Thermal Annealing of Laser Damage Precursors on Fused Silica Surfaces

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ISBN 13 :
Total Pages : 19 pages
Book Rating : 4.:/5 (951 download)

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Book Synopsis Thermal Annealing of Laser Damage Precursors on Fused Silica Surfaces by :

Download or read book Thermal Annealing of Laser Damage Precursors on Fused Silica Surfaces written by and published by . This book was released on 2012 with total page 19 pages. Available in PDF, EPUB and Kindle. Book excerpt: Previous studies have identified two significant precursors of laser damage on fused silica surfaces at fluenes below H"35 J/cm2, photoactive impurities in the polishing layer and surface fractures. In the present work, isothermal heating is studied as a means of remediating the highly absorptive, defect structure associated with surface fractures. A series of Vickers indentations were applied to silica surfaces at loads between 0.5N and 10N creating fracture networks between H"10{micro}m and H"50{micro}m in diameter. The indentations were characterized prior to and following thermal annealing under various times and temperature conditions using confocal time-resolved photo-luminescence (CTP) imaging, and R/1 optical damage testing with 3ns, 355nm laser pulses. Significant improvements in the damage thresholds, together with corresponding reductions in CTP intensity, were observed at temperatures well below the glass transition temperature (T{sub g}). For example, the damage threshold on 05.N indentations which typically initiates at fluences 8 J/cm2 could be improved35 J/cm2 through the use of a H"750 C thermal treatment. Larger fracture networks required longer or higher temperature treatment to achieve similar results. At an annealing temperature> 1100 C, optical microscopy indicates morphological changes in some of the fracture structure of indentations, although remnants of the original fracture and significant deformation was still observed after thermal annealing. This study demonstrates the potential of using isothermal annealing as a means of improving the laser damage resistance of fused silica optical components. Similarly, it provides a means of further understanding the physics associated with optical damage and related mitigation processes.

Effect of Thermal Anneal on Growth Behavior of Laser-Induced Damage Sites on the Exit Surface of Fused Silica

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ISBN 13 :
Total Pages : 12 pages
Book Rating : 4.:/5 (16 download)

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Book Synopsis Effect of Thermal Anneal on Growth Behavior of Laser-Induced Damage Sites on the Exit Surface of Fused Silica by :

Download or read book Effect of Thermal Anneal on Growth Behavior of Laser-Induced Damage Sites on the Exit Surface of Fused Silica written by and published by . This book was released on 2012 with total page 12 pages. Available in PDF, EPUB and Kindle. Book excerpt:

High-power Laser Damage in Fused Silica

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ISBN 13 :
Total Pages : 606 pages
Book Rating : 4.:/5 (34 download)

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Book Synopsis High-power Laser Damage in Fused Silica by : Alberto Salleo

Download or read book High-power Laser Damage in Fused Silica written by Alberto Salleo and published by . This book was released on 2001 with total page 606 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Ultra-violet Laser Damage in Fused Silica

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ISBN 13 :
Total Pages : 248 pages
Book Rating : 4.:/5 (34 download)

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Book Synopsis Ultra-violet Laser Damage in Fused Silica by : Alberto Salleo

Download or read book Ultra-violet Laser Damage in Fused Silica written by Alberto Salleo and published by . This book was released on 1998 with total page 248 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Laser Damage Precursors in Fused Silica

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ISBN 13 :
Total Pages : 14 pages
Book Rating : 4.:/5 (727 download)

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Book Synopsis Laser Damage Precursors in Fused Silica by :

Download or read book Laser Damage Precursors in Fused Silica written by and published by . This book was released on 2009 with total page 14 pages. Available in PDF, EPUB and Kindle. Book excerpt: There is a longstanding, and largely unexplained, correlation between the laser damage susceptibility of optical components and both the surface quality of the optics, and the presence of near surface fractures in an optic. In the present work, a combination of acid leaching, acid etching, and confocal time resolved photoluminescence (CTP) microscopy has been used to study laser damage initiation at indentation sites. The combination of localized polishing and variations in indentation loads allows one to isolate and characterize the laser damage susceptibility of densified, plastically flowed and fractured fused silica. The present results suggest that: (1) laser damage initiation and growth are strongly correlated with fracture surfaces, while densified and plastically flowed material is relatively benign, and (2) fracture events result in the formation of an electronically defective rich surface layer which promotes energy transfer from the optical beam to the glass matrix.

Thin Film Contamination Effects on Laser-induced Damage of Fused Silica Surfaces at 355 Nm

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ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (683 download)

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Book Synopsis Thin Film Contamination Effects on Laser-induced Damage of Fused Silica Surfaces at 355 Nm by :

Download or read book Thin Film Contamination Effects on Laser-induced Damage of Fused Silica Surfaces at 355 Nm written by and published by . This book was released on 1998 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Fused silica windows were artificially contaminated to estimate the resistance of target chamber debris shields against laser damage during NIF operation. Uniform contamination thin films (1 to 5 nm thick) were prepared by sputtering various materials (Au, Al, Cu, and B4C). The loss of transmission of the samples was first measured. They were then tested at 355 nm in air with an 8-ns Nd:YAG laser. The damage morphologies were characterized by Nomarski optical microscopy and SEM. Both theory and experiments showed that metal contamination for films as thin as 1 nm leads to a substantial loss of transmission. The laser damage resistance dropped very uniformly across the entire surface (e.g. 6 J/cm2 for 5 nm of Cu). The damage morphology characterization showed that contrary to clean silica, metal coated samples did not produce pits on the surface. B4C coated silica, on the other hand, led to a higher density of such damage pits. A model for light absorption in the thin film was coupled with a simple heat deposition and diffusion model to perform preliminary theoretical estimates of damage thresholds. The estimates of the loss due to light absorption and reflection pointed out significant .differences between metals (e.g. Al and Au). The damage threshold predictions were in qualitative agreement with experimental measurements.

HF-based Etching Processes for Improving Laser Damage Resistance of Fused Silica Optical Surfaces

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ISBN 13 :
Total Pages : 32 pages
Book Rating : 4.:/5 (727 download)

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Book Synopsis HF-based Etching Processes for Improving Laser Damage Resistance of Fused Silica Optical Surfaces by :

Download or read book HF-based Etching Processes for Improving Laser Damage Resistance of Fused Silica Optical Surfaces written by and published by . This book was released on 2010 with total page 32 pages. Available in PDF, EPUB and Kindle. Book excerpt: The effect of various HF-based etching processes on the laser damage resistance of scratched fused silica surfaces has been investigated. Conventionally polished and subsequently scratched fused silica plates were treated by submerging in various HF-based etchants (HF or NH4F:HF at various ratios and concentrations) under different process conditions (e.g., agitation frequencies, etch times, rinse conditions, and environmental cleanliness). Subsequently, the laser damage resistance (at 351 or 355 nm) of the treated surface was measured. The laser damage resistance was found to be strongly process dependent and scaled inversely with scratch width. The etching process was optimized to remove or prevent the presence of identified precursors (chemical impurities, fracture surfaces, and silica-based redeposit) known to lead to laser damage initiation. The redeposit precursor was reduced (and hence the damage threshold was increased) by: (1) increasing the SiF62− solubility through reduction in the NH4F concentration and impurity cation impurities, and (2) improving the mass transport of reaction product (SiF62−) (using high frequency ultrasonic agitation and excessive spray rinsing) away from the etched surface. A 2D finite element crack-etching and rinsing mass transport model (incorporating diffusion and advection) was used to predict reaction product concentration. The predictions are consistent with the experimentally observed process trends. The laser damage thresholds also increased with etched amount (up to ≈30 [mu]m), which has been attributed to: (1) etching through lateral cracks where there is poor acid penetration, and (2) increasing the crack opening resulting in increased mass transport rates. With the optimized etch process, laser damage resistance increased dramatically; the average threshold fluence for damage initiation for 30 [mu]m wide scratches increased from 7 to 41 J/cm2, and the statistical probability of damage initiation at 12 J/cm2 of an ensemble of scratches decreased from ≈100 mm−1 of scratch length to ≈0.001 mm−1.

Laser Induced Damage in Optical Materials

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ISBN 13 :
Total Pages : 644 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Laser Induced Damage in Optical Materials by :

Download or read book Laser Induced Damage in Optical Materials written by and published by . This book was released on 1993 with total page 644 pages. Available in PDF, EPUB and Kindle. Book excerpt:

The Effect of Laser Annealing on Laser Induced Damage Threshold

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ISBN 13 :
Total Pages : 16 pages
Book Rating : 4.:/5 (125 download)

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Book Synopsis The Effect of Laser Annealing on Laser Induced Damage Threshold by : DC. Emmony

Download or read book The Effect of Laser Annealing on Laser Induced Damage Threshold written by DC. Emmony and published by . This book was released on 1990 with total page 16 pages. Available in PDF, EPUB and Kindle. Book excerpt: A significant enhancement of the single shot Laser Induced Damage Threshold of CaF2 and fused silica and a moderate enhancement for GaAs and Al has been observed as the result of laser annealing using an excimer laser operating at 248 nm. This phenomenon is primarily attributed to a reduction of the residual surface roughness of the samples.

1.06 ?m Laser-Induced Breakdown of CO2-Laser-Polished Fused SiO2

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ISBN 13 :
Total Pages : 10 pages
Book Rating : 4.:/5 (125 download)

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Book Synopsis 1.06 ?m Laser-Induced Breakdown of CO2-Laser-Polished Fused SiO2 by : PA. Temple

Download or read book 1.06 ?m Laser-Induced Breakdown of CO2-Laser-Polished Fused SiO2 written by PA. Temple and published by . This book was released on 1981 with total page 10 pages. Available in PDF, EPUB and Kindle. Book excerpt: Fused silica surfaces have been treated with continuous wave CO2-laser radiation in an improved raster technique. Laser damage data for 1.06-?m, 9-nsec, small-spot irradiation are presented. It is shown that a reasonably sharp transition from laser damage prone to laser damage resistant surfaces takes place over a small CO2-laser power range. The transition to high damage resistance takes place at a silica surface temperature where material flow begins to take place, as evidenced by the onset of residual strain in the CO2-processed part. These data are taken as evidence that microcrack healing is an important mechanism in increased damage resistance in CO2-polished parts. Also presented are data which show that CO2-treated surfaces have a small-spot damage threshold at least as high as the bulk damage threshold of SiO2. In addition, these treated parts show no obvious change in surface appearance, as seen in total internal reflection microscopy. They also show little change in transmissive figure. It is suggested that uniform preheating be used to eliminate the strain presently seen in CO2-treated parts.

Comprehensive Materials Finishing

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Publisher : Elsevier
ISBN 13 : 0128032502
Total Pages : 1467 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Comprehensive Materials Finishing by : M.S.J. Hashmi

Download or read book Comprehensive Materials Finishing written by M.S.J. Hashmi and published by Elsevier. This book was released on 2016-08-29 with total page 1467 pages. Available in PDF, EPUB and Kindle. Book excerpt: Finish Manufacturing Processes are those final stage processing techniques which are deployed to bring a product to readiness for marketing and putting in service. Over recent decades a number of finish manufacturing processes have been newly developed by researchers and technologists. Many of these developments have been reported and illustrated in existing literature in a piecemeal manner or in relation only to specific applications. For the first time, Comprehensive Materials Finishing, Three Volume Set integrates a wide body of this knowledge and understanding into a single, comprehensive work. Containing a mixture of review articles, case studies and research findings resulting from R & D activities in industrial and academic domains, this reference work focuses on how some finish manufacturing processes are advantageous for a broad range of technologies. These include applicability, energy and technological costs as well as practicability of implementation. The work covers a wide range of materials such as ferrous, non-ferrous and polymeric materials. There are three main distinct types of finishing processes: Surface Treatment by which the properties of the material are modified without generally changing the physical dimensions of the surface; Finish Machining Processes by which a small layer of material is removed from the surface by various machining processes to render improved surface characteristics; and Surface Coating Processes by which the surface properties are improved by adding fine layer(s) of materials with superior surface characteristics. Each of these primary finishing processes is presented in its own volume for ease of use, making Comprehensive Materials Finishing an essential reference source for researchers and professionals at all career stages in academia and industry. Provides an interdisciplinary focus, allowing readers to become familiar with the broad range of uses for materials finishing Brings together all known research in materials finishing in a single reference for the first time Includes case studies that illustrate theory and show how it is applied in practice

Mitigation of Laser Damage Growth in Fused Silica NIF Optics with a Galvanometer Scanned Carbon Dioxide Laser

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ISBN 13 :
Total Pages : 12 pages
Book Rating : 4.:/5 (316 download)

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Book Synopsis Mitigation of Laser Damage Growth in Fused Silica NIF Optics with a Galvanometer Scanned Carbon Dioxide Laser by : M. A. Norton

Download or read book Mitigation of Laser Damage Growth in Fused Silica NIF Optics with a Galvanometer Scanned Carbon Dioxide Laser written by M. A. Norton and published by . This book was released on 2006 with total page 12 pages. Available in PDF, EPUB and Kindle. Book excerpt: Economic operation of the National Ignition Facility at the Lawrence Livermore National Laboratory depends on controlling growth of laser damage in the large, high cost optics exposed to UV light at 351 nm. Mitigation of the growth of damage sites on fused silica surfaces greater than several hundred microns in diameter has been previously reported by us using galvanometer scanning of a tightly focused 10.6 {micro}m CO{sub 2} laser spot over an area encompassing the laser damage. Further investigation revealed that fused silica vapor re-deposited on the surface as ''debris'' led to laser damage at unexpectedly low fluences when exposed to multiple laser shots at 351 nm. Additionally, laser power and spatial mode fluctuations in the mitigation laser led to poor repeatability of the process. We also found that the shape of the mitigation pit could produce downstream intensification that could damage other NIF optics. Modifications were made to both the laser system and the mitigation process in order to address these issues. Debris was completely eliminated by these changes, but repeatability and downstream intensification issues still persist.

Mitigation of Laser Damage Growth in Fused Silica with a Galvanometer Scanned CO2 Laser

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ISBN 13 :
Total Pages : 12 pages
Book Rating : 4.:/5 (316 download)

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Book Synopsis Mitigation of Laser Damage Growth in Fused Silica with a Galvanometer Scanned CO2 Laser by : I. L. Bass

Download or read book Mitigation of Laser Damage Growth in Fused Silica with a Galvanometer Scanned CO2 Laser written by I. L. Bass and published by . This book was released on 2005 with total page 12 pages. Available in PDF, EPUB and Kindle. Book excerpt: At the National Ignition Facility (NIF) at the Lawrence Livermore National Laboratory (LLNL), mitigation of laser surface damage growth on fused silica using single and multiple CO{sub 2} laser pulses has been consistently successful for damage sites whose lateral dimensions are less than 100 {micro}m, but has not been for larger sites. Cracks would often radiate outward from the damage when a CO{sub 2} pulse was applied to the larger sites. An investigation was conducted to mitigate large surface damage sites using galvanometer scanning of a tightly focused CO{sub 2} laser spot over an area encompassing the laser damage. It was thought that by initially scanning the CO{sub 2} spot outside the damage site, radiating crack propagation would be inhibited. Scan patterns were typically inward moving spirals starting at radii somewhat larger than that of the damage site. The duration of the mitigation spiral pattern was {approx}110 ms during which a total of {approx}1.3 J of energy was delivered to the sample. The CO{sub 2} laser spot had a 1/e{sup 2}-diameter of {approx}200 {micro}m. Thus, there was general heating of a large area around the damage site while rapid evaporation occurred locally at the laser spot position in the spiral. A 30 to 40 {micro}m deep crater was typically generated by this spiral with a diameter of {approx}600 {micro}m. The spiral would be repeated until there was no evidence of the original damage in microscope images. Using this technique, damage sites as large as 300 mm in size did not display new damage after mitigation when exposed to fluences exceeding 22 J/cm{sup 2} at 355 nm, 7.5 ns. It was found necessary to use a vacuum nozzle during the mitigation process to reduce the amount of re-deposited fused silica. In addition, curing spiral patterns at lower laser powers were used to presumably ''re-melt'' any re-deposited fused silica. A compact, shearing interferometer microscope was developed to permit in situ measurement of the depth of mitigation sites.

The Effect of Pulse Duration on the Growth Rate of Laser-induced Damage Sites at 351 Nm on Fused Silica Surfaces

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ISBN 13 :
Total Pages : 10 pages
Book Rating : 4.:/5 (893 download)

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Book Synopsis The Effect of Pulse Duration on the Growth Rate of Laser-induced Damage Sites at 351 Nm on Fused Silica Surfaces by :

Download or read book The Effect of Pulse Duration on the Growth Rate of Laser-induced Damage Sites at 351 Nm on Fused Silica Surfaces written by and published by . This book was released on 2009 with total page 10 pages. Available in PDF, EPUB and Kindle. Book excerpt: Past work in the area of laser-induced damage growth has shown growth rates to be primarily dependent on the laser fluence and wavelength. More recent studies suggest that growth rate, similar to the damage initiation process, is affected by a number of additional parameters including pulse duration, pulse shape, site size, and internal structure. In this study, we focus on the effect of pulse duration on the growth rate of laser damage sites located on the exit surface of fused silica optics. Our results demonstrate, for the first time, a significant dependence of growth rate at 351 nm on pulse duration from 1 ns to 15 ns as [tau]{sup 0.3} for sites in the 50-100 [mu]m size range.

Fracture Induced Sub-Band Absorption as a Precursor to Optical Damage on Fused Silica Surfaces

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ISBN 13 :
Total Pages : 15 pages
Book Rating : 4.:/5 (727 download)

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Book Synopsis Fracture Induced Sub-Band Absorption as a Precursor to Optical Damage on Fused Silica Surfaces by :

Download or read book Fracture Induced Sub-Band Absorption as a Precursor to Optical Damage on Fused Silica Surfaces written by and published by . This book was released on 2010 with total page 15 pages. Available in PDF, EPUB and Kindle. Book excerpt: The optical damage threshold of indentation induced flaws on fused silica surfaces was explored. Mechanical flaws were characterized by laser damaged testing, SEM, optical, and photoluminescence microscopy. Localized polishing, chemical etching, and the control of indentation morphology were used to isolate the structural features which limit optical damage. A thin defect layer on fracture surfaces, including those smaller than the wavelength of visible light, was found to be the dominant source of laser damage initiation during illumination with 355nm, 3ns laser pulses. Little evidence was found that either displaced or densified material or fluence intensification plays a significant role in optical damage at fluences>35J/cm2. Elimination of the defect layer was shown to increase the overall damage performance of fused silica optics.

Amṯāl Sulaimān

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ISBN 13 :
Total Pages : 96 pages
Book Rating : 4.:/5 (165 download)

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Download or read book Amṯāl Sulaimān written by and published by . This book was released on 1834 with total page 96 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Chemical Etch Effects on Laser-Induced Surface Damage Growth in Fused Silica

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ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (682 download)

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Book Synopsis Chemical Etch Effects on Laser-Induced Surface Damage Growth in Fused Silica by :

Download or read book Chemical Etch Effects on Laser-Induced Surface Damage Growth in Fused Silica written by and published by . This book was released on 2005 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Abstract not provided.