Water Determination By Karl Fischer Titration

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Karl Fischer Titration

Author : Eugen Scholz
Publisher : Springer Science & Business Media
ISBN 13 : 3642699898
Total Pages : 142 pages
Book Rating : 4.6/5 (426 download)

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Book Synopsis Karl Fischer Titration by : Eugen Scholz

Download or read book Karl Fischer Titration written by Eugen Scholz and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 142 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Karl Fischer titration is used in many different ways following its publication in 1935 and further applications are continually being explored. At the present time we are experiencing another phase of expansion, as shown by the development of new titration equipment and new reagents. KF equipment increasingly incorporates microprocessors which enable the course of a titration to be programmed thus sim plifying the titration. Coulometric titrators allow water determinations in the micro gram-range: the KF titration has become a micro-method. The new pyridine-free re agents make its application significantly more pleasant and open up further possibili ties on account of their accuracy. To make the approach to Karl Fischer titrations easier, we have summarized the present knowledge in this monograph and we have complemented it with our own studies and practical experience. As this book should remain "readable", we have tried to keep the fundamentals to a minimum. Historical developments are only mentioned if they seem to be necessary for understanding the KF reaction. The ap plications are described more fully. Specific details which may interest a particular reader can be found in the original publications cited. The referenced literature is in chronological order as the year of publication may also prove informative. Thus, [6902] for example denotes 69 for 1969 being the year of publication and 02 is a non-recurring progressive number. The referenced litera ture includes summaries which we hope will be of help to find the "right" publica tion easily.

Water Determination by Karl Fischer Titration

Author : G. Wieland
Publisher :
ISBN 13 :
Total Pages : 114 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Water Determination by Karl Fischer Titration by : G. Wieland

Download or read book Water Determination by Karl Fischer Titration written by G. Wieland and published by . This book was released on 1987 with total page 114 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Development and Validation of Analytical Methods

Author : Christopher M. Riley
Publisher : Elsevier
ISBN 13 : 0080530354
Total Pages : 363 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Development and Validation of Analytical Methods by : Christopher M. Riley

Download or read book Development and Validation of Analytical Methods written by Christopher M. Riley and published by Elsevier. This book was released on 1996-05-29 with total page 363 pages. Available in PDF, EPUB and Kindle. Book excerpt: The need to validate an analytical or bioanalytical method is encountered by analysts in the pharmaceutical industry on an almost daily basis, because adequately validated methods are a necessity for approvable regulatory filings. What constitutes a validated method, however, is subject to analyst interpretation because there is no universally accepted industry practice for assay validation. This book is intended to serve as a guide to the analyst in terms of the issues and parameters that must be considered in the development and validation of analytical methods. In addition to the critical issues surrounding method validation, this book also deals with other related factors such as method development, data acquisition, automation, cleaning validation and regulatory considerations. The book is divided into three parts. Part One, comprising two chapters, looks at some of the basic concepts of method validation. Chapter 1 discusses the general concept of validation and its role in the process of transferring methods from laboratory to laboratory. Chapter 2 looks at some of the critical parameters included in a validation program and the various statistical treatments given to these parameters. Part Two (Chapters 3, 4 and 5) of the book focuses on the regulatory perspective of analytical validation. Chapter 3 discusses in some detail how validation is treated by various regulatory agencies around the world, including the United States, Canada, the European Community, Australia and Japan. This chapter also discusses the International Conference on Harmonization (ICH) treatment of assay validation. Chapters 4 and 5 cover the issues and various perspectives of the recent United States vs. Barr Laboratories Inc. case involving the retesting of samples. Part Three (Chapters 6 - 12) covers the development and validation of various analytical components of the pharmaceutical product development process. This part of the book contains specific chapters dedicated to bulk drug substances and finished products, dissolution studies, robotics and automated workstations, biotechnology products, biological samples, analytical methods for cleaning procedures and computer systems and computer-aided validation. Each chapter goes into some detail describing the critical development and related validation considerations for each topic. This book is not intended to be a practical description of the analytical validation process, but more of a guide to the critical parameters and considerations that must be attended to in a pharmaceutical development program. Despite the existence of numerous guidelines including the recent attempts by the ICH to be implemented in 1998, the practical part of assay validation will always remain, to a certain extent, a matter of the personal preference of the analyst or company. Nevertheless, this book brings together the perspectives of several experts having extensive experience in different capacities in the pharmaceutical industry in an attempt to bring some consistency to analytical method development and validation.

Determination of Water: Coulometric Karl Fischer Titration Method: NBN EN ISO 12937

Author : Belgisch Instituut voor Normalisatie
Publisher :
ISBN 13 :
Total Pages : 12 pages
Book Rating : 4.:/5 (92 download)

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Book Synopsis Determination of Water: Coulometric Karl Fischer Titration Method: NBN EN ISO 12937 by : Belgisch Instituut voor Normalisatie

Download or read book Determination of Water: Coulometric Karl Fischer Titration Method: NBN EN ISO 12937 written by Belgisch Instituut voor Normalisatie and published by . This book was released on 2001 with total page 12 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Food Analysis

Author : Y. Pomeranz
Publisher : Springer Science & Business Media
ISBN 13 : 1461569982
Total Pages : 788 pages
Book Rating : 4.4/5 (615 download)

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Book Synopsis Food Analysis by : Y. Pomeranz

Download or read book Food Analysis written by Y. Pomeranz and published by Springer Science & Business Media. This book was released on 2013-12-01 with total page 788 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first edition of Food Analysis: Theory and Practice was published in 1971 and was revised in 1978. The second edition was published in 1987, and in 1993 we found it necessary to prepare a third edition to reflect and cover the most recent advances in the field of food analysis. A complete revision of a book is an arduous and anguished task. The following are challenges that we wanted to address in this revision: to update the material without eliminating classic and time-preserved and honored methods used by the food analyst; to broaden and deepen the coverage and scope without increasing the size of the book; and to produce a textbook (for senior undergraduate and graduate students) with regard to objectives, scope, and outlay while providing a reference and resource for the worker and researcher in the field of food analysis. To meet those challenges we added much new material and took out practically the same amount of "rel atively outdated" material. Every chapter has been extensively updated and revised; many of the pictures in the previous editions were deleted and, whenever available and appropriate, were replaced by diagrams or flow sheets. In Part I we have expanded the seetions on sampling, preparation of sam pIes, reporting results, and reliability of analyses.

Karl Fischer Titration

Author : Eugen Scholz
Publisher :
ISBN 13 : 9783642699900
Total Pages : 152 pages
Book Rating : 4.6/5 (999 download)

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Book Synopsis Karl Fischer Titration by : Eugen Scholz

Download or read book Karl Fischer Titration written by Eugen Scholz and published by . This book was released on 1984-11-01 with total page 152 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Food Analysis Laboratory Manual

Author : S. Suzanne Nielsen
Publisher : Springer Science & Business Media
ISBN 13 : 1441914633
Total Pages : 150 pages
Book Rating : 4.4/5 (419 download)

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Book Synopsis Food Analysis Laboratory Manual by : S. Suzanne Nielsen

Download or read book Food Analysis Laboratory Manual written by S. Suzanne Nielsen and published by Springer Science & Business Media. This book was released on 2010-03-20 with total page 150 pages. Available in PDF, EPUB and Kindle. Book excerpt: This second edition laboratory manual was written to accompany Food Analysis, Fourth Edition, ISBN 978-1-4419-1477-4, by the same author. The 21 laboratory exercises in the manual cover 20 of the 32 chapters in the textbook. Many of the laboratory exercises have multiple sections to cover several methods of analysis for a particular food component of characteristic. Most of the laboratory exercises include the following: introduction, reading assignment, objective, principle of method, chemicals, reagents, precautions and waste disposal, supplies, equipment, procedure, data and calculations, questions, and references. This laboratory manual is ideal for the laboratory portion of undergraduate courses in food analysis.

The Determination of Water by Coulometric Titration

Author : A. S. Meyer
Publisher :
ISBN 13 :
Total Pages : 52 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis The Determination of Water by Coulometric Titration by : A. S. Meyer

Download or read book The Determination of Water by Coulometric Titration written by A. S. Meyer and published by . This book was released on 1955 with total page 52 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Handbook of Processed Meats and Poultry Analysis

Author : Leo M.L. Nollet
Publisher : CRC Press
ISBN 13 : 1420045334
Total Pages : 782 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Handbook of Processed Meats and Poultry Analysis by : Leo M.L. Nollet

Download or read book Handbook of Processed Meats and Poultry Analysis written by Leo M.L. Nollet and published by CRC Press. This book was released on 2008-11-12 with total page 782 pages. Available in PDF, EPUB and Kindle. Book excerpt: Muscle foods include a wide range of processed meats and poultry, and therefore represent an important percentage of total worldwide food consumption. The sheer volume of products and the variety of processes available makes analyzing them problematic. Co-Edited by Fidel Toldra - Recipient of the 2010 Distinguished Research Award from the American

Introduction to Food Chemistry

Author : Vassilis Kontogiorgos
Publisher : Springer Nature
ISBN 13 : 3031535588
Total Pages : 175 pages
Book Rating : 4.0/5 (315 download)

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Book Synopsis Introduction to Food Chemistry by : Vassilis Kontogiorgos

Download or read book Introduction to Food Chemistry written by Vassilis Kontogiorgos and published by Springer Nature. This book was released on with total page 175 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Determination of Water in Phenols by Means of Karl Fischer Titration

Author : E. Scholz
Publisher :
ISBN 13 :
Total Pages : 13 pages
Book Rating : 4.:/5 ( download)

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Book Synopsis Determination of Water in Phenols by Means of Karl Fischer Titration by : E. Scholz

Download or read book Determination of Water in Phenols by Means of Karl Fischer Titration written by E. Scholz and published by . This book was released on 1988 with total page 13 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Traceability, Validation and Measurement Uncertainty in Chemistry: Vol. 3

Author : Nineta Hrastelj
Publisher : Springer
ISBN 13 : 3030203476
Total Pages : 129 pages
Book Rating : 4.0/5 (32 download)

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Book Synopsis Traceability, Validation and Measurement Uncertainty in Chemistry: Vol. 3 by : Nineta Hrastelj

Download or read book Traceability, Validation and Measurement Uncertainty in Chemistry: Vol. 3 written by Nineta Hrastelj and published by Springer. This book was released on 2019-08-13 with total page 129 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents worked examples of five analytical procedures. These practical examples address traceability, validation and measurement uncertainty aspects in a systematic and consistent way, and cover applications in the analysis of water, food, as well as ores and minerals. This concept is based on the experiences of the TrainMiCc program, in which more than 9000 laboratory professionals all over Europe have participated.

A Practical Guide to Instrumental Analysis

Author : Erno Pungor
Publisher : CRC Press
ISBN 13 : 1000142442
Total Pages : 404 pages
Book Rating : 4.0/5 (1 download)

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Book Synopsis A Practical Guide to Instrumental Analysis by : Erno Pungor

Download or read book A Practical Guide to Instrumental Analysis written by Erno Pungor and published by CRC Press. This book was released on 2020-11-25 with total page 404 pages. Available in PDF, EPUB and Kindle. Book excerpt: A Practical Guide to Instrumental Analysis covers basic methods of instrumental analysis, including electroanalytical techniques, optical techniques, atomic spectroscopy, X-ray diffraction, thermoanalytical techniques, separation techniques, and flow analytical techniques. Each chapter provides a brief theoretical introduction followed by basic and special application experiments. This book is ideal for readers who need a knowledge of special techniques in order to use instrumental methods to conduct their own analytical tasks.

WATER DETERMINATION IN TERPHENYLS USING THE KARL FISCHER COULOMETRIC TITRATION.

Author :
Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (111 download)

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Book Synopsis WATER DETERMINATION IN TERPHENYLS USING THE KARL FISCHER COULOMETRIC TITRATION. by :

Download or read book WATER DETERMINATION IN TERPHENYLS USING THE KARL FISCHER COULOMETRIC TITRATION. written by and published by . This book was released on 1964 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Aquametry

Author : John Mitchell
Publisher :
ISBN 13 :
Total Pages : 464 pages
Book Rating : 4.:/5 (34 download)

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Book Synopsis Aquametry by : John Mitchell

Download or read book Aquametry written by John Mitchell and published by . This book was released on 1948 with total page 464 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Methods of Seawater Analysis

Author : Klaus Grasshoff
Publisher : John Wiley & Sons
ISBN 13 : 3527613994
Total Pages : 632 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Methods of Seawater Analysis by : Klaus Grasshoff

Download or read book Methods of Seawater Analysis written by Klaus Grasshoff and published by John Wiley & Sons. This book was released on 2009-07-30 with total page 632 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the book first appeared in 1976, Methods of Seawater Analysis has found widespread acceptance as a reliable and detailed source of information. Its second extended and revised edition published in 1983 reflected the rapid pace of instrumental and methodological evolution in the preceding years. The development has lost nothing of its momentum, and many methods and procedures still suffering their teething troubles then have now matured into dependable tools for the analyst. This is especially evident for trace and ultra-trace analyses of organic and inorganic seawater constituents which have diversified considerably and now require more space for their description than before. Methods to determine volatile halocarbons, dimethyl sulphide, photosynthetic pigments and natural radioactive tracers have been added as well as applications of X-ray fluorescence spectroscopy and various electrochemical methods for trace metal analysis. Another method not previously described deals with the determination of the partial pressure of carbon dioxide as part of standardised procedures to describe the marine CO2 system.

Confectionery Science and Technology

Author : Richard W. Hartel
Publisher : Springer
ISBN 13 : 3319617427
Total Pages : 542 pages
Book Rating : 4.3/5 (196 download)

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Book Synopsis Confectionery Science and Technology by : Richard W. Hartel

Download or read book Confectionery Science and Technology written by Richard W. Hartel and published by Springer. This book was released on 2017-10-09 with total page 542 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book examines both the primary ingredients and the processing technology for making candies. In the first section, the chemistry, structure, and physical properties of the primary ingredients are described, as are the characteristics of commercial ingredients. The second section explores the processing steps for each of the major sugar confectionery groups, while the third section covers chocolate and coatings. The manner in which ingredients function together to provide the desired texture and sensory properties of the product is analyzed, and chemical reactions and physical changes that occur during processing are examined. Trouble shooting and common problems are also discussed in each section. Designed as a complete reference and guide, Confectionery Science and Technology provides personnel in industry with solutions to the problems concerning the manufacture of high-quality confectionery products.