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Development Of A Methodology To Detect Pharmaceutical Compounds In Water Using Solid Phase Extraction Spe And Gas Chromatography Mass Spectrometry Gc Ms
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Book Synopsis Development of a Methodology to Detect Pharmaceutical Compounds in Water Using Solid Phase Extraction (SPE) and Gas Chromatography-Mass Spectrometry (GC/MS) by : Jennifer Ann Quiñones González
Download or read book Development of a Methodology to Detect Pharmaceutical Compounds in Water Using Solid Phase Extraction (SPE) and Gas Chromatography-Mass Spectrometry (GC/MS) written by Jennifer Ann Quiñones González and published by . This book was released on 2011 with total page 242 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Practical HPLC Method Development by : Lloyd R. Snyder
Download or read book Practical HPLC Method Development written by Lloyd R. Snyder and published by John Wiley & Sons. This book was released on 2012-12-03 with total page 665 pages. Available in PDF, EPUB and Kindle. Book excerpt: This revision brings the reader completely up to date on the evolving methods associated with increasingly more complex sample types analyzed using high-performance liquid chromatography, or HPLC. The book also incorporates updated discussions of many of the fundamental components of HPLC systems and practical issues associated with the use of this analytical method. This edition includes new or expanded treatments of sample preparation, computer assisted method development, as well as biochemical samples, and chiral separations.
Book Synopsis Analytical Methods for the Determination of Pollutants in Pharmaceutical Manufacturing Industry Wastewater by :
Download or read book Analytical Methods for the Determination of Pollutants in Pharmaceutical Manufacturing Industry Wastewater written by and published by . This book was released on 1995 with total page 140 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Bioanalysis of Pharmaceuticals by : Steen Honoré Hansen
Download or read book Bioanalysis of Pharmaceuticals written by Steen Honoré Hansen and published by John Wiley & Sons. This book was released on 2015-07-20 with total page 332 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bioanalysis of Pharmaceuticals: Sample Preparation, Separation Techniques and Mass Spectrometry is the first student textbook on the separation science and mass spectrometry of pharmaceuticals present in biological fluids with an educational presentation of the principles, concepts and applications. It discusses the chemical structures and properties of low- and high-molecular drug substances; the different types of biological samples and fluids that are used; how to prepare the samples by extraction, and how to perform the appropriate analytical measurements by chromatographic and mass spectrometric methods. Bioanalysis of Pharmaceuticals: Sample Preparation, Separation Techniques and Mass Spectrometry: Is an introductory student textbook discussing the different principles and concepts clearly and comprehensively, with many relevant and educational examples Focuses on substances that are administered as human drugs, including low-molecular drug substances, peptides, and proteins Presents both the basic principles that are regularly taught in universities, along with the practical use of bioanalysis as carried out by researchers in the pharmaceutical industry and in hospital laboratories Is aimed at undergraduate students, scientists, technicians and researchers in industry working in the areas of pharmaceutical analyses, biopharmaceutical analyses, biological and life sciences The book includes multiple examples to illustrate the theory and application, with many practical aspects including calculations, thus helping the student to learn how to convert the data recorded by instruments into the real concentration of the drug substances within the biological sample.
Book Synopsis Chromatographic Analysis of the Environment by : Leo M.L. Nollet
Download or read book Chromatographic Analysis of the Environment written by Leo M.L. Nollet and published by CRC Press. This book was released on 2017-03-03 with total page 618 pages. Available in PDF, EPUB and Kindle. Book excerpt: This detailed handbook covers different chromatographic analysis techniques and chromatographic data for compounds found in air, water, and soil, and sludge. The new edition outlines developments relevant to environmental analysis, especially when using chromatographic mass spectrometric techniques. It addresses new issues, new lines of discussion, and new findings, and develops in greater detail the aspects related to chromatographic analysis in the environment. It also includes different analytical methodologies, addresses instrumental aspects, and outlines conclusions and perspectives for the future.
Book Synopsis Investigation of Occurrence, Elimination and Degradation of Pharmaceutical and Personal Care Products in Drinking Water Using Liquid Chromatography-tandem Mass Spectrometry by : Chuan Wang
Download or read book Investigation of Occurrence, Elimination and Degradation of Pharmaceutical and Personal Care Products in Drinking Water Using Liquid Chromatography-tandem Mass Spectrometry written by Chuan Wang and published by . This book was released on 2011 with total page 192 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Pharmaceutical and personal care products have benefited humans and animals around the world. However, their presence in natural and treated water system as emerging contaminates may have potentially adverse effects on the aquatic environment and cause development of bacterial resistance. In this research project, a comprehensive liquid chromatography tandem mass spectrometry method has been developed and validated for the analysis of sixteen pharmaceutical compounds using solid phase extraction. Treated and untreated water samples collected across Missouri from water treatment facilities were analyzed to access the distribution of sixteen pharmaceutical compounds in both winter and summer seasons. The results of the occurrence study indicated that these pharmaceutical compounds in different types of water resources were usually below 80 ng/L, except caffeine. It was also found that the treatment processes in water facilities were effective to remove pharmaceutical compounds in most cases. The study of pharmaceutical elimination is still crucial in providing information for the disinfection strategy in water treatment facilities. The follow-up study was performed to investigate both the treatability and elimination of eight detected pharmaceuticals in the occurrence study as a function of treatment approach, types of disinfections (free chlorine, monochloramine, ozone and permanganate ), and treatment conditions (e.g., pH, contact time, etc). The results indicated that the degradation levels of pharmaceutical compounds varied significantly in different oxidation processes. Chlorination at 1 mg/L was found to be highly effective in the elimination of the selected pharmaceuticals. The pH conditions also played an important role in pharmaceutical removal, and its effect was conditional based on the oxidation system and pharmaceutical involved"--Abstract, leaf iv.
Book Synopsis Tools, Techniques and Protocols for Monitoring Environmental Contaminants by : Satinder Kaur Brar
Download or read book Tools, Techniques and Protocols for Monitoring Environmental Contaminants written by Satinder Kaur Brar and published by Elsevier. This book was released on 2019-09-15 with total page 432 pages. Available in PDF, EPUB and Kindle. Book excerpt: Tools, Techniques and Protocols for Monitoring Environmental Contaminants describes information on the strategic integration of available monitoring methods with molecular techniques, with a focus on omics (DNA, RNA and protein based) and molecular imprinted polymer and nanomaterial based advanced biosensors for environmental applications. It discusses the most commonly practiced analytic techniques, such as HPLC, MS, GCMS and traditional biosensors, giving an overview of the benefits of advanced biosensors over commonly practiced methods in the rapid and reliable assessment of environmental contaminants. As environmental contaminants have become one of the serious concerns in terms of their rapid growth and monitoring in the environment, which is often limited due to costly and laborious methods, this book provides a comprehensive update on their removal, the challenges they create for environmental regulatory agencies, and their diverse effects on terrestrial and aquatic environments. Provides methods for assessing and monitoring environmental contaminants Includes recent advancement in molecular techniques Outlines rapid environmental monitoring methods Explains the use of biosensors for environmental monitoring Reviews monitoring methods beyond conventional analytic techniques
Book Synopsis Fate of Pharmaceuticals in the Environment and in Water Treatment Systems by : Diana S. Aga
Download or read book Fate of Pharmaceuticals in the Environment and in Water Treatment Systems written by Diana S. Aga and published by CRC Press. This book was released on 2007-12-26 with total page 408 pages. Available in PDF, EPUB and Kindle. Book excerpt: The detection of pharmaceutical residues remained elusive until instruments such as liquid chromatography and mass spectrometry became commonplace in environmental laboratories. The documentation of the occurrence of pharmaceutical residues and endocrine disrupting chemicals in water resources has raused questions about their long-term effects
Book Synopsis Handbook of LC-MS Bioanalysis by : Wenkui Li
Download or read book Handbook of LC-MS Bioanalysis written by Wenkui Li and published by John Wiley & Sons. This book was released on 2013-10-21 with total page 709 pages. Available in PDF, EPUB and Kindle. Book excerpt: Consolidates the information LC-MS bioanalytical scientists need to analyze small molecules and macromolecules The field of bioanalysis has advanced rapidly, propelled by new approaches for developing bioanalytical methods, new liquid chromatographic (LC) techniques, and new mass spectrometric (MS) instruments. Moreover, there are a host of guidelines and regulations designed to ensure the quality of bioanalytical results. Presenting the best practices, experimental protocols, and the latest understanding of regulations, this book offers a comprehensive review of LC-MS bioanalysis of small molecules and macromolecules. It not only addresses the needs of bioanalytical scientists working on routine projects, but also explores advanced and emerging technologies such as high-resolution mass spectrometry and dried blood spot microsampling. Handbook of LC-MS Bioanalysis features contributions from an international team of leading bioanalytical scientists. Their contributions reflect a review of the latest findings, practices, and regulations as well as their own firsthand analytical laboratory experience. The book thoroughly examines: Fundamentals of LC-MS bioanalysis in drug discovery, drug development, and therapeutic drug monitoring The current understanding of regulations governing LC-MS bioanalysis Best practices and detailed technical instructions for LC-MS bioanalysis method development, validation, and stability assessment of analyte(s) of interest Experimental guidelines and protocols for quantitative LC-MS bioanalysis of challenging molecules, including pro-drugs, acyl glucuronides, N-oxides, reactive compounds, and photosensitive and autooxidative compounds With its focus on current bioanalytical practice, Handbook of LC-MS Bioanalysis enables bioanalytical scientists to develop and validate robust LC-MS assay methods, all in compliance with current regulations and standards.
Book Synopsis Toxicology of Organophosphate and Carbamate Compounds by : Ramesh C Gupta
Download or read book Toxicology of Organophosphate and Carbamate Compounds written by Ramesh C Gupta and published by Academic Press. This book was released on 2011-04-28 with total page 781 pages. Available in PDF, EPUB and Kindle. Book excerpt: This text/reference book provides the most comprehensive coverage of anticholinesterase compounds (Organophosphates and Carbamates), which constitute the largest number of chemicals that are primarily used as insecticides in agriculture, industry, and around the home/garden. Some OPs (nerve agents) have been used in chemical warfare and terrorist attacks, while some OPs and CMs have been recommended as therapeutic agents in human medicine as well as in veterinary medicine. Many chemicals of both classes are extremely toxic and lack selectivity, thus their inadvertent/accidental use continues to pose a threat to human and animal health, aquatic systems and wildlife. These anticholinesterase agents produce a variety of toxicological effects in target and nontarget organs. In light of this complexicity, this multi-authored book is written by the well known scientists from many countries. The book is organized into nine sections, with a total of 49 chapters, to provide in-depth knowledge on various aspects of OP and CM compounds, including their use, classification, mechanism-based toxicity, and prophylactic and therapeutic measurements. Several chapters are written with special emphasis to cover timely topics, such as chemical warfare agents, physiologically-based pharmacokinetic modeling, structure and function of cholinesterases, paraoxonase, carboxylesterases; developmental neurotoxicity, the intermediate syndrome, oxidative stress, endocrine disruption, and DNA damage/gene expression and carcinogenesis. Section-VI with 5 chapters is specifically devoted to risk assessment, and safety and regulatory guidelines for pesticides. - Describes everything you need to know about Organophosphates and Carbamates - Extensively covers pesticides, nerve agents, therapeutic drugs, and flame retardants - Describes epidemiology of the world's major disasters involving Organophosphates and Carbamates - Covers animal, human, aquatic, and wildlife toxicity of Anticholinesterases - Insights into in-depth cholinergic and noncholinergic mechanisms of toxicity - Describes recent advancements in cholinesterases, paraoxonases, carboxylesterases, oxidative stress, endocrine disruption, cardiac and pulmonary toxicity, and carcinogenesis - Provides in vitro and in vivo models for neurotoxicity testing - Integrates knowledge of studies in lab animals and humans - Offers risk/safety assessment and national/international guidelines for permissible levels of pesticide residues - Describes management of Anticholinesterase poisoning in humans
Book Synopsis Practical Guidelines for the Analysis of Seawater by : Oliver Wurl
Download or read book Practical Guidelines for the Analysis of Seawater written by Oliver Wurl and published by CRC Press. This book was released on 2009-06-09 with total page 404 pages. Available in PDF, EPUB and Kindle. Book excerpt: As we discover more about the role of the ocean in global changes and identify the effects of global change on the ocean, understanding its chemical composition and processes becomes increasingly paramount. However, understanding these processes requires a wide range of measurements in the vast ocean, from the sea surface to deep-ocean trenches, fr
Book Synopsis Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites by : Despina Tsipi
Download or read book Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites written by Despina Tsipi and published by John Wiley & Sons. This book was released on 2015-04-27 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides an overview of the use of mass spectrometry (MS) for the analysis of pesticide residues and their metabolites. Presents state of the-art MS techniques for the identification of pesticides and their transformation products in food and environment Covers important advances in MS techniques including MS instrumentation and chromatographic separations (e.g. UPLC, HILIC, comprehensive GCxGC) and applications Illustrates the main sample preparation techniques (SPE, QuEChERS, microextraction) used in combination with MS for the analysis of pesticides Describes various established and new ionization techniques as well as the main MS platforms, software tools and mass spectral libraries
Download or read book Method 529 written by J. W. Munch and published by . This book was released on 2002 with total page 60 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Determination of Organic Compounds in Drinking Water by Liquid-solid Extraction and Capillary Column Gas Chromatography/mass Spectrometry by :
Download or read book Determination of Organic Compounds in Drinking Water by Liquid-solid Extraction and Capillary Column Gas Chromatography/mass Spectrometry written by and published by . This book was released on 1988 with total page 76 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Analysis of Endocrine Disrupting Compounds in Food by : Leo M. L. Nollet
Download or read book Analysis of Endocrine Disrupting Compounds in Food written by Leo M. L. Nollet and published by John Wiley & Sons. This book was released on 2011-06-09 with total page 506 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analysis of Endocrine Disrupting Compounds in Food provides a unique and comprehensive professional reference source covering most of the recent analytical methodology of endocrine disrupting compounds in food. Editor Nollet and his broad team of international contributors address the most recent advances in analysis of endocrine disrupting chemicals in food. While covering conventional (typically lab-based) methods of analysis, the book focuses on leading-edge technologies that recently have been introduced. The book looks at areas such as food quality assurance and safety. Issues such as persistent organic pollutants, monitoring pesticide and herbicide residues in food, determining heavy and other metals in food and discussing the impacts of dioxins, PCBs, PCDFs and many other suspected chemicals are covered. The book discusses the relationship between chemical compounds and hormone activity. What are the health impacts of different chemical compounds for men and animals? How are these compounds entering in foodstuffs? Analysis of Endocrine Disrupting Compounds in Food offers the food professional what its title promises – a compendium of sample preparation and analysis techniques of possible endocrine disrupting compounds in food. Special Features: Uniquely concentrates on analysis and detection methods of EDCs in foodstuffs Extensive coverage of the main types of globally available analytical techniques and methodologies Fully detailed properties, sample procedures, and analysis steps for each EDC Renowned editor Leo Nollet leads a broad team of international experts
Book Synopsis Analysis of Pesticides in Food and Environmental Samples, Second Edition by : Jose L. Tadeo
Download or read book Analysis of Pesticides in Food and Environmental Samples, Second Edition written by Jose L. Tadeo and published by CRC Press. This book was released on 2019-03-04 with total page 423 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a critical overview of analytical methods used for the determination of pesticide residues and other contaminants in food and environmental samples by modern instrumental analysis. It contains up-to-date material including recent trends in sample preparation, general methods used for pesticide analysis and quality assurance aspects, and chromatographic and immunoassay methods. The rest of the book describes particular analytical methods used for the determination of pesticides in food and soil, water and air. In addition, the levels of these chemicals found in food, their regulatory aspects and the monitoring of pesticides in the environment are described.
Book Synopsis Handbook of Solid Phase Microextraction by : Janusz Pawliszyn
Download or read book Handbook of Solid Phase Microextraction written by Janusz Pawliszyn and published by Elsevier. This book was released on 2011-12-01 with total page 497 pages. Available in PDF, EPUB and Kindle. Book excerpt: The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. - Practical application of Solid Phase Microextraction methods including detailed steps - Provides history of extraction methods to better understand the process - Suitable for all levels, from beginning student to experienced practitioner