration, scientists are continually extending known families and preparing porous solids with novel structures. In turn, the novel properties that these possess stimulate further research and applications. Microporous Framework Solids describes fundamental principles and experimental practices of the synthetic chemistry and physical characterisation of crystalline microporous solids. It al.

Chemistry of Zeolites and Related Porous Materials

Author : Ruren Xu
Publisher : John Wiley & Sons
ISBN 13 : 0470822368
Total Pages : 695 pages
Book Rating : 4.4/5 (78 download)

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Book Synopsis Chemistry of Zeolites and Related Porous Materials by : Ruren Xu

Download or read book Chemistry of Zeolites and Related Porous Materials written by Ruren Xu and published by John Wiley & Sons. This book was released on 2009-05-29 with total page 695 pages. Available in PDF, EPUB and Kindle. Book excerpt: Widely used in adsorption, catalysis and ion exchange, the family of molecular sieves such as zeolites has been greatly extended and many advances have recently been achieved in the field of molecular sieves synthesis and related porous materials. Chemistry of Zeolites and Related Porous Materials focuses on the synthetic and structural chemistry of the major types of molecular sieves. It offers a systematic introduction to and an in-depth discussion of microporous, mesoporous, and macroporous materials and also includes metal-organic frameworks. Provides focused coverage of the key aspects of molecular sieves Features two frontier subjects: molecular engineering and host-guest advanced materials Comprehensively covers both theory and application with particular emphasis on industrial uses This book is essential reading for researches in the chemical and materials industries and research institutions. The book is also indispensable for researches and engineers in R&D (for catalysis) divisions of companies in petroleum refining and the petrochemical and fine chemical industries.

Nanoporous Materials: Science And Engineering

Author : G Q Max Lu
Publisher : World Scientific
ISBN 13 : 178326179X
Total Pages : 911 pages
Book Rating : 4.7/5 (832 download)

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Book Synopsis Nanoporous Materials: Science And Engineering by : G Q Max Lu

Download or read book Nanoporous Materials: Science And Engineering written by G Q Max Lu and published by World Scientific. This book was released on 2004-11-22 with total page 911 pages. Available in PDF, EPUB and Kindle. Book excerpt: Porous materials are of scientific and technological importance because of the presence of voids of controllable dimensions at the atomic, molecular, and nanometer scales, enabling them to discriminate and interact with molecules and clusters. Interestingly the big deal about this class of materials is about the “nothingness” within — the pore space. International Union of Pure and Applied Chemistry (IUPAC) classifies porous materials into three categories — micropores of less than 2 nm in diameter, mesopores between 2 and 50 nm, and macropores of greater than 50 nm. In this book, nanoporous materials are defined as those porous materials with pore diameters less than 100 nm.Over the last decade, there has been an ever increasing interest and research effort in the synthesis, characterization, functionalization, molecular modeling and design of nanoporous materials. The main challenges in research include the fundamental understanding of structure-property relations and tailor-design of nanostructures for specific properties and applications. Research efforts in this field have been driven by the rapid growing emerging applications such as biosensor, drug delivery, gas separation, energy storage and fuel cell technology, nanocatalysis and photonics. These applications offer exciting new opportunities for scientists to develop new strategies and techniques for the synthesis and applications of these materials.This book provides a series of systematic reviews of the recent developments in nanoporous materials. It covers the following topics: (1) synthesis, processing, characterization and property evaluation; (2) functionalization by physical and/or chemical treatments; (3) experimental and computational studies on fundamental properties, such as catalytic effects, transport and adsorption, molecular sieving and biosorption; (4) applications, including photonic devices, catalysis, environmental pollution control, biological molecules separation and isolation, sensors, membranes, hydrogen and energy storage, etc./a

Perovskites and Related Mixed Oxides

Author : Pascal Granger
Publisher : John Wiley & Sons
ISBN 13 : 3527337636
Total Pages : 1050 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Perovskites and Related Mixed Oxides by : Pascal Granger

Download or read book Perovskites and Related Mixed Oxides written by Pascal Granger and published by John Wiley & Sons. This book was released on 2016-02-23 with total page 1050 pages. Available in PDF, EPUB and Kindle. Book excerpt: This comprehensive handbook and ready reference details all the main achievements in the field of perovskite-based and related mixed-oxide materials. The authors discuss, in an unbiased manner, the potentials as well as the challenges related to their use, thus offering new perspectives for research and development on both an academic and industrial level. The first volume begins by summarizing the different synthesis routes from molten salts at high temperatures to colloidal crystal template methods, before going on to focus on the physical properties of the resulting materials and their related applications in the fields of electronics, energy harvesting, and storage as well as electromechanics and superconductivity. The second volume is dedicated to the catalytic applications of perovskites and related mixed oxides, including, but not limited to total oxidation of hydrocarbons, dry reforming of methane and denitrogenation. The concluding section deals with the development of chemical reactors and novel perovskite-based applications, such as fuel cells and high-performance ceramic membranes. Throughout, the contributions clearly point out the intimate links between structure, properties and applications of these materials, making this an invaluable tool for materials scientists and for catalytic and physical chemists.

Nanochemistry

Author : Geoffrey A Ozin
Publisher : Royal Society of Chemistry
ISBN 13 : 1782626263
Total Pages : 840 pages
Book Rating : 4.7/5 (826 download)

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Book Synopsis Nanochemistry by : Geoffrey A Ozin

Download or read book Nanochemistry written by Geoffrey A Ozin and published by Royal Society of Chemistry. This book was released on 2015-10-09 with total page 840 pages. Available in PDF, EPUB and Kindle. Book excerpt: International interest in nanoscience research has flourished in recent years, as it becomes an integral part in the development of future technologies. The diverse, interdisciplinary nature of nanoscience means effective communication between disciplines is pivotal in the successful utilization of the science. Nanochemistry: A Chemical Approach to Nanomaterials is the first textbook for teaching nanochemistry and adopts an interdisciplinary and comprehensive approach to the subject. It presents a basic chemical strategy for making nanomaterials and describes some of the principles of materials self-assembly over 'all' scales. It demonstrates how nanometre and micrometre scale building blocks (with a wide range of shapes, compositions and surface functionalities) can be coerced through chemistry to organize spontaneously into unprecedented structures, which can serve as tailored functional materials. Suggestions of new ways to tackle research problems and speculations on how to think about assembling the future of nanotechnology are given. Primarily designed for teaching, this book will appeal to graduate and advanced undergraduate students. It is well illustrated with graphical representations of the structure and form of nanomaterials and contains problem sets as well as other pedagogical features such as further reading, case studies and a comprehensive bibliography.

Mesoporous Molecular Sieves 1998

Author : L. Bonneviot
Publisher : Elsevier
ISBN 13 : 0080536247
Total Pages : 633 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Mesoporous Molecular Sieves 1998 by : L. Bonneviot

Download or read book Mesoporous Molecular Sieves 1998 written by L. Bonneviot and published by Elsevier. This book was released on 1998-07-08 with total page 633 pages. Available in PDF, EPUB and Kindle. Book excerpt: The original properties of mesoporous molecular sieves are so unique that the design of most existing catalysts could be reconsidered. It might indeed be of interest to introduce MMS either as a support or as the active phase, merely on the basis of their high surface areas, narrow pore size distribution and flexibility in composition. The recent literature provides examples of MMS based catalysts of many types such as acid-base solids, supported metals and supported oxides, mixed oxides, anchored complexes and clusters, grafted organic functional groups and others. Examples of all these developments are documented in the present proceedings including some spectacular new proposals. The new metallic (Pt) mesophases are specially worth mentioning because they represent a new approach to producing non-supported highly dispersed metals.In these proceedings the reader will find feature articles and regular papers from many worldwide groups, covering all aspects of synthesis, physical characterization and catalytic reactivity of MMS and their chemically modified forms. It is actually remarkable that this recent development brought together an even broader spectrum of scientists from traditionally unrelated fields such as those of liquid crystals, surfactants, sol-gels, amorphous oxides and mixed oxides, solid state, adsorbents and heterogeneous catalysts. Obviously, this is a fast-growing research area which triggers the imagination and creativity at the cross-road between material design, molecular surface tailoring and catalytic applications.

Basic Principles in Applied Catalysis

Author : Manfred Baerns
Publisher : Springer Science & Business Media
ISBN 13 : 3662059819
Total Pages : 540 pages
Book Rating : 4.6/5 (62 download)

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Book Synopsis Basic Principles in Applied Catalysis by : Manfred Baerns

Download or read book Basic Principles in Applied Catalysis written by Manfred Baerns and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 540 pages. Available in PDF, EPUB and Kindle. Book excerpt: Written by a team of internationally recognized experts, this book addresses the most important types of catalytic reactions and catalysts as used in industrial practice. Both applied aspects and the essential scientific principles are described. The main topics can be summarized as follows: heterogeneous, homogeneous and biocatalysis, catalyst preparation and characterization, catalytic reaction engineering and kinetics, catalyst deactivation and industrial perspective.

Microporous and Mesoporous Solid Catalysts

Author : E. G. Derouane
Publisher :
ISBN 13 :
Total Pages : 272 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Microporous and Mesoporous Solid Catalysts by : E. G. Derouane

Download or read book Microporous and Mesoporous Solid Catalysts written by E. G. Derouane and published by . This book was released on 2006 with total page 272 pages. Available in PDF, EPUB and Kindle. Book excerpt: This series offers practical help for advanced undergraduate, graduate and postgraduate students, as well as experienced chemists in industry and academia working with catalysts in organic and organometallic synthesis. It features tested and validated procedures, authoritative reviews on classes of catalysts, and assessments of all types of catalysts. Micro- and Mesoporous Solid Catalysts describes the use of zeolites and mesoporous solids as catalysts for the production of fine and specialty chemicals. Specific tips and hints are provided and some typical procedures are described in detail. In addition to discussing the pros and cons, several major organic transformations are examined including aromatic substitutions, heterocyclic ring formation, amines synthesis, oligomerisation, oxidation and hydroxylation, and other regioselective and stereoselective reactions. Features tutorial introductory chapters, including tips and hints for achieving successful organic transformations. Important reactions are featured together with recommendations to resolve potential problems.

Chemistry of Silica and Zeolite-Based Materials

Author : Abderrazzak Douhal
Publisher : Elsevier
ISBN 13 : 0128178140
Total Pages : 465 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Chemistry of Silica and Zeolite-Based Materials by : Abderrazzak Douhal

Download or read book Chemistry of Silica and Zeolite-Based Materials written by Abderrazzak Douhal and published by Elsevier. This book was released on 2019-07-04 with total page 465 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemistry of Silica and Zeolite-Based Materials covers a wide range of topics related to silica-based materials from design and synthesis to applications in different fields of science and technology. Since silica is transparent and inert to the light, it is a very attractive host material for constructing artificial photosynthesis systems. As an earth-abundant oxide, silica is an ideal and basic material for application of various oxides, and the science and technology of silica-based materials are fundamentally important for understanding other oxide-based materials. The book examines nanosolvation and confined molecules in silica hosts, catalysis and photocatalysis, photonics, photosensors, photovoltaics, energy, environmental sciences, drug delivery, and health. Written by a highly experienced and internationally renowned team from around the world, Chemistry of Silica and Zeolite-Based Materials is ideal for chemists, materials scientists, chemical engineers, physicists, biologists, biomedical sciences, environmental scientists, toxicologists, and pharma scientists. --- "The enormous versatility of silica for building a large variety of materials with unique properties has been very well illustrated in this book.... The reader will be exposed to numerous potential applications of these materials – from photocatalytic, optical and electronic applications, to chemical reactivity in confined spaces and biological applications. This book is of clear interest not only to PhD students and postdocs, but also to researchers in this field seeking an understanding of the possible applications of meso and microporous silica-derived materials." - Professor Avelino Corma, Institute of Chemical Technology (ITQ-CSIC) and Polytechnical University of Valencia, Spain - Discusses the most important advances in various fields using silica materials, including nanosolvation and confined molecules in silica hosts, catalysis and photocatalysis, and other topics - Written by a global team of experts from a variety of science and technology disciplines - Ideal resource for chemists, materials scientists, and chemical engineers working with oxide-based materials

Heterogeneous Catalysts

Author : Wey Yang Teoh
Publisher : John Wiley & Sons
ISBN 13 : 352781356X
Total Pages : 768 pages
Book Rating : 4.5/5 (278 download)

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Book Synopsis Heterogeneous Catalysts by : Wey Yang Teoh

Download or read book Heterogeneous Catalysts written by Wey Yang Teoh and published by John Wiley & Sons. This book was released on 2021-02-23 with total page 768 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents state-of-the-art knowledge of heterogeneous catalysts including new applications in energy and environmental fields This book focuses on emerging techniques in heterogeneous catalysis, from new methodology for catalysts design and synthesis, surface studies and operando spectroscopies, ab initio techniques, to critical catalytic systems as relevant to energy and the environment. It provides the vision of addressing the foreseeable knowledge gap unfilled by classical knowledge in the field. Heterogeneous Catalysts: Advanced Design, Characterization and Applications begins with an overview on the evolution in catalysts synthesis and introduces readers to facets engineering on catalysts; electrochemical synthesis of nanostructured catalytic thin films; and bandgap engineering of semiconductor photocatalysts. Next, it examines how we are gaining a more precise understanding of catalytic events and materials under working conditions. It covers bridging pressure gap in surface catalytic studies; tomography in catalysts design; and resolving catalyst performance at nanoscale via fluorescence microscopy. Quantum approaches to predicting molecular reactions on catalytic surfaces follows that, along with chapters on Density Functional Theory in heterogeneous catalysis; first principles simulation of electrified interfaces in electrochemistry; and high-throughput computational design of novel catalytic materials. The book also discusses embracing the energy and environmental challenges of the 21st century through heterogeneous catalysis and much more. Presents recent developments in heterogeneous catalysis with emphasis on new fundamentals and emerging techniques Offers a comprehensive look at the important aspects of heterogeneous catalysis Provides an applications-oriented, bottoms-up approach to a high-interest subject that plays a vital role in industry and is widely applied in areas related to energy and environment Heterogeneous Catalysts: Advanced Design, Characterization and Applications is an important book for catalytic chemists, materials scientists, surface chemists, physical chemists, inorganic chemists, chemical engineers, and other professionals working in the chemical industry.

Hierarchically Structured Porous Materials

Author : B.-L. Su
Publisher : John Wiley & Sons
ISBN 13 : 3527639594
Total Pages : 676 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Hierarchically Structured Porous Materials by : B.-L. Su

Download or read book Hierarchically Structured Porous Materials written by B.-L. Su and published by John Wiley & Sons. This book was released on 2012-04-06 with total page 676 pages. Available in PDF, EPUB and Kindle. Book excerpt: This first book devoted to this hot field of science covers materials with bimodal, trimodal and multimodal pore size, with an emphasis on the successful design, synthesis and characterization of all kinds of hierarchically porous materials using different synthesis strategies. It details formation mechanisms related to different synthesis strategies while also introducing natural phenomena of hierarchy and perspectives of hierarchical science in polymers, physics, engineering, biology and life science. Examples are given to illustrate how to design an optimal hierarchically porous material for specific applications ranging from catalysis and separation to biomedicine, photonics, and energy conversion and storage. With individual chapters written by leading experts, this is the authoritative treatment, serving as an essential reference for researchers and beginners alike.

Nanocatalysis

Author : Vanesa Calvino-Casilda
Publisher : CRC Press
ISBN 13 : 1351786695
Total Pages : 241 pages
Book Rating : 4.3/5 (517 download)

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Book Synopsis Nanocatalysis by : Vanesa Calvino-Casilda

Download or read book Nanocatalysis written by Vanesa Calvino-Casilda and published by CRC Press. This book was released on 2019-02-14 with total page 241 pages. Available in PDF, EPUB and Kindle. Book excerpt: Synthesis and design of new nanocatalysts is an important area of research that aims to introduce multiple types of useful applications in a greener market. The necessity of nanostructuring the active sites has emerged as the key point in a successful design of the catalysts. The book covers the progress in this research area done in the last ten years. It includes the classification of catalysts and structure of active sites at the nanoscale. The book covers examples to present the concept, evolution of nanocatalysts from the perspective of chemistry of materials and their applications.

Zeolites and Metal-organic Frameworks

Author : Vincent Blay
Publisher :
ISBN 13 : 9789462985568
Total Pages : 0 pages
Book Rating : 4.9/5 (855 download)

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Book Synopsis Zeolites and Metal-organic Frameworks by : Vincent Blay

Download or read book Zeolites and Metal-organic Frameworks written by Vincent Blay and published by . This book was released on 2018 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book examines Zeolites and Metal-Organic Frameworks. It explains the different synthetic routes available to prepare these materials, and examines how they are used by science and industry.

Zeolite Characterization and Catalysis

Author : Arthur W. Chester
Publisher : Springer Science & Business Media
ISBN 13 : 140209678X
Total Pages : 372 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Zeolite Characterization and Catalysis by : Arthur W. Chester

Download or read book Zeolite Characterization and Catalysis written by Arthur W. Chester and published by Springer Science & Business Media. This book was released on 2009-10-03 with total page 372 pages. Available in PDF, EPUB and Kindle. Book excerpt: The idea for putting together a tutorial on zeolites came originally from my co-editor, Eric Derouane, about 5 years ago. I ?rst met Eric in the mid-1980s when he spent 2 years working for Mobil R&D at our then Corporate lab at Princeton, NJ. He was on the senior technical staff with projects in the synthesis and characterization of new materials. At that time, I managed a group at our Paulsboro lab that was responsible for catalyst characterization in support of our catalyst and process development efforts, and also had a substantial group working on new material synthesis. Hence, our interests overlapped considerably and we met regularly. After Eric moved back to Namur (initially), we maintained contact, and in the 1990s, we met a number of times in Europe on projects of joint interest. It was after I retired from ExxonMobil in 2002 that we began to discuss the tutorial concept seriously. Eric had (semi-)retired and lived on the Algarve, the southern coast of Portugal. In January 2003, my wife and I spent 3 weeks outside of Lagos, and I worked parts of most days with Eric on the proposed content of the book. We decided on a comprehensive approach that ultimately amounted to some 20+ chapters covering all of zeolite chemistry and catalysis and gave it the title Zeolite Chemistry and Catalysis: An integrated Approach and Tutorial.

Verified Synthesis of Zeolitic Materials

Author : H. Robson
Publisher : Gulf Professional Publishing
ISBN 13 : 9780444507037
Total Pages : 288 pages
Book Rating : 4.5/5 (7 download)

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Book Synopsis Verified Synthesis of Zeolitic Materials by : H. Robson

Download or read book Verified Synthesis of Zeolitic Materials written by H. Robson and published by Gulf Professional Publishing. This book was released on 2001-06-26 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Zeolite synthesis is an active field of research. As long as this continues, new phases will be discovered and new techniques for preparing existing phases will appear. This edition of Verified Synthesis of Zeolitic Materials contains all the recipes from the first edition plus 24 new recipes. Five new introductory articles have been included plus those from the first edition, some of which have been substantially revised. The XRD patterns have been recorded using different instrument settings from those in the first edition and are intended to conform to typical X-ray diffraction practice. In most cases, only the XRD pattern for the productas synthesised is printed here. The exceptions are those phases which show marked changes in the XRD pattern upon calcination.