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Temperature Programmed Gas Chromatography
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Book Synopsis Temperature-Programmed Gas Chromatography by : Leonid M. Blumberg
Download or read book Temperature-Programmed Gas Chromatography written by Leonid M. Blumberg and published by John Wiley & Sons. This book was released on 2011-09-22 with total page 363 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a comprehensive up-to-date overview of temperature-programmed gas chromatography (GC). The first part of the book introduces the reader to the basics concepts of GC, as well as the key properties of GC columns. The second part describes the mathematical and physical background of GC. In the third part, different aspects in the formation of a chromatogram are discussed, including retention times, peak spacing and peak widths. An invaluable reference for any chromatographer and analytical chemist, it provides all the answers to questions like: At what temperature does a solute elute in a temperature-programmed analysis? What is the value of the retention factor of eluting solute? How wide are the peaks? How large is the time distance between two peaks? How do all these parameters depend on the heating rate?
Book Synopsis Basic Gas Chromatography by : Harold M. McNair
Download or read book Basic Gas Chromatography written by Harold M. McNair and published by John Wiley & Sons. This book was released on 2011-09-20 with total page 195 pages. Available in PDF, EPUB and Kindle. Book excerpt: The New Edition of the Well-Regarded Handbook on Gas Chromatography Since the publication of the highly successful first edition of Basic Gas Chromatography, the practice of chromatography has undergone several notable developments. Basic Gas Chromatography, Second Edition covers the latest in the field, giving readers the most up-to-date guide available, while maintaining the first edition's practical, applied approach to the subject and its accessibility to a wide range of readers. The text provides comprehensive coverage of basic topics in the field, such as stationary phases, packed columns and inlets, capillary columns and inlets, detectors, and qualitative and quantitative analysis. At the same time, the coverage also features key additions and updated topics including: Gas chromatography-mass spectrometry (GC-MS) Sampling methods Multidimensional gas chromatography Fast gas chromatography Gas chromatography analysis of nonvolatile compounds Inverse gas chromatography and pyrolysis gas chromatography Along with these new and updated topics, the references, resources, and Web sites in Basic Gas Chromatography have been revised to reflect the state of the field. Concise and fundamental in its coverage, Basic Gas Chromatography, Second Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists.
Book Synopsis Split and Splitless Injection for Quantitative Gas Chromatography by : Konrad Grob
Download or read book Split and Splitless Injection for Quantitative Gas Chromatography written by Konrad Grob and published by John Wiley & Sons. This book was released on 2008-11-21 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated. This new edition offers: - New insights concerning sample evaporation in the injector - Information about matrix effects - A new chapter on injector design The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book. Furthermore the reader will understand the concepts of injection techniques and get a knowledge of the sources of error. The handbook also includes many practical guidelines. From reviews of former editions: "This substantial book is on injection techniques alone, which ... demonstrates this can have many pitfalls ... no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book ..." The Analyst "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day-to-day world of the working gas chromatographer. It will be useful ... for anyone who must work hands-on with GC." Journal of High Resolution Chromatography
Book Synopsis Programmed Temperature Gas Chromatography by : Walter Edgar Harris
Download or read book Programmed Temperature Gas Chromatography written by Walter Edgar Harris and published by New York : J. Wiley. This book was released on 1966 with total page 334 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis A Programmed Introduction to Gas-liquid Chromatography by : James Bulmer Pattison
Download or read book A Programmed Introduction to Gas-liquid Chromatography written by James Bulmer Pattison and published by . This book was released on 1973 with total page 372 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Rapid Temperature Programming and Pyrolysis Gas Chromatography by : Ronald R. Goforth
Download or read book Rapid Temperature Programming and Pyrolysis Gas Chromatography written by Ronald R. Goforth and published by . This book was released on 1967 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: A system has been developed whereby a pyrogram may be obtained for each separated component in a gas chromatographic effluent. These pyrograms may be used for "fingerprint" identifications of the peaks on a chromatogram. During the development of this system the characteristics of a low- pressure-drop packed column were examined as well as gas phase pyrolysis and rapid temperature programming. Linear temperature programming with program rates up to 400°C per minute was developed and used with a wide range of carrier gas flow rates. Retention temperatures predicted from isothermal data were verified. The importance of correc tly specifying the flow rate during rapid temperature programming became apparent during the investigation when predicted retention temperatures were otherwise less than the experimentally observed values. Pyrolyzer design for gas phase pyrolysis was considered. The temperature profile for a tubular pyrolyzer was examined experimentally. The effects of temperature and residence time on gas phase pyrolysis were studied using several hydrocarbons.
Book Synopsis Columns for Gas Chromatography by : Eugene F. Barry
Download or read book Columns for Gas Chromatography written by Eugene F. Barry and published by John Wiley & Sons. This book was released on 2007-04-27 with total page 315 pages. Available in PDF, EPUB and Kindle. Book excerpt: Choosing the right column is key in Gas Chromatography Gas Chromatography (GC) is the most widely used method for separating and analyzing a wide variety of organic compounds and gases. There have been many recent advancements in both packed column and capillary column GC. With numerous options and considerations, selecting the right column can be complicated. This resource provides essential guidance for scientists and technicians, including: Methods of choosing both capillary and packed columns Selection of dimensions (column length, I.D., film thickness, etc.) and type of column Guidelines for proper connections of the column to the injector and detector United States Pharmacopeia and National Formulary chromatographic methods ASTM, EPA, NIOSH, and OSHA column selection specifications Information on the advantages of computer assistance in GC and multidimensional GC Comprehensive information on column oven temperature control Columns for Gas Chromatography: Performance and Selection is a hands-on reference for scientists and technicians using GC.
Book Synopsis Programmable Selectivity and Fast Temperature Programming for High-speed GC Analysis of Wide Boiling-point-range Mixtures by : Carrie Ann Leonard Coutant
Download or read book Programmable Selectivity and Fast Temperature Programming for High-speed GC Analysis of Wide Boiling-point-range Mixtures written by Carrie Ann Leonard Coutant and published by . This book was released on 2000 with total page 366 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Gas Chromatography by : Brian Stuart
Download or read book Gas Chromatography written by Brian Stuart and published by Royal Society of Chemistry. This book was released on 2003 with total page 52 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book looks at gas chromatography, the most widely used technique in analytical chemistry.
Book Synopsis Analytical Gas Chromatography by : Walter Jennings
Download or read book Analytical Gas Chromatography written by Walter Jennings and published by Elsevier. This book was released on 2012-12-02 with total page 270 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Gas Chromatography is a free-standing introduction to and guide through the rapidly progressing field of analytical gas chromatography. The book is divided into 10 chapters that cover various aspects of analytical gas chromatography, from most advantageous column type to troubleshooting. The opening chapters of the book discuss the advantages of the open tubular column over the packed column. This topic is followed by significant chapters on various variables in the gas chromatographic process, including sample injection, stationary phase, carrier gas, and installation. The effect of changes in these variables on the solution elution order is also considered. A chapter also examines the influence of instrumental design features, such as excessive or unswept volumes in the flow path; suitability of the detection mode; and speed and fidelity of the data-handling equipment. The book also presents selected methods that have been employed to achieve better results for a given gas chromatographic problem. The application areas of gas chromatographic process, including food, flavor, fragrance, petroleum- and chemical-related, environment, biology, and medicine, are also presented. The concluding chapter addresses the basic troubleshooting knowledge and considers other chromatographic problems and methods for their rectification.
Book Synopsis Low-power Temperature-programmed Micro Gas Chromatography Columns by : Masoud Agah
Download or read book Low-power Temperature-programmed Micro Gas Chromatography Columns written by Masoud Agah and published by . This book was released on 2005 with total page 258 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Modern Practice of Gas Chromatography by : Robert L. Grob, PhD
Download or read book Modern Practice of Gas Chromatography written by Robert L. Grob, PhD and published by John Wiley & Sons. This book was released on 2004-08-04 with total page 1059 pages. Available in PDF, EPUB and Kindle. Book excerpt: The bible of gas chromatography-offering everything the professional and the novice need to know about running, maintaining, and interpreting the results from GC Analytical chemists, technicians, and scientists in allied disciplines have come to regard Modern Practice of Gas Chomatography as the standard reference in gas chromatography. In addition to serving as an invaluable reference for the experienced practitioner, this bestselling work provides the beginner with a solid understanding of gas chromatographic theory and basic techniques. This new Fourth Edition incorporates the most recent developments in the field, including entirely new chapters on gas chromatography/mass spectrometry (GC/MS); optimization of separations and computer assistance; high speed or fast gas chromatography; mobile phase requirements: gas system requirements and sample preparation techniques; qualitative and quantitative analysis by GC; updated information on detectors; validation and QA/QC of chromatographic methods; and useful hints for good gas chromatography. As in previous editions, contributing authors have been chosen for their expertise and active participation in their respective areas. Modern Practice of Gas Chromatography, Fourth Edition presents a well-rounded and comprehensive overview of the current state of this important technology, providing a practical reference that will greatly appeal to both experienced chomatographers and novices.
Book Synopsis Fire Debris Analysis by : Eric Stauffer
Download or read book Fire Debris Analysis written by Eric Stauffer and published by Academic Press. This book was released on 2007-12-10 with total page 683 pages. Available in PDF, EPUB and Kindle. Book excerpt: The study of fire debris analysis is vital to the function of all fire investigations, and, as such, Fire Debris Analysis is an essential resource for fire investigators. The present methods of analysis include the use of gas chromatography and gas chromatography-mass spectrometry, techniques which are well established and used by crime laboratories throughout the world. However, despite their universality, this is the first comprehensive resource that addresses their application to fire debris analysis. Fire Debris Analysis covers topics such as the physics and chemistry of fire and liquid fuels, the interpretation of data obtained from fire debris, and the future of the subject. Its cutting-edge material and experienced author team distinguishes this book as a quality reference that should be on the shelves of all crime laboratories. Serves as a comprehensive guide to the science of fire debris analysis Presents both basic and advanced concepts in an easily readable, logical sequence Includes a full-color insert with figures that illustrate key concepts discussed in the text
Book Synopsis Practical Gas Chromatography by : Katja Dettmer-Wilde
Download or read book Practical Gas Chromatography written by Katja Dettmer-Wilde and published by Springer. This book was released on 2014-11-05 with total page 904 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.
Book Synopsis Quantitative Gas Chromatography for Laboratory Analyses and On-Line Process Control by : G. Guiochon
Download or read book Quantitative Gas Chromatography for Laboratory Analyses and On-Line Process Control written by G. Guiochon and published by Elsevier. This book was released on 1988-06-01 with total page 796 pages. Available in PDF, EPUB and Kindle. Book excerpt: Here is an invaluable new book on quantitative gas chromatography which explains how the method can - or should - be used for accurate and precise analysis. Gas chromatography is firmly established as one of the few major methods for the quantitative analysis of complex mixtures. It is fast, accurate and inexpensive, with a broad range of applications. It has however become very complex and involved: over 200 stationary phases, more than 10 detector principles and several very different column types are available from among the catalogs of over 100 manufacturers and major retailers. The progressive changes in the nature of gas chromatography have created new needs for information which are not satisfied by the literature presently available. This book provides a complete discussion of all the problems involved in the achievement of quantitative analysis by gas chromatography, whether in the research laboratory, in the routine analysis laboratory or in process control. For this reason the presentation of theoretical concepts has been limited to the essential, while extensive explanations have been devoted to the various steps involved in the derivation of precise and accurate data. This starts with the selection of the instrumentation and column, continues with the choice of optimum experimental conditions, then calibration and ends with the use of correct procedures for data acquisition and calculations. Finally, there is almost always a way to reduce errors and an entire chapter deals with this single issue. Numerous relevant examples are presented. The first part of the book presents the theoretical background, simple enough to be understood by all analytical chemists, but still complete and up-to-date. It discusses the problems of flow dynamics, retention and band broadening. The changes in band profile associated with column overloading are explained without much recourse to mathematics. The second part describes the gas chromatograph and discusses the properties of each of its parts: gas flow and pressure controller sampling system, oven, column switching valves, detectors. The different implementations, their advantages and drawbacks are discussed and compared. In addition, three chapters present packed column technology, open tubular column technology and some sophisticated new phase systems, respectively. The new phase systems described use adsorbents, modified by coating or grafting organic phase, and carrier gases containing vapors which are sorbed by the stationary phase and modify it, such as steam. The third part discusses the applications in qualitative and quantitative analysis. Calibration, peak integration, sources of errors arising from the various parts of the instrument as well as from the measurement process itself are carefully described in four detailed chapters. Methods to carry out accurate and precise analysis are presented. A last chapter is devoted to process control analysis and gives a number of detailed examples of applications. A lexicon explaining the most important chromatographic terms and a detailed index complete the book. This is a book which no chemical analyst should be without. It should be on the library shelf of all universities, instrument companies and any laboratory and plant where gas chromatography is used.
Download or read book Gas Chromatography written by Colin Poole and published by Elsevier. This book was released on 2012-06-19 with total page 754 pages. Available in PDF, EPUB and Kindle. Book excerpt: A single source of authoritative information on all aspects of the practice of modern gas chromatography, from theory, to methods, to selected applications. It also provides access to core data for practical work, comparison of results, and decision making and facilitates the search for sources in related areas of study.
Book Synopsis The Development of a High Temperature (10000 C) Gas Chromatograph by : Charles B. Euston
Download or read book The Development of a High Temperature (10000 C) Gas Chromatograph written by Charles B. Euston and published by . This book was released on 1961 with total page 36 pages. Available in PDF, EPUB and Kindle. Book excerpt:
