Experimental Methods In Catalytic Research

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Experimental Methods in Catalytic Research

Author : Robert B. Anderson
Publisher : Academic Press
ISBN 13 : 1483191400
Total Pages : 513 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis Experimental Methods in Catalytic Research by : Robert B. Anderson

Download or read book Experimental Methods in Catalytic Research written by Robert B. Anderson and published by Academic Press. This book was released on 2013-10-22 with total page 513 pages. Available in PDF, EPUB and Kindle. Book excerpt: Experimental Methods in Catalytic Research, Volume I provides a useful account of procedures in various areas of catalytic research. This book describes the method and its fundamental principles, the apparatus used, the data obtained and their interpretation, and the account of the special problems related to catalytic research. Organized into 11 chapters, this volume begins with an overview of the kinetic phenomena such as quantitative studies of reaction rate and factors influencing rate. This text then examines the general properties that are of major importance to catalysis since catalytic rates depend mainly on available active surface. Other chapters consider the detailed mechanism of any catalytic reaction, which include the electronic structure of the chemisorption bond. This book discusses as well several experimental methods developed to study surface reactions under highly idealized conditions. The final chapter deals with the phenomenon associated with the spin of an electron. This book is a valuable resource for chemical engineers.

Experimental Methods in Catalytic Research

Author : Peter T. Dawson
Publisher : New York : Academic Press
ISBN 13 :
Total Pages : 520 pages
Book Rating : 4.:/5 (89 download)

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Book Synopsis Experimental Methods in Catalytic Research by : Peter T. Dawson

Download or read book Experimental Methods in Catalytic Research written by Peter T. Dawson and published by New York : Academic Press. This book was released on 1968 with total page 520 pages. Available in PDF, EPUB and Kindle. Book excerpt: Experimental Methods in Catalytic Research, Volume I provides a useful account of procedures in various areas of catalytic research. This book describes the method and its fundamental principles, the apparatus used, the data obtained and their interpretation, and the account of the special problems related to catalytic research. Organized into 11 chapters, this volume begins with an overview of the kinetic phenomena such as quantitative studies of reaction rate and factors influencing rate. This text then examines the general properties that are of major importance to catalysis since catalytic ...

Experimental Methods in Catalytic Research: Experimental methods in catalytic research

Author : Robert Bernard Anderson
Publisher :
ISBN 13 :
Total Pages : 0 pages
Book Rating : 4.:/5 (378 download)

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Book Synopsis Experimental Methods in Catalytic Research: Experimental methods in catalytic research by : Robert Bernard Anderson

Download or read book Experimental Methods in Catalytic Research: Experimental methods in catalytic research written by Robert Bernard Anderson and published by . This book was released on 1968 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Experiments in Catalytic Reaction Engineering

Author : J.M. Berty
Publisher : Elsevier
ISBN 13 : 0080531423
Total Pages : 289 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Experiments in Catalytic Reaction Engineering by : J.M. Berty

Download or read book Experiments in Catalytic Reaction Engineering written by J.M. Berty and published by Elsevier. This book was released on 1999-08-11 with total page 289 pages. Available in PDF, EPUB and Kindle. Book excerpt: The science of catalytic reaction engineering studies the catalyst and the catalytic process in the laboratory in order to predict how they will perform in production-scale reactors. Surprises are to be avoided in the scaleup of industrial processes. The laboratory results must account for flow, heat and mass transfer influences on reaction rate to be useful for scaleup. Calculated performance based on these results must also be useful to maximization of profit and safety and minimization of pollution. To this end, information on products as well as byproducts and heat produced must be generated. If a sufficiently large database of knowledge is produced, optimization studies will be possible later if economic conditions change.The field of reaction engineering required new tools. For kinetic and catalyst testing, the most successful of these tools was the internal recycle reactor. Studies in recycle reactors can be made under well-defined conditions of flow and associated transfer processes, and close to commercial operation. The recycle reactor eliminates or minimizes the effect of transfer process, and allows the remaining ones to be known.Features of this book:• Provides insight into a field that is neither well understood nor properly appreciated.• Gives a deeper understanding of reaction engineering practice.• Helps avoid frustration and disappointment in industrial research. This book is short and clear enough to assist all members of the R&D and Engineering team, whether reaction engineers, or specialists in other fields. This is critical in this new age of computation and communication, when team members must each know at least something of their colleagues' fields. Additionally, many scientists in more exploratory or fundamental fields can use recycle reactors to study basic phenomena free of transfer interactions.

Experimental Methods in Catalytic Research

Author : Robert Bernard Anderson
Publisher : New York : Academic Press
ISBN 13 :
Total Pages : 352 pages
Book Rating : 4.E/5 ( download)

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Book Synopsis Experimental Methods in Catalytic Research by : Robert Bernard Anderson

Download or read book Experimental Methods in Catalytic Research written by Robert Bernard Anderson and published by New York : Academic Press. This book was released on 1968 with total page 352 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Catalysis Looks to the Future

Author : National Research Council
Publisher : National Academies Press
ISBN 13 : 0309045843
Total Pages : 97 pages
Book Rating : 4.3/5 (9 download)

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Book Synopsis Catalysis Looks to the Future by : National Research Council

Download or read book Catalysis Looks to the Future written by National Research Council and published by National Academies Press. This book was released on 1992-02-01 with total page 97 pages. Available in PDF, EPUB and Kindle. Book excerpt: The impact of catalysis on the nation's economy is evidenced by the fact that catalytic technologies generate U.S. sales in excess of $400 billion per year and a net positive balance of trade of $16 billion annually. This book outlines recent accomplishments in the science and technology of catalysis and summarizes important likely challenges and opportunities on the near horizon. It also presents recommendations for investment of financial and human resources by industry, academe, national laboratories, and relevant federal agencies if the nation is to maintain continuing leadership in this fieldâ€"one that is critical to the chemical and petroleum processing industries, essential for energy-efficient means for environmental protection, and vital for the production of a broad range of pharmaceuticals.

Experimental Methods for Evaluation of Hydrotreating Catalysts

Author : Jorge Ancheyta
Publisher : John Wiley & Sons
ISBN 13 : 1119517990
Total Pages : 429 pages
Book Rating : 4.1/5 (195 download)

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Book Synopsis Experimental Methods for Evaluation of Hydrotreating Catalysts by : Jorge Ancheyta

Download or read book Experimental Methods for Evaluation of Hydrotreating Catalysts written by Jorge Ancheyta and published by John Wiley & Sons. This book was released on 2020-06-08 with total page 429 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents detailed information and study cases on experiments on hydrotreating catalysts for the petroleum industry Catalytic hydrotreating (HDT) is a process used in the petroleum refining industry for upgrading hydrocarbon streams—removing impurities, eliminating metals, converting asphaltene molecules, and hydrocracking heavy fractions. The major applications of HDT in refinery operations include feed pretreatment for conversion processes, post-hydrotreating distillates, and upgrading heavy crude oils. Designing HDT processes and catalysts for successful commercial application requires experimental studies based on appropriate methodologies. Experimental Methods for Evaluation of Hydrotreating Catalysts provides detailed descriptions of experiments in different reaction scales for studying the hydrotreating of various petroleum distillates. Emphasizing step-by-step methodologies in each level of experimentation, this comprehensive volume presents numerous examples of evaluation methods, operating conditions, reactor and catalyst types, and process configurations. In-depth chapters describe experimental setup and procedure, analytical methods, calculations, testing and characterization of catalyst and liquid products, and interpretation of experiment data and results. The text describes experimental procedure at different levels of experimentation—glass reactor, batch reactor, continuous stirred tank reactor, and multiple scales of tubular reactors—using model compounds, middle distillates and heavy oil. This authoritative volume: Introduces experimental setups used for conducting research studies, such as type of operation, selection of reactor, and analysis of products Features examples focused on the evaluation of different reaction parameters and catalysts with a variety of petroleum feedstocks Provides experimental data collected from different reaction scales Includes experiments for determining mass transfer limitations and deviation from ideality of flow pattern Presents contributions from leading scientists and researchers in the field of petroleum refining Experimental Methods for Evaluation of Hydrotreating Catalysts is an indispensable reference for researchers and professionals working in the area of catalytic hydrotreating, as well as an ideal textbook for courses in fields such as chemical engineering, petrochemical engineering, and biotechnology.

Heterogeneous Catalytic Materials

Author : Guido Busca
Publisher : Newnes
ISBN 13 : 044459521X
Total Pages : 479 pages
Book Rating : 4.4/5 (445 download)

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Book Synopsis Heterogeneous Catalytic Materials by : Guido Busca

Download or read book Heterogeneous Catalytic Materials written by Guido Busca and published by Newnes. This book was released on 2014-05-23 with total page 479 pages. Available in PDF, EPUB and Kindle. Book excerpt: Heterogeneous Catalytic Materials discusses experimental methods and the latest developments in three areas of research: heterogeneous catalysis; surface chemistry; and the chemistry of catalysts. Catalytic materials are those solids that allow the chemical reaction to occur efficiently and cost-effectively. This book provides you with all necessary information to synthesize, characterize, and relate the properties of a catalyst to its behavior, enabling you to select the appropriate catalyst for the process and reactor system. Oxides (used both as catalysts and as supports for catalysts), mixed and complex oxides and salts, halides, sulfides, carbides, and unsupported and supported metals are all considered. The book encompasses applications in industrial chemistry, refinery, petrochemistry, biomass conversion, energy production, and environmental protection technologies. - Provides a systematic and clear approach of the synthesis, solid state chemistry and surface chemistry of all solid state catalysts - Covers widely used instrumental techniques for catalyst characterization, such as x-ray photoelectron spectroscopy, scanning electron microscopy, and more - Includes characterization methods and lists all catalytic behavior of the solid state catalysts - Discusses new developments in nanocatalysts and their advantages over conventional catalysts

Operando Research in Heterogeneous Catalysis

Author : Joost Frenken
Publisher : Springer
ISBN 13 : 3319444395
Total Pages : 232 pages
Book Rating : 4.3/5 (194 download)

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Book Synopsis Operando Research in Heterogeneous Catalysis by : Joost Frenken

Download or read book Operando Research in Heterogeneous Catalysis written by Joost Frenken and published by Springer. This book was released on 2016-12-26 with total page 232 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is devoted to the emerging field of techniques for visualizing atomic-scale properties of active catalysts under actual working conditions, i.e. high gas pressures and high temperatures. It explains how to understand these observations in terms of the surface structures and dynamics and their detailed interplay with the gas phase. This provides an important new link between fundamental surface physics and chemistry, and applied catalysis. The book explains the motivation and the necessity of operando studies, and positions these with respect to the more traditional low-pressure investigations on the one hand and the reality of industrial catalysis on the other. The last decade has witnessed a rapid development of new experimental and theoretical tools for operando studies of heterogeneous catalysis. The book has a strong emphasis on the new techniques and illustrates how the challenges introduced by the harsh, operando conditions are faced for each of these new tools. Therefore, one can also read this book as a collection of recipes for the development of operando instruments. At present, the number of scientific results obtained under operando conditions is still limited and mostly focused on a simple test reaction, the catalytic oxidation of CO. This reaction thus forms a natural binding element between the chapters, linking the demonstrations of new techniques, and also connecting the theoretical and experimental studies. Some first results on other reactions are also presented. If there is one thing that can be concluded already in this early stage, it is that the catalytic conditions themselves can have dramatic effects on the structure and composition of the surfaces of catalysts, which, in turn can greatly affect the mechanisms, the activity, and the selectivity of the chemical reactions that they catalyze.

Catalog of Copyright Entries. Third Series

Author : Library of Congress. Copyright Office
Publisher : Copyright Office, Library of Congress
ISBN 13 :
Total Pages : 1686 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Catalog of Copyright Entries. Third Series by : Library of Congress. Copyright Office

Download or read book Catalog of Copyright Entries. Third Series written by Library of Congress. Copyright Office and published by Copyright Office, Library of Congress. This book was released on 1978 with total page 1686 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Experimental Methods for Evaluation of Hydrotreating Catalysts

Author : Jorge Ancheyta
Publisher : John Wiley & Sons
ISBN 13 : 1119518008
Total Pages : 561 pages
Book Rating : 4.1/5 (195 download)

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Book Synopsis Experimental Methods for Evaluation of Hydrotreating Catalysts by : Jorge Ancheyta

Download or read book Experimental Methods for Evaluation of Hydrotreating Catalysts written by Jorge Ancheyta and published by John Wiley & Sons. This book was released on 2020-03-13 with total page 561 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents detailed information and study cases on experiments on hydrotreating catalysts for the petroleum industry Catalytic hydrotreating (HDT) is a process used in the petroleum refining industry for upgrading hydrocarbon streams—removing impurities, eliminating metals, converting asphaltene molecules, and hydrocracking heavy fractions. The major applications of HDT in refinery operations include feed pretreatment for conversion processes, post-hydrotreating distillates, and upgrading heavy crude oils. Designing HDT processes and catalysts for successful commercial application requires experimental studies based on appropriate methodologies. Experimental Methods for Evaluation of Hydrotreating Catalysts provides detailed descriptions of experiments in different reaction scales for studying the hydrotreating of various petroleum distillates. Emphasizing step-by-step methodologies in each level of experimentation, this comprehensive volume presents numerous examples of evaluation methods, operating conditions, reactor and catalyst types, and process configurations. In-depth chapters describe experimental setup and procedure, analytical methods, calculations, testing and characterization of catalyst and liquid products, and interpretation of experiment data and results. The text describes experimental procedure at different levels of experimentation—glass reactor, batch reactor, continuous stirred tank reactor, and multiple scales of tubular reactors—using model compounds, middle distillates and heavy oil. This authoritative volume: Introduces experimental setups used for conducting research studies, such as type of operation, selection of reactor, and analysis of products Features examples focused on the evaluation of different reaction parameters and catalysts with a variety of petroleum feedstocks Provides experimental data collected from different reaction scales Includes experiments for determining mass transfer limitations and deviation from ideality of flow pattern Presents contributions from leading scientists and researchers in the field of petroleum refining Experimental Methods for Evaluation of Hydrotreating Catalysts is an indispensable reference for researchers and professionals working in the area of catalytic hydrotreating, as well as an ideal textbook for courses in fields such as chemical engineering, petrochemical engineering, and biotechnology.

Catalysis

Author : B. Viswanathan
Publisher : CRC Press
ISBN 13 : 9780849324246
Total Pages : 428 pages
Book Rating : 4.3/5 (242 download)

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Book Synopsis Catalysis by : B. Viswanathan

Download or read book Catalysis written by B. Viswanathan and published by CRC Press. This book was released on 2002 with total page 428 pages. Available in PDF, EPUB and Kindle. Book excerpt: Students contemplating careers in chemistry, whether in research, practice, or academia, obviously need a solid grounding in proper research methodology, reasoning, and analysis. However, there are few resources available that efficiently and effectively introduce these concepts and techniques and inspire students to undertake advanced research, particularly in the area of catalysis. Catalysis: Principles and Applications evolved out of a special, resoundingly successful short course for graduate students interested in catalysis. It covers nearly the entire gamut of the subject, from its fundamentals to its modern, applied aspects. The chapters were contributed by catalysis specialists from leading academic institutions, national laboratories and industrial R&D labs. Because they are based on the authors' lecture notes, each chapter is highly accessible and for the most part self-contained. Topics include various spectroscopic methods, biocatalysis, x-ray and thermal analysis, photocatalysis, and recent developments, such as solid acid catalysts, fine chemical synthesis, and computer-aided catalyst design. The book also contains discussions on a variety of modern applications, including environmental pollution control, petroleum refining, fuel cells, and monomolecular films. Logically presented, well-illustrated, and thoroughly referenced, Catalysis: Principles and Applications offers an outstanding basis for courses in catalysis. It not only imparts the fundamentals, synthesis, characterization, and applications of catalysis, but does so in a way that will motivate students to pursue more advanced studies and ultimately careers in the field.

Catalysis

Author : John R. Anderson
Publisher : Springer Science & Business Media
ISBN 13 : 3642932479
Total Pages : 289 pages
Book Rating : 4.6/5 (429 download)

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Book Synopsis Catalysis by : John R. Anderson

Download or read book Catalysis written by John R. Anderson and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 289 pages. Available in PDF, EPUB and Kindle. Book excerpt: Catalytic steam reforming has grown during the last two or three decades into one of the world's great catalytic processes. It is of major economic significance since the products from it form the feed for a number of other major processes. Nevertheless, catalytic steam reforming is a relatively difficult technology. It operates at high temperatures where problems of the maintenance of materials integrity and of catalyst stability and activity are severe, the establishment of high thermal efficiency of the plant is economically vital, and reactor operation is strongly influenced by mass and heat transport effects. The process is the subject of a thorough review by Dr. J. R. Rostrup-Nielsen who discusses both the basic cataly tic chemistry and the way in which this is interrelated with reactor and plant design. The use of catalytic converters for the purification of automotive exhaust gases is a relatively new technology which was brought into existence by social pressures for the preservation of acceptable environmental conditions. The majority of catalytic practitioners have been able to watch the growth of this technology from its inception to its current state of sophistication. Automotive catalytic converter technology is now in a mature state, and the chapter in this volume by Dr. K. C. Taylor provides a review which covers both the process chemistry and the most important converter design factors.

Fundamental Concepts in Heterogeneous Catalysis

Author : Jens K. Nørskov
Publisher : John Wiley & Sons
ISBN 13 : 1118888952
Total Pages : 228 pages
Book Rating : 4.1/5 (188 download)

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Book Synopsis Fundamental Concepts in Heterogeneous Catalysis by : Jens K. Nørskov

Download or read book Fundamental Concepts in Heterogeneous Catalysis written by Jens K. Nørskov and published by John Wiley & Sons. This book was released on 2014-10-27 with total page 228 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is based on a graduate course and suitable as a primer for any newcomer to the field, this book is a detailed introduction to the experimental and computational methods that are used to study how solid surfaces act as catalysts. Features include: First comprehensive description of modern theory of heterogeneous catalysis Basis for understanding and designing experiments in the field Allows reader to understand catalyst design principles Introduction to important elements of energy transformation technology Test driven at Stanford University over several semesters

Calorimetry and Thermal Methods in Catalysis

Author : Aline Auroux
Publisher : Springer Science & Business Media
ISBN 13 : 3642119549
Total Pages : 569 pages
Book Rating : 4.6/5 (421 download)

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Book Synopsis Calorimetry and Thermal Methods in Catalysis by : Aline Auroux

Download or read book Calorimetry and Thermal Methods in Catalysis written by Aline Auroux and published by Springer Science & Business Media. This book was released on 2013-09-18 with total page 569 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book is about calorimetry and thermal analysis methods, alone or linked to other techniques, as applied to the characterization of catalysts, supports and adsorbents, and to the study of catalytic reactions in various domains: air and wastewater treatment, clean and renewable energies, refining of hydrocarbons, green chemistry, hydrogen production and storage. The book is intended to fill the gap between the basic thermodynamic and kinetics concepts acquired by students during their academic formation, and the use of experimental techniques such as thermal analysis and calorimetry to answer practical questions. Moreover, it supplies insights into the various thermal and calorimetric methods which can be employed in studies aimed at characterizing the physico-chemical properties of solid adsorbents, supports and catalysts, and the processes related to the adsorption desorption phenomena of the reactants and/or products of catalytic reactions. The book also covers the basic concepts for physico-chemical comprehension of the relevant phenomena. Thermodynamic and kinetic aspects of the catalytic reactions can be fruitfully investigated by means of thermal analysis and calorimetric methods, in order to better understand the sequence of the elemental steps in the catalysed reaction. So the fundamental theory behind the various thermal analysis and calorimetric techniques and methods also are illustrated.

Catalysis

Author : C Kemball
Publisher : Royal Society of Chemistry
ISBN 13 : 1847553168
Total Pages : 270 pages
Book Rating : 4.8/5 (475 download)

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Book Synopsis Catalysis by : C Kemball

Download or read book Catalysis written by C Kemball and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 270 pages. Available in PDF, EPUB and Kindle. Book excerpt: There is an increasing challenge for chemical industry and research institutions to find cost-efficient and environmentally sound methods of converting natural resources into fuels chemicals and energy. Catalysts are essential to these processes and the Catalysis Specialist Periodical Report series serves to highlight major developments in this area. This series provides systematic and detailed reviews of topics of interest to scientists and engineers in the catalysis field. The coverage includes all major areas of heterogeneous and homogeneous catalysis and also specific applications of catalysis such as NOx control kinetics and experimental techniques such as microcalorimetry. Each chapter is compiled by recognised experts within their specialist fields and provides a summary of the current literature. This series will be of interest to all those in academia and industry who need an up-to-date critical analysis and summary of catalysis research and applications. Catalysis will be of interest to anyone working in academia and industry that needs an up-to-date critical analysis and summary of catalysis research and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr

Chemical Reaction and Reactor Engineering

Author : James John Carberry
Publisher : CRC Press
ISBN 13 : 1000146766
Total Pages : 1086 pages
Book Rating : 4.0/5 (1 download)

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Book Synopsis Chemical Reaction and Reactor Engineering by : James John Carberry

Download or read book Chemical Reaction and Reactor Engineering written by James John Carberry and published by CRC Press. This book was released on 2020-08-27 with total page 1086 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents an authoritative progress report that will remain germane to the topic and prove to be a substantial inspiration to further progress. It is valuable to academic and industrial practitioners of the art and science of chemical reaction and reactor engineering.