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Extreme Diffusion Limited Electropolishing Of Niobium Radiofrequency Cavities
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Book Synopsis Extreme Diffusion Limited Electropolishing of Niobium Radiofrequency Cavities by :
Download or read book Extreme Diffusion Limited Electropolishing of Niobium Radiofrequency Cavities written by and published by . This book was released on 2017 with total page 6 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this study, a deeply modulated, regular, continuous, oscillating current waveform is reliably and repeatably achieved during electropolishing of niobium single-cell elliptical radiofrequency cavities. Details of the technique and cavity test results are reported here. The method is applicable for cavity frequencies in the range 500 MHz to 3.9 GHz and can be extended to multicell structures.
Book Synopsis Superconducting Radiofrequency Technology for Accelerators by : Hasan Padamsee
Download or read book Superconducting Radiofrequency Technology for Accelerators written by Hasan Padamsee and published by John Wiley & Sons. This book was released on 2023-05-15 with total page 405 pages. Available in PDF, EPUB and Kindle. Book excerpt: Superconducting Radiofrequency Technology for Accelerators Single source reference enabling readers to understand and master state-of-the-art accelerator technology Superconducting Radiofrequency Technology for Accelerators provides a quick yet thorough overview of the key technologies for current and future accelerators, including those projected to enable breakthrough developments in materials science, nuclear and astrophysics, high energy physics, neutrino research and quantum computing. The work is divided into three sections. The first part provides a review of RF superconductivity basics, the second covers new techniques such as nitrogen doping, nitrogen infusion, oxide-free niobium, new surface treatments, and magnetic flux expulsion, high field Q slope, complemented by discussions of the physics of the improvements stemming from diagnostic techniques and surface analysis as well as from theory. The third part reviews the on-going applications of RF superconductivity in already operational facilities and those under construction such as light sources, proton accelerators, neutron and neutrino sources, ion accelerators, and crab cavity facilities. The third part discusses planned accelerator projects such as the International Linear Collider, the Future Circular Collider, the Chinese Electron Positron Collider, and the Proton Improvement Plan-III facility at Fermilab as well as exciting new developments in quantum computing using superconducting niobium cavities. Written by the leading expert in the field of radiofrequency superconductivity, Superconducting Radiofrequency Technology for Accelerators covers other sample topics such as: Fabrication and processing on Nb-based SRF structures, covering cavity fabrication, preparation, and a decade of progress in the field SRF physics, covering zero DC resistance, the Meissner effect, surface resistance and surface impedance in RF fields, and non-local response of supercurrent N-doping and residual resistance, covering trapped DC flux losses, hydride losses, and tunneling measurements Theories for anti-Q-slope, covering the Xiao theory, the Gurevich theory, non-equilibrium superconductivity, and two fluid model based on weak defects Superconducting Radiofrequency Technology for Accelerators is an essential reference for high energy physicists, power engineers, and electrical engineers who want to understand the latest developments of accelerator technology and be able to harness it to further research interest and practical applications.
Book Synopsis Buffered Electropolishing - A New Way for Achieving Extremely Smooth Surface Finish on Nb SRF Cavities to be Used in Particle Accelerators by :
Download or read book Buffered Electropolishing - A New Way for Achieving Extremely Smooth Surface Finish on Nb SRF Cavities to be Used in Particle Accelerators written by and published by . This book was released on 2009 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Future accelerators require unprecedented cavity performance, which is strongly influenced by interior surface nano-smoothness. Electropolishing (EP) is the technique of choice to be developed for high-field superconducting radio frequency (SRF) cavities. Electrochemical impedance spectroscopy (EIS) and related techniques point to the electropolishing mechanism of Nb in a sulphuric and hydrofluoric acid electrolyte controlled by a compact surface salt film under F- diffusion-limited mass transport control. These and other findings are guiding a systematic characterization to form the basis for cavities process optimization.
Book Synopsis Basic Electropolishing Process Research and Development in Support of Improved Reliable Performance SRF Cavities for the Future Accelerator by :
Download or read book Basic Electropolishing Process Research and Development in Support of Improved Reliable Performance SRF Cavities for the Future Accelerator written by and published by . This book was released on 2009 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Future accelerators require unprecedented cavity performance, which is strongly influenced by interior surface nanosmoothness. Electropolishing is the technique of choice to be developed for high-field superconducting radiofrequency cavities. Electrochemical impedance spectroscopy (EIS) and related techniques point to the electropolishing mechanism of Nb in a sulfuric and hydrofluoric acid electrolyte of controlled by a compact surface salt film under F- diffusion-limited mass transport control. These and other findings are currently guiding a systematic characterization to form the basis for cavity process optimization, such as flowrate, electrolyte composition and temperature. This integrated analysis is expected to provide optimum EP parameter sets for a controlled, reproducible and uniform surface leveling for Nb SRF cavities.
Book Synopsis On the Mechanism of Niobium Electropolishing by : Ashwini Chandra
Download or read book On the Mechanism of Niobium Electropolishing written by Ashwini Chandra and published by . This book was released on 2012 with total page 118 pages. Available in PDF, EPUB and Kindle. Book excerpt: Abstract: Pure Niobium is the material used to make Superconducting Radio Frequency (SRF) cavities. These cavities need to be free from surface defects like pits, bumps and protrusions to achieve the best performance. Electropolishing is commonly used as a final process to give a good surface finish to the niobium surface. The standard electrolyte used for electropolishing niobium is a 1:9 ratio of HF (48%) and H2SO4 (96%) respectively. The mechanism of electropolishing is not fully understood and also the best electropolishing parameters need to be determined. Acid concentration, stirring, temperature and amount of material removed are the parameters expected to affect the surface finish. Their effect is studied using electrochemical polarization measurement, galvanostatic and potentiostatic techniques. The electro-dissolution occurring needs to be under mass transport control for the phenomenon of electropolishing to occur. This is characterized by the presence of a current density plateau in the niobium polarization curves. However Galvanostatic experimental result analysis points to other interfering transport processes as well. Results based on microscopy, surface profile measurement and current transient measurements for different electrode configurations indicate the presence of natural convection as one of the reason which could be causing deviation from a perfect semi infinite linear diffusion model.
Book Synopsis Research and Development for Electropolishing of Nb for ILC Accelerator Cavities by :
Download or read book Research and Development for Electropolishing of Nb for ILC Accelerator Cavities written by and published by . This book was released on 2009 with total page 7 pages. Available in PDF, EPUB and Kindle. Book excerpt: The objectives of this project are to 1, Expand the scientific and technological understanding of the effect of post-treatment (electropolish, buffered chemical polish, low-temperature baking) on the surface of niobium; 2, Relate the knowledge to the performance of niobium superconducting radiofrequency accelerator cavities; and, 3, Thereby design and demonstrate an electropolish process that can be applied to complete cavities.
Book Synopsis Nanostructural Features Degrading the Performance of Superconducting Radio Frequency Niobium Cavities Revealed by Transmission Electron Microscopy and Electron Energy Loss Spectroscopy by :
Download or read book Nanostructural Features Degrading the Performance of Superconducting Radio Frequency Niobium Cavities Revealed by Transmission Electron Microscopy and Electron Energy Loss Spectroscopy written by and published by . This book was released on 2015 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanoscale defect structure within the magnetic penetration depth of ~100 nm is key to the performance limitations of niobium superconducting radio frequency cavities. Using a unique combination of advanced thermometry during cavity RF measurements, and TEM structural and compositional characterization of the samples extracted from cavity walls, we discover the existence of nanoscale hydrides in electropolished cavities limited by the high field Q slope, and show the decreased hydride formation in the electropolished cavity after 120°C baking. Furthermore, we demonstrate that adding 800°C hydrogen degassing followed by light buffered chemical polishing restores the hydride formation to the pre-120°C bake level. We also show absence of niobium oxides along the grain boundaries and the modifications of the surface oxide upon 120°C bake.
Book Synopsis Advance in Vertical Buffered Electropolishing on Niobium for Particle Accelerators* by :
Download or read book Advance in Vertical Buffered Electropolishing on Niobium for Particle Accelerators* written by and published by . This book was released on 2011 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Niobium (Nb) is the most popular material that has been employed for making superconducting radio frequency (SRF) cavities to be used in various particle accelerators over the last couple of decades. One of the most important steps in fabricating Nb SRF cavities is the final chemical removal of 150 [mu]m of Nb from the inner surfaces of the SRF cavities. This is usually done by either buffered chemical polishing (BCP) or electropolishing (EP). Recently a new Nb surface treatment technique called buffered electropolishing (BEP) has been developed at Jefferson Lab. It has been demonstrated that BEP can produce the smoothest surface finish on Nb ever reported in the literature while realizing a Nb removal rate as high as 10 [mu]m/min that is more than 25 and 5 times quicker than those of EP and BCP(112) respectively. In this contribution, recent advance in optimizing and understanding BEP treatment technique is reviewed. Latest results from RF measurements on BEP treated Nb single cell cavities by our unique vertical polishing system will be reported.
Book Synopsis Exploiting New Electrochemical Understanding of Niobium Electropolishing for Improved Performance of SRF Cavities for CEBAF. by :
Download or read book Exploiting New Electrochemical Understanding of Niobium Electropolishing for Improved Performance of SRF Cavities for CEBAF. written by and published by . This book was released on 2010 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Recent incorporation of analytic electrochemistry into the development of protocols for electropolishing niobium SRF cavities has yielded new insights for optimizing this process for consistent, high-performance results. Use of reference electrodes in the electrolyte, electrochemical impedance spectroscopy (EIS), rotating disk electrodes (RDE), and controlled sample temperatures has greatly clarified the process dynamics over the empirical understanding developed via years of practice. Minimizing RF losses at high operational gradients is very valuable for CW linacs. Jefferson Lab is applying these new insights to the low-loss 7-cell cavity design developed for the CEBAF 12 GeV Upgrade. Together with controlled cleaning and assembly techniques to guard against field-emission-causing particulates, the resulting process is yielding consistent cavity performance that exceeds project requirements. Cavity tests show BCS-limited Q well above 30 MV/m. Detailed process data, interpretation, and resulting rf performance data will be presented.
Book Synopsis Investigation of the Superconducting Properties of Niobium Radio-frequency Cavities by : Gianluigi Ciovati
Download or read book Investigation of the Superconducting Properties of Niobium Radio-frequency Cavities written by Gianluigi Ciovati and published by . This book was released on 2005 with total page 398 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Fastest Electropolishing Technique on Niobium for Particle Accelerators by :
Download or read book Fastest Electropolishing Technique on Niobium for Particle Accelerators written by and published by . This book was released on 2011 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Field emission on the inner surfaces of niobium (Nb) superconducting radio frequency (SRF) cavities is still one of the major obstacles for reaching high accelerating gradients for SRF community. Our previous experimental results [1] seemed to imply that the threshold of field emission was related to the thickness of Nb surface oxide layers. In this contribution, a more detailed study on the influences of the surface oxide layers on the field emission on Nb surfaces will be reported. By anodization technique, the thickness of the surface pentoxide layer was artificially fabricated from 3nm up to 460nm. A home-made scanning field emission microscope (SFEM) was employed to perform the scans on the surfaces. Emitters were characterized using a scanning electron microscope together with an energy dispersive x-ray analyzer. The experimental results could be understood by a simple model calculation based on classic electromagnetic theory as shown in Ref. 1. Possibly implications for Nb SRF cavity applications from this study will be discussed.
Book Synopsis Surface Polishing of Niobium for Superconducting Radio Frequency (SRF) Cavity Application by : Liang Zhao (Ph. D.)
Download or read book Surface Polishing of Niobium for Superconducting Radio Frequency (SRF) Cavity Application written by Liang Zhao (Ph. D.) and published by . This book was released on 2015 with total page 237 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Surface Polishing of Niobium for Superconducting Radio Frequency (SRF) Cavity Applications by :
Download or read book Surface Polishing of Niobium for Superconducting Radio Frequency (SRF) Cavity Applications written by and published by . This book was released on 2014 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Niobium cavities are important components in modern particle accelerators based on superconducting radio frequency (SRF) technology. The interior of SRF cavities are cleaned and polished in order to produce high accelerating field and low power dissipation on the cavity wall. Current polishing methods, buffered chemical polishing (BCP) and electro-polishing (EP), have their advantages and limitations. We seek to improve current methods and explore laser polishing (LP) as a greener alternative of chemical methods. The topography and removal rate of BCP at different conditions (duration, temperature, sample orientation, flow rate) was studied with optical microscopy, scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD). Differential etching on different crystal orientations is the main contributor to fine grain niobium BCP topography, with gas evolution playing a secondary role. The surface of single crystal and bi-crystal niobium is smooth even after heavy BCP. The topography of fine grain niobium depends on total removal. The removal rate increases with temperature and surface acid flow rate within the rage of 0~20 °C, with chemical reaction being the possible dominate rate control mechanism. Surface flow helps to regulate temperature and avoid gas accumulation on the surface. The effect of surface flow rate on niobium EP was studied with optical microscopy, atomic force microscopy (AFM), and power spectral density (PSD) analysis. Within the range of 0~3.7 cm/s, no significant difference was found on the removal rate and the macro roughness. Possible improvement on the micro roughness with increased surface flow rate was observed. The effect of fluence and pulse accumulation on niobium topography during LP was studied with optical microscopy, SEM, AFM, and PSD analysis. Polishing on micro scale was achieved within fluence range of 0.57~0.90 J/cm2, with pulse accumulation adjusted accordingly. Larger area treatment was proved possible by overlapping laser tracks at proper ratio. Comparison of topography and PSD indicates that LP smooths the surface in a way similar to EP. The optimized LP parameters were applied to different types of niobium surfaces representing different stages in cavity fabrication. LP reduces the sharpness on rough surfaces effectively, while doing no harm to smooth surfaces. Secondary ion mass spectrometer (SIMS) analysis showed that LP reduces the oxide layer slightly and no contamination occurred from LP. EBSD showed no significant change on crystal structure after LP.
Book Synopsis High Gradient Superconducting Niobium Cavities by :
Download or read book High Gradient Superconducting Niobium Cavities written by and published by . This book was released on 1998 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Superconducting niobium cavities used in particle accelerators are limited in their rf performance by two phenomena: quench field levels below the theoretical limit of the material caused by defects, and field emission loading resulting from artificial contamination of the superconducting surfaces during surface treatment and assembly procedures. In recent years, the community involved in SRF technology developments has successfully improved cavity performances by applying advanced surface treatment methods such as chemical polishing, electropolishing, tumbling, high temperature heat treatment, high pressure rinsing, ''in situ'' high peak power processing, and clean room assembly procedures. In addition, improvements in the material properties such as thermal conductivity by ''solid state'' gettering'' and very strict QA methods, both in material inspection and during cavity fabrication, have resulted in cavity performance levels of E{sub acc} up to 40 MV/m in monocells and gradients in the vicinity of 30 MV/m in multicell structures at Q-values of (almost equal to) 101° at a temperature of 2K. More recently the fabrication of ''seamless'' cavities by spinning is being pursued with encouraging results. This process eliminates electron beam welds, which sometimes are the causes of performance degradations.
Book Synopsis Innovative Severe Plastic Deformation of Niobium with Application to Superconducting Radio Frequency Cavities by : Nicholas Gutzmore Bembridge
Download or read book Innovative Severe Plastic Deformation of Niobium with Application to Superconducting Radio Frequency Cavities written by Nicholas Gutzmore Bembridge and published by . This book was released on 2011 with total page 276 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Probing the Fundamental Limit of Niobium in High Radiofrequency Fields by Dual Mode Excitation in Superconducting Radiofrequency Cavities by :
Download or read book Probing the Fundamental Limit of Niobium in High Radiofrequency Fields by Dual Mode Excitation in Superconducting Radiofrequency Cavities written by and published by . This book was released on 2011 with total page 4 pages. Available in PDF, EPUB and Kindle. Book excerpt: We have studied thermal breakdown in several multicell superconducting radiofrequency cavity by simultaneous excitation of two TM010 passband modes. Unlike measurements done in the past, which indicated a clear thermal nature of the breakdown, our measurements present a more complex picture with interplay of both thermal and magnetic effects. JLab LG-1 that we studied was limited at 40.5 MV/m, corresponding to B{sub peak} = 173 mT, in 8?/9 mode. Dual mode measurements on this quench indicate that this quench is not purely magnetic, and so we conclude that this field is not the fundamental limit in SRF cavities.
Book Synopsis Surface Characterization of Nb Samples Electropolished Together with Real Superconducting Rf Accelerator Cavities by :
Download or read book Surface Characterization of Nb Samples Electropolished Together with Real Superconducting Rf Accelerator Cavities written by and published by . This book was released on 2010 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Here, we report the results of surface characterizations of niobium (Nb) samples electropolished together with a single cell superconducting radio-frequency accelerator cavity. These witness samples were located in three regions of the cavity, namely at the equator, the iris and the beam-pipe. Auger electron spectroscopy (AES) was utilized to probe the chemical composition of the topmost four atomic layers. Scanning electron microscopy with energy dispersive X-ray for elemental analysis (SEM/EDX) was used to observe the surface topography and chemical composition at the micrometer scale. A few atomic layers of sulfur (S) were found covering the samples non-uniformly. Niobium oxide granules with a sharp geometry were observed on every sample. Some Nb-O granules appeared to also contain sulfur.
