Thermal Methods of Polymer Analysis

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Author :
Publisher : Smithers Rapra
ISBN 13 : 184735663X
Total Pages : 256 pages
Book Rating : 4.8/5 (473 download)

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Book Synopsis Thermal Methods of Polymer Analysis by : T.R Crompton

Download or read book Thermal Methods of Polymer Analysis written by T.R Crompton and published by Smithers Rapra. This book was released on 2013-01-29 with total page 256 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book reviews the various thermal methods used for the characterisation of polymer properties and composition. All these methods study the properties of polymers as they change with temperature. The methods discussed in this book are: differential photocalorimetry, differential scanning calorimetry, dielectric thermal analysis, differential thermal analysis, dynamic mechanical analysis, evolved gas analysis, gas chromatography, gas chromatography combined with mass spectrometry, mass spectrometry, microthermal analysis, thermal volatilisation, thermogravimetric analysis and thermomechanical analysis. Each technique is discussed in detail and examples of the use of each technique are also given. Each chapter has an extensive list of references so that the reader can follow up topics of interest. This book will be a useful reference for those who already use any of these thermal methods but will also be of interest to undergraduates and those who are just starting to use these techniques.

Thermal Analysis of Polymeric Materials

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Publisher : Springer Science & Business Media
ISBN 13 : 9783540236290
Total Pages : 918 pages
Book Rating : 4.2/5 (362 download)

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Book Synopsis Thermal Analysis of Polymeric Materials by : Bernhard Wunderlich

Download or read book Thermal Analysis of Polymeric Materials written by Bernhard Wunderlich and published by Springer Science & Business Media. This book was released on 2005-04-04 with total page 918 pages. Available in PDF, EPUB and Kindle. Book excerpt: Table of Contents Table of Contents 1 Atoms, small, and large molecules 2 Basics of thermal analysis 3 Dynamics of chemical and phase changes 4 Thermal analysis tools 5 Structure and properties of materials 6 Single component materials 7 Multiple component materials App. A.1 Table of thermal properties of linear macromolecules and related small molecules - the ATHAS data bank App. A.2 Radiation scattering App. A.3 Derivation of the Rayleigh ratio App. A.4 Neural network predictions App. A.5 Legendre transformations, Maxwell relations, linking of entropy and probability, and derivation of (dS/dT) App. A.6 Boltzmann distribution, harmonic vibration, complex numbers, and normal modes App. A.7 Summary of the basic kinetics of chemical reactions App. A.8 The ITS 1990 and the Krypton-86 length standard App. A.9 Development of classical DTA to DSC App. A.10 Examples of DTA and DSC under extreme conditions App. A.11 Description of an online correction of the heat-flow rate App. A.12 Derivation of the heat-flow equations App. A.13 Description of sawtooth-modulation response App. A.14 An introduction to group theory, definitions of configurations and conformations, and a summary of rational and irrational numbers App. A.15 Summary of birefringence and polarizing microscopy App. A.16 Summary of X-ray diffraction and interference effects App. A.17 Optical analog of electron double diffraction to produce Moire patterns.

Thermal Analysis of Polymers

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Publisher : John Wiley & Sons
ISBN 13 : 1118995996
Total Pages : 607 pages
Book Rating : 4.1/5 (189 download)

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Book Synopsis Thermal Analysis of Polymers by : Joseph D. Menczel

Download or read book Thermal Analysis of Polymers written by Joseph D. Menczel and published by John Wiley & Sons. This book was released on 2014-07-09 with total page 607 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.

Thermal Analysis of Polymers

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Publisher : iSmithers Rapra Publishing
ISBN 13 : 9781859571071
Total Pages : 130 pages
Book Rating : 4.5/5 (71 download)

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Book Synopsis Thermal Analysis of Polymers by : M. P. Sepe

Download or read book Thermal Analysis of Polymers written by M. P. Sepe and published by iSmithers Rapra Publishing. This book was released on 1997 with total page 130 pages. Available in PDF, EPUB and Kindle. Book excerpt: The techniques which are particularly relevant to polymer characterisation are evaluated in this new report. For each technique the author describes the method of operation and the output obtained, and then considers its application to polymer characterisation. An additional indexed section containing several hundred abstracts from the Rapra Polymer Library database provides useful references for further reading.

Polymer Characterization by Thermal Methods of Analysis

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Publisher :
ISBN 13 :
Total Pages : 272 pages
Book Rating : 4.:/5 (318 download)

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Book Synopsis Polymer Characterization by Thermal Methods of Analysis by : Jen Chiu

Download or read book Polymer Characterization by Thermal Methods of Analysis written by Jen Chiu and published by . This book was released on 1974 with total page 272 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Thermal Methods in Polymer Analysis

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Author :
Publisher : Lawrence Erlbaum Associates
ISBN 13 :
Total Pages : 216 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Thermal Methods in Polymer Analysis by : Shalaby W. Shalaby

Download or read book Thermal Methods in Polymer Analysis written by Shalaby W. Shalaby and published by Lawrence Erlbaum Associates. This book was released on 1978 with total page 216 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Polymer Characterization by Thermal Methods of Analysis

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Publisher :
ISBN 13 : 9780608159102
Total Pages : 254 pages
Book Rating : 4.1/5 (591 download)

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Book Synopsis Polymer Characterization by Thermal Methods of Analysis by : Jen Chiu

Download or read book Polymer Characterization by Thermal Methods of Analysis written by Jen Chiu and published by . This book was released on 1974 with total page 254 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Thermal Characterization of Polymeric Materials

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Publisher :
ISBN 13 : 9780127037837
Total Pages : pages
Book Rating : 4.0/5 (378 download)

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Book Synopsis Thermal Characterization of Polymeric Materials by : Edith A. Turi

Download or read book Thermal Characterization of Polymeric Materials written by Edith A. Turi and published by . This book was released on 1996 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Polymer characterization by thermal methods of analysis

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Author :
Publisher :
ISBN 13 :
Total Pages : 254 pages
Book Rating : 4.:/5 (252 download)

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Book Synopsis Polymer characterization by thermal methods of analysis by : Jen Chiu

Download or read book Polymer characterization by thermal methods of analysis written by Jen Chiu and published by . This book was released on 1974 with total page 254 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Thermal Methods of Analysis

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Author :
Publisher : Springer Science & Business Media
ISBN 13 : 9401113246
Total Pages : 297 pages
Book Rating : 4.4/5 (11 download)

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Book Synopsis Thermal Methods of Analysis by : P.J. Haines

Download or read book Thermal Methods of Analysis written by P.J. Haines and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 297 pages. Available in PDF, EPUB and Kindle. Book excerpt: The wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu tors by colleagues and instrument manufacturers is most gratefully ack nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC).

Thermal Characterization of Polymeric Materials

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Publisher : Elsevier
ISBN 13 : 0323141889
Total Pages : 987 pages
Book Rating : 4.3/5 (231 download)

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Book Synopsis Thermal Characterization of Polymeric Materials by : Edith Turi

Download or read book Thermal Characterization of Polymeric Materials written by Edith Turi and published by Elsevier. This book was released on 2012-12-02 with total page 987 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Characterization of Polymeric Materials is a critical review and a concise evaluation of the application of thermal analysis in polymer science and engineering. This book is divided into nine chapters that specifically tackle the instrumentation, theory, and a wide variety of applications of thermal characterization. The introductory chapters provide an overview of all aspects of thermal analytical methods and apparatus and the theory underlying the basic principles of thermal analysis. These chapters also examine the theories and functions of state for thermometry, dilatometry, thermomechanical analysis, calorimetry, thermogravimetry. These topics are followed by a discussion on single-component and multicomponent systems and their phase transitions, as influenced by concentration, pressure, deformation, molecular weight, and copolymerization. The subsequent chapters explore the influence of important chemical and physical parameters on the glass transition, crystallization, and melting of thermoplastic materials. The discussion then shifts to the theoretical aspects of polymer-polymer compatibility, phase separation, and miscibility in mixed polymer systems. This book further considers the thermal analysis in thermosets, elastomers, and fibers. The concluding chapters present the methods of obtaining information on the relative flammability properties of polymers, for screening fire retardant additives, and for studying the mechanism of flame inhibition. These chapters also look into the thermal analysis of antioxidants, stabilizers, lubricants, plasticizers, impact modifiers, and fire retardants. Polymer scientists and researchers will find this book invaluable.

Principles and Applications of Thermal Analysis

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Publisher : John Wiley & Sons
ISBN 13 : 0470698128
Total Pages : 480 pages
Book Rating : 4.4/5 (76 download)

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Book Synopsis Principles and Applications of Thermal Analysis by : Paul Gabbott

Download or read book Principles and Applications of Thermal Analysis written by Paul Gabbott and published by John Wiley & Sons. This book was released on 2008-04-30 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Analytical Methods for Polymer Characterization

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Publisher : CRC Press
ISBN 13 : 135121313X
Total Pages : 342 pages
Book Rating : 4.3/5 (512 download)

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Book Synopsis Analytical Methods for Polymer Characterization by : Rui Yang

Download or read book Analytical Methods for Polymer Characterization written by Rui Yang and published by CRC Press. This book was released on 2018-01-09 with total page 342 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Methods for Polymer Characterization presents a collection of methods for polymer analysis. Topics include chromatographic methods (gas chromatography, inverse gas chromatography, and pyrolysis gas chromatography), mass spectrometry, spectroscopic methods (ultraviolet-visible spectroscopy, infrared spectroscopy, Raman spectroscopy, and nuclear magnetic resonance), thermal analysis (differential scanning calorimetry and thermogravimetry), microscopy methods (scanning electron microscopy, transmission electron microscopy, and atomic force microscopy), and x-ray diffraction. The author also discusses mechanical and dynamic mechanical properties.

Hyphenated Techniques in Polymer Characterization

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Publisher :
ISBN 13 :
Total Pages : 208 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Hyphenated Techniques in Polymer Characterization by : Theodore Provder

Download or read book Hyphenated Techniques in Polymer Characterization written by Theodore Provder and published by . This book was released on 1994 with total page 208 pages. Available in PDF, EPUB and Kindle. Book excerpt: Covers significant advances in hyphenated techniques in polymer characterization. Presents coupled thermal techniques and couple-thermal-spectroscopic techniques, including STA-MS, STA-FTIR, TG/IR, GC/IR, TGA/IR, TB/FTIR, DSC/FTIR, and TGA/FTIR.

Introduction to Thermal Analysis

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Publisher : Springer Science & Business Media
ISBN 13 : 0306484048
Total Pages : 264 pages
Book Rating : 4.3/5 (64 download)

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Book Synopsis Introduction to Thermal Analysis by : M.E. Brown

Download or read book Introduction to Thermal Analysis written by M.E. Brown and published by Springer Science & Business Media. This book was released on 2006-04-11 with total page 264 pages. Available in PDF, EPUB and Kindle. Book excerpt: to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.

Modulated Temperature Differential Scanning Calorimetry

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Publisher : Springer Science & Business Media
ISBN 13 : 1402037503
Total Pages : 340 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Modulated Temperature Differential Scanning Calorimetry by : Mike Reading

Download or read book Modulated Temperature Differential Scanning Calorimetry written by Mike Reading and published by Springer Science & Business Media. This book was released on 2006-10-12 with total page 340 pages. Available in PDF, EPUB and Kindle. Book excerpt: MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.

Thermal Analysis of Polymeric Materials

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Publisher : Springer Science & Business Media
ISBN 13 : 3540263608
Total Pages : 894 pages
Book Rating : 4.5/5 (42 download)

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Book Synopsis Thermal Analysis of Polymeric Materials by : Bernhard Wunderlich

Download or read book Thermal Analysis of Polymeric Materials written by Bernhard Wunderlich and published by Springer Science & Business Media. This book was released on 2005-12-06 with total page 894 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal analysis is an old technique. It has been neglected to some degree because developments of convenient methods of measurement have been slow and teaching of the understanding of the basics of thermal analysis is often wanting. Flexible, linear macromolecules, also not as accurately simply called polymers, make up the final, third, class of molecules which only was identified in 1920. Polymers have neverbeenfullyintegratedintothedisciplinesofscienceandengineering. Thisbook is designed to teach thermal analysis and the understanding of all materials, flexible macromolecules, as well as those of the small molecules and rigid macromolecules. The macroscopic tool of inquiry is thermal analysis, and the results are linked to microscopic molecular structure and motion. Measurements of heat and mass are the two roots of quantitative science. The macroscopic heat is connected to the microscopic atomic motion, while the macroscopic mass is linked to the microscopic atomic structure. The macroscopic unitsofmeasurementofheatandmassarethejouleandthegram,chosentobeeasily discernable by the human senses. The microscopic units of motion and structure are 12 10 the picosecond (10 seconds) and the ångstrom (10 meters), chosen to fit the atomic scales. One notes a factor of 10,000 between the two atomic units when expressed in “human” units, second and gram—with one gram being equal to one cubic centimeter when considering water. Perhaps this is the reason for the much better understanding and greater interest in the structure of materials, being closer to human experience when compared to molecular motion.