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Synthesis And Characterization Of Zinc Oxide Nanowires
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Book Synopsis Zinc Oxide Nanostructures: Synthesis and Characterization by : Sotirios Baskoutas
Download or read book Zinc Oxide Nanostructures: Synthesis and Characterization written by Sotirios Baskoutas and published by MDPI. This book was released on 2018-12-04 with total page 303 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is a printed edition of the Special Issue "Zinc Oxide Nanostructures: Synthesis and Characterization" that was published in Materials
Book Synopsis Synthesis and Characterization of Zinc Oxide Nanowires by : Swee Yong Pung
Download or read book Synthesis and Characterization of Zinc Oxide Nanowires written by Swee Yong Pung and published by . This book was released on 2010 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: A rapid expansion in research work on zinc oxide nanowires (ZnO NWs) has been observed in recent years. The unique properties of wide bandgap and large exciton binding energy make ZnO NW s suitable for a wide range of devices, such as transistors, photodetectors, light-emitting diodes and laser diodes that operate in the blue and ultraviolet region of the spectrum. Currently, the principal development of ZnO NWs is focused on the gold (Au) catalyst and heteroepitaxial approach. However, the presence of Au may generate undesired deep level traps in the ZnO bandgap, which can be very harmful to the performance of transistors. The objective of this project is to synthesize undoped/doped ZnO NWs via homoepitaxial growth without using a foreign catalyst by Chemical Vapour Deposition (CVD) technique. A modified CVD process using Zn powder as the precursor has been established to produce high density by area of ZnO NWs. This modified CVD technique was reliable for the growth of NWs as suggested by the single factor Analysis of Variance. Both highly (00.2) oriented ZnO seed layer and slow growth processing conditions were the key requirements for growing vertically aligned ZnO NWs via the homoepitaxial approach by this modified CVD technique. The (00.2) dominant ZnO seed layers was deposited by the Atomic Layer Deposition technique. These seed layers had a smooth surface (RMS roughness: 2.850 nm), high transmittance (89.9±6.7%) and low film resistivity (4.l31xl0'3 a.cm). The growth ofself-catalyzed ZnO NWs was governed by the Vapour-Solid mechanism whereas a combined Vapour-Liquid-Solid and Vapour-Liquid mechanism was more appropriate in describing the growth mechanism of Au-catalyzed ZnO NWs. The surface energy of crystal planes which relate to the effectiveness of capturing adsorbed atoms determined the growth rate and proportion of crystallographic planes of self-catalyzed ZnO NWs. Lastly, in-situ Al doping on ZnO NWs has been demonstrated for the first time using Aerosol Assisted Chemical Vapour Deposition technique.
Book Synopsis Synthesis and Characterization of Zinc Oxide Nanowires, and Their Use in Spintronic and Photovoltaic Applications by : Benjamin Daniel Yuhas
Download or read book Synthesis and Characterization of Zinc Oxide Nanowires, and Their Use in Spintronic and Photovoltaic Applications written by Benjamin Daniel Yuhas and published by . This book was released on 2009 with total page 328 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis and Characterization of Zinc Oxide and Bismuth Oxide Nanowires Grown by Magnetron Sputtering by : Ben Sirota
Download or read book Synthesis and Characterization of Zinc Oxide and Bismuth Oxide Nanowires Grown by Magnetron Sputtering written by Ben Sirota and published by . This book was released on 2011 with total page 114 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanowires of Zinc oxide and bismuth oxide were grown on silicon substrates using vapor-liquid-solid (VLS) and unbalanced magnetron sputtering. Characterization using x-ray diffraction (XRD) and scanning electron microscopy (SEM) was conducted to investigate how growth conditions influence the structural and morphological properties of the materials. Optical properties were investigated using photoluminescence (PL), direct absorption spectra and cyclic voltammetry. The physical properties of sputtered ZnO were found to be dependent on oxygen flow rate, temperature, and the initial foreign metal catalysis seed layer. Nanowires were grown using a two-step process whereby an initial Au layer was deposited followed by Zn with oxygen. Doped ZnO-TiO 2 nanostructures were created by sputtering Ti and Zn simultaneously. Homo- and hetero-structured ZnO-ZnO and ZnO-TiO 2 were created using additional sputtering cycles. A systematic approach was taken to produce nanoarrays of Bi2 O3 by adjusting initial seed layer thickness and oxygen flow rates. A two step process involving variable oxygen flow rates was found to create the highest density of Bi 2 O3 nanowires in the array. Top-view and cross-sectional SEM micrographs suggested that the resulting Bi2 O3 nanowires were approximately 300 nm in length with diameters of 100 nm at the base and 30 nm at the top. Investigation into the growth method suggests a self-catalytic VLS-like process. Degradation tests using rhodamine 6G dye were compared to SEM images. Samples of ZnO and Bi 2 O3 displayed a direct correlation between nanowire density and photocatalytic efficiency.
Book Synopsis Nanostructured Zinc Oxide by : Kamlendra Awasthi
Download or read book Nanostructured Zinc Oxide written by Kamlendra Awasthi and published by Elsevier. This book was released on 2021-08-10 with total page 781 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanostructured Zinc Oxide covers the various routes for the synthesis of different types of nanostructured zinc oxide including; 1D (nanorods, nanowires etc.), 2D and 3D (nanosheets, nanoparticles, nanospheres etc.). This comprehensive overview provides readers with a clear understanding of the various parameters controlling morphologies. The book also reviews key properties of ZnO including optical, electronic, thermal, piezoelectric and surface properties and techniques in order to tailor key properties. There is a large emphasis in the book on ZnO nanostructures and their role in optoelectronics. ZnO is very interesting and widely investigated material for a number of applications. This book presents up-to-date information about the ZnO nanostructures-based applications such as gas sensing, pH sensing, photocatalysis, antibacterial activity, drug delivery, and electrodes for optoelectronics. Reviews methods to synthesize, tailor, and characterize 1D, 2D, and 3D zinc oxide nanostructured materials Discusses key properties of zinc oxide nanostructured materials including optical, electronic, thermal, piezoelectric, and surface properties Addresses most relevant zinc oxide applications in optoelectronics such as light-emitting diodes, solar cells, and sensors
Book Synopsis Synthesis and Characterization of Zinc Oxide Nanoparticles by : Zewdu Weldemichael Zena
Download or read book Synthesis and Characterization of Zinc Oxide Nanoparticles written by Zewdu Weldemichael Zena and published by LAP Lambert Academic Publishing. This book was released on 2013 with total page 92 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book reports study on the synthesis and characterization of ZnO nanoparticles by a two-step synthesis procedure. The first step is the solution-free mechanochemical synthesis of zinc tartarate followed by thermal decomposition. The synthesized ZnO nanoparticles were characterized by XRD, Uv-Vis spectrophotometer, Transmission electron microscope, Scanning electron microscope, Energy dispersive x-ray spectroscopy and Elemental mapping analysis techniques, and the corresponding results were clearly described in this work.I confidently recommend that this book can be used as a reference for physicists, chemists and university students concerning to the fields of Nanoscience and Nanotechnology
Book Synopsis Multifunctional Oxide-Based Materials: From Synthesis to Application by : Teofil Jesionowski
Download or read book Multifunctional Oxide-Based Materials: From Synthesis to Application written by Teofil Jesionowski and published by MDPI. This book was released on 2019-09-03 with total page 204 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book deals with novel aspects and perspectives in metal oxide and hybrid material fabrication. The contributions are mainly focused on the search for a new group of advanced materials with designed physicochemical properties, especially an expanded porous structure and defined surface activity. The proposed technological procedures result in an enhanced activity of the synthesized hybrid materials, which is of great importance when considering their potential fields of application. The use of such materials in different technological disciplines, including aspects associated with environmental protection, allows for the verification of the proposed synthesis method. Thus, it can be stated that those aspects are of interdisciplinary character and may be located at the interface of three scientific disciplines—chemistry, materials science, and engineering—as well as environmental protection. Furthermore, the presented scientific scope is in some way an answer to the continuous demand for such types of materials and opens new perspectives for their practical use
Book Synopsis Zinc-Based Nanostructures for Environmental and Agricultural Applications by : Kamel A. Abd-Elsalam
Download or read book Zinc-Based Nanostructures for Environmental and Agricultural Applications written by Kamel A. Abd-Elsalam and published by Elsevier. This book was released on 2021-05-22 with total page 678 pages. Available in PDF, EPUB and Kindle. Book excerpt: Zinc-Based Nanostructures for Environmental and Agricultural Applications shows how zinc nanostructures are being used in agriculture, food and the environment. The book has been divided into two parts: Part I deals with the synthesis and characterization of zinc-based nanostructures such as biogenic, plant, microbial, and actinobacteria mediated synthesis of zinc nanoparticles, Part II is focused on agri-food applications such as antibacterial, antifungal, antimicrobial, plant disease management, controlling post-harvest diseases, pesticide sensing and degradations, plant promotions, ZnO nanostructure for food packaging application, safe animal food and feed supplement, elimination of mycotoxins, and veterinary applications. Part III reviews technological developments in environmental applications such as risks and benefits for aquatic organisms and the marine environment, antiseptic activity and toxicity mechanisms, wastewater treatment, and zinc oxide-based nanomaterials for photocatalytic degradation of environmental and agricultural pollutants. The book discusses various aspects, including the application of zinc-based nanostructures to enhance plant health and growth, the effect on soil microbial activity, antimicrobial mechanism, phytotoxicity and accumulation in plants, the possible impact of zinc-based nanostructures in the agricultural sector as nanofertilizer, enhancing crop productivity, and other possible antimicrobial mechanisms of ZnO nanomaterials. Explores the impact of a large variety of zinc-based nanostructures on agri-food and environment sectors Outlines how the properties of zinc-based nanostructures mean they are particularly efficient in environmental and agricultural application areas Assesses the major challenges of synthesizing and processing zinc-based nanostructured materials
Book Synopsis Nanocomposites for Electrochemical Capacitors by : Inamuddin
Download or read book Nanocomposites for Electrochemical Capacitors written by Inamuddin and published by Materials Research Forum LLC. This book was released on 2018-01-15 with total page 215 pages. Available in PDF, EPUB and Kindle. Book excerpt: Electrochemical capacitors or supercapacitors offer a number of advantages over batteries; they are more safe and reliable, charge quicker, have an indefinite lifespan, exhibit a high power density and a wide range of working temperature. Supercapacitors demonstrate an extraordinary potential in both consumer electronics and large-sized energy storage applications, e.g. in communications, transportation, aviation, and power industries. The book explores recent developments in the area of composite applications for supercapacitor electrodes based von conducting polymers, graphene, biomass, or carbonaceous quantum dots. Synthesis strategies of composite materials and electrode preparation methods are discussed in detail. Electrochemical Capacitors, Supercapacitors, Energy Storage, Supercapacitor Electrodes, Conducting Polymer Composites, Graphene-based Composites, Biomass-based Capacitors, Carbonaceous Quantum Dot Composites, Sol-Gel Synthesis, Sonochemical Synthesis, Polyaniline-Zirconia Nanofibers
Book Synopsis Synthesis of Zinc Oxide by Sol–Gel Method for Photoelectrochemical Cells by : Siti Salwa Alias
Download or read book Synthesis of Zinc Oxide by Sol–Gel Method for Photoelectrochemical Cells written by Siti Salwa Alias and published by Springer Science & Business Media. This book was released on 2013-11-20 with total page 59 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book focuses on the study of synthesized ZnO powder using Zn(CH3COO)2∙2H2O precursor, methanol (as solvent), and sodium hydroxide (NaOH) to vary the pH. The successfully synthesized ZnO powder from the sol-gel centrifugation and sol-gel storage methods were characterized and investigated by X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy, Fourier-transform infrared spectroscopy, UV–visible spectroscopy, and photoluminescence test to compare the properties of the nanoparticles. The best characteristic of the ZnO powder from both methods was observed when the powders were coated on an ITO glass to fabricate a PEC. The current density–voltage performances of both PECs were investigated under luminescent and dark conditions.
Book Synopsis Synthesis and Characterization of ZnO/Graphene Nanostructures for Electronics and Photocatalysis by : Seyed Ebrahim Chalangar
Download or read book Synthesis and Characterization of ZnO/Graphene Nanostructures for Electronics and Photocatalysis written by Seyed Ebrahim Chalangar and published by Linköping University Electronic Press. This book was released on 2021-04-08 with total page 132 pages. Available in PDF, EPUB and Kindle. Book excerpt: Recent rapid development of electronics and electro-optical devices demands affordable and reliable materials with enhanced performance. Forming nanocomposites of already well-known materials is one possible route towards novel functional materials with desirable synergistic enhanced properties. Incompatible chemical properties, mismatched crystal structures and weak bonding interactions between the substances, however, often limit the number of possible nanocomposites. Moreover, using an inexpensive, facile, large-area and flexible fabrication technique is crucial to employ the new composites in industrially viable applications. This thesis focuses on the synthesis and characterization of different zinc oxide/graphene (ZnO/GR) nanocomposites, well suited for optoelectronics and photocatalysis applications. Two different approaches of i) substrate-free random synthesis, and ii) template-assisted selective area synthesis were studied in detail. In the first approach, ZnO nanoparticles/rods were grown on GR. The obtained nanocomposites were investigated for better GR dispersity, electrical conductivity and optical properties. Besides, by adding silver iodide to the nanocomposite, an enhanced plasmonic solar-driven photocatalyst was synthesized and analyzed. In the second approach, arrays of single, vertically aligned ZnO nanorods were synthesized using a colloidal lithography-patterned sol-gel ZnO seed layer. Our demonstrated nanofabrication technique with simple, substrate independent, and large wafer-scale area compatibility improved the alignment and surface density of ZnO nanorods over large selective growth areas. Eventually, we found a novel method to further enhance the vertical alignment of the ZnO nanorods by introducing a GR buffer layer between the Si substrate and the ZnO seed layer, together with the mentioned patterning technique. The synthesized nanocomposites were analyzed using a large variety of experimental techniques including electron microscopy, photoelectron spectroscopy, x-ray diffraction, photoluminescence and cathodoluminescence spectroscopy for in-depth studies of their morphology, chemical and optical properties. Our findings show that the designed ZnO/GR nanocomposites with vertically aligned ZnO nanorods of high crystalline quality, synthesized with the developed low-cost nanofabrication technique, can lead to novel devices offering higher performance at a significantly lower fabrication cost.
Book Synopsis Synthesis and Characterization of Zinc Oxide Based Nanostructures and Composites for Energy Related Applications by : Ahmed Salah Mahdi Al-Asadi
Download or read book Synthesis and Characterization of Zinc Oxide Based Nanostructures and Composites for Energy Related Applications written by Ahmed Salah Mahdi Al-Asadi and published by . This book was released on 2016 with total page 214 pages. Available in PDF, EPUB and Kindle. Book excerpt: The main objective of this communication is to report the synthesis and characterization of zinc oxide (ZnO) based nanostructures and composites for energy related applications using a simple and cost-effective chemical bath deposition (CBD) technique. Highly crystalline zinc oxide (ZnO) nanowires (NWs) were synthesized through CBD method using a simple seeding technique. This seeding process includes dispersion of commercially available ZnO nanoparticles through spraying on a desired substrate prior to the CBD growth. A typical growth period of 16 h produced ZnO NW assemblies with an average diameter of ~45 nm and lengths of 1–1.3 μm, with an optical band gap of ~3.61 eV. The NWs growth was successfully achieved on various substrates (e.g silicon dioxide, plastic sheets, copper grid, and carbon nanotube buckypaper). The as-prepared ZnO NWs were found to be photoactive under ultra violet (UV) illumination. UV photosensor devices fabricated using these NW assemblies demonstrated a high photodetection abilities at room temperature under moderate UV illumination power of ~ 250 μW/cm2. These findings indicate the possibility of using ZnO NWs, grown using the same seeding method, for various opto-electronic applications. The same seeding technique was also used to grow ZnO NWs onto aligned multi-wall carbon nanotubes (MWCNTs), which were synthesized by using air assisted chemical vapor deposition (CVD) onto a SiO2/Si substrate. This ZnO NW/MWCNT hybrid structure was characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and Raman spectroscopy. The fabricated structure was used as an electrode for supercapacitor (SC) measurements. Good electrochemical performance was accomplished with a specific capacitance of ~192 F/g along with a maximum energy density of ~3.8Wh/kg and a high power density of ~ 28 kW/kg. The fabricated device showed high stability and it retained over 99% of its initial specific capacitance value after 2000 cycles. In addition, we report on the synthesis & electrochemical characterization of two-dimensional Zinc-Aluminum (ZnAl) layered double hydroxides (LDHs) directly grown on Al substrate by using CBD method. After details structural characterization by SEM, Raman spectroscopy, EDS elemental mapping, and X-ray powder diffraction (XRD), the electrochemical performances of an electrode fabricated based on this material were evaluated via cyclic voltammetry and galvanostatic charge-discharge using various electrolytes. The ionic electrolyte device showed a maximum specific capacitance of 120 F/g along with a maximum energy density of 5.17 Wh/Kg and a high power density of 8.4 kW/h. Additionally, we found that a high specific capacitance value of 358 F/g was achieved using an aqueous electrolyte.
Download or read book Nanowires written by Simas Rackauskas and published by BoD – Books on Demand. This book was released on 2019-04-10 with total page 122 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanowires are attracting wide scientific interest due to the unique properties associated with their one-dimensional geometry. Developments in the understanding of the fundamental principles of the nanowire growth mechanisms and mastering functionalization provide tools to control crystal structure, morphology, and the interactions at the material interface, and create characteristics that are superior to those of planar geometries. This book provides a comprehensive overview of the most important developments in the field of nanowires, starting from their synthesis, discussing properties, and finalizing with nanowire applications. The book consists of two parts: the first is devoted to the synthesis of nanowires and characterization, and the second investigates the properties of nanowires and their applications in future devices.
Book Synopsis Zinc Oxide Based Nano Materials and Devices by : , Prof. Dr. Ahmed Nahhas
Download or read book Zinc Oxide Based Nano Materials and Devices written by , Prof. Dr. Ahmed Nahhas and published by BoD – Books on Demand. This book was released on 2019-10-09 with total page 148 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents a review of recent advances in ZnO-based nanomaterials and devices. ZnO as a nanomaterial has gained substantial interest in the research area of wide bandgap semiconductors and is considered to be one of the major candidates for electronic and photonic applications. ZnO has distinguished and interesting electrical and optical properties and is considered to be a potential material in optoelectronic applications such as solar cells, surface acoustic wave devices, and UV emitters. ZnO's unique properties have attracted several researchers to study its electrical and optical properties. As a nanostructured material, ZnO exhibits many advantages for nanodevices. Moreover, it has the ability to absorb the UV radiation.
Book Synopsis Photocatalytic Reaction Engineering by : Hugo de Lasa
Download or read book Photocatalytic Reaction Engineering written by Hugo de Lasa and published by Springer Science & Business Media. This book was released on 2006-10-31 with total page 194 pages. Available in PDF, EPUB and Kindle. Book excerpt: Heterogeneous photocatalysis is a novel technique for water purification. Publications on photocatalysis span a relatively recent period of not more than 25 years. This is a technique that, according to our extensive experience on the development of laboratory scale and pilot plant units, has great promise to eliminate water and air pollutants. Photocatalysis offers much more than competitive techniques where pollutants are transferred from phases; photocatalysis can achieve complete mineralization of pollutants leaving non-toxic species such as CO2 and H2O and can be exploited at close to room temperature and ambient pressure.
Book Synopsis System-Materials Nanoarchitectonics by : Yutaka Wakayama
Download or read book System-Materials Nanoarchitectonics written by Yutaka Wakayama and published by Springer Nature. This book was released on 2022-01-03 with total page 334 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is the first publication to widely introduce the contributions of nanoarchitectonics to the development of functional materials and systems. The book opens up pathways to novel nanotechnology based on bottom-up techniques. In fields of nanotechnology, theoretical and practical limitations are expected in the bottom-up nanofabrication process. Instead, some supramolecular processes for nano- and microstructure formation including molecular recognition, self-assembly, and template synthesis have gained great attention as novel key technologies to break through expected limitations in current nanotechnology. This volume describes future images of nanotechnology and related materials and device science as well as practical applications for energy and biotechnology. Readers including specialists, non-specialists, graduate students, and undergraduate students can focus on the parts of the book that interest and concern them most. Target fields include materials chemistry, organic chemistry, physical chemistry, nanotechnology, and even biotechnology.
Book Synopsis Synthesis and Characterization of Zinc Oxide Complex Nanostructures by : Dinghao Tang
Download or read book Synthesis and Characterization of Zinc Oxide Complex Nanostructures written by Dinghao Tang and published by . This book was released on 2010 with total page 63 pages. Available in PDF, EPUB and Kindle. Book excerpt: Zinc Oxide nanostructures are important for many applications, specifically for developing novel catalysts and sensors which our research group has been working on. The objectives of this thesis are: (1) synthesis and characterization of complex ZnO nanostructures; (2) development of synthesis protocols for high-yield and reliable synthesis of nanostructures. In this thesis, chapter 1 introduces the background of nanoscience and nanotechnology, with a focus on nanomaterials. In chapter 2, the fundamental knowledge of ZnO and relevant characterization techniques are introduced, specifically the crystallography of ZnO wurtzite structure and the scanning (transmission) electron microscopy. Several goals have been achieved and they are reported in chapter 3 and 4. First, the nano-pyramid decorated microwires were fabricated. A growth mechanism for those complex nanostructures was proposed. Second, surface modification such as grooved surfaces of ZnO nanostructures has been realized. Grooved nanowires, microbelts, and micrometer-scale tetra-pods are discussed. Third, the effects of oxygen partial pressure on the growth of ZnO have been investigated. All the ZnO nanostructures reported in this thesis were synthesized by a physical vapor deposition method. The field-emission scanning electron microscope was used to examine the morphologies of the synthesized nanostructures. Aberration-corrected scanning transmission electron microscopy provided information on the fabricated nanostructures.
