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Synthesis And Application Of Mesoporous Silica
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Book Synopsis Functional Materials by : Mario Leclerc
Download or read book Functional Materials written by Mario Leclerc and published by Walter de Gruyter GmbH & Co KG. This book was released on 2014-10-10 with total page 513 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Functional Materials textbook is not simply a review of the vast body of literature of the recent years, as it holds the focus upon various aspects of application. Moreover, it selects only a few topics in favor of a solid and thorough treatment of the relevant aspects. This book comes in a good time, when a large body of academic literature has been accumulated and is waiting for a critical inspection in the light of the real demands of application." Professor Gerhard Wegner, Max-Planck Institute for Polymer Research, Mainz, Germany The chapters cover three important fields in the development of functional materials: energy, environment, and biomedical applications. These topics are explained and discussed from both an experimental and a theoretical perspective. Functional organic and inorganic materials are at the center of most technological breakthroughs. Therefore, the understanding of material properties is fundamental to the development of novel functionalities and applications.
Book Synopsis Nanoparticles for Biomedical Applications by : Eun Ji Chung
Download or read book Nanoparticles for Biomedical Applications written by Eun Ji Chung and published by Elsevier. This book was released on 2019-11-19 with total page 442 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanoparticles for Biomedical Applications: Fundamental Concepts, Biological Interactions and Clinical Applications brings into one place information on the design and biomedical applications of different classes of nanoparticles. While aspects are dealt with in individual journal articles, there is not one source that covers this area comprehensively. This book fills this gap in the literature. - Outlines an in-depth review of biomedical applications of a variety of nanoparticle classes - Discusses the major techniques for designing nanoparticles for use in biomedicine - Explores safety and regulatory aspects for the use of nanoparticles in biomedicine
Book Synopsis Synthesis and Application of Mesoporous Silica by : Xinqing Chen
Download or read book Synthesis and Application of Mesoporous Silica written by Xinqing Chen and published by . This book was released on 2011 with total page 197 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Mesoporous Silica-based Nanomaterials and Biomedical Applications - Part A by :
Download or read book Mesoporous Silica-based Nanomaterials and Biomedical Applications - Part A written by and published by Academic Press. This book was released on 2018-09-24 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Cancer Therapy and Diagnosis, Part A, Volume 43 in The Enzymes series, highlights new advances in the field, with this new volume presenting interesting chapters on Mesoporous silica nanoparticle synthesis, Periodic mesoporous organosilica, Nanovalves and other nanomachine-equipped nanoparticles and controlled release, Two-photon light control and photodynamic therapy, Biodegradable PMO nanoparticles, Cationic mesoporous silica and protein delivery, Drug loading, stimuli-responsive delivery and cancer treatment, Animal models and cancer therapy, siRNA delivery and TWIST shutdown for ovarian cancer treatment, and TBC (mesoporous silica nanoparticles and cancer therapy or biodistribution of MSN).
Book Synopsis Design, Synthesis, Multifunctionalization and Biomedical Applications of Multifunctional Mesoporous Silica-Based Drug Delivery Nanosystems by : Yu Chen
Download or read book Design, Synthesis, Multifunctionalization and Biomedical Applications of Multifunctional Mesoporous Silica-Based Drug Delivery Nanosystems written by Yu Chen and published by Springer. This book was released on 2015-10-14 with total page 100 pages. Available in PDF, EPUB and Kindle. Book excerpt: This thesis reports on essential advances in the design, synthesis and biomedical applications of multifunctional Mesoporous Silica Nanoparticles (MSNs). It provides several examples of multifunctional MSN-based drug delivery nanosystems and demonstrates successful synergistic cancer therapies combining MSNs and high-intensity focused ultrasound. The book will especially be of interest to researchers and graduate students in the fields of biomaterials, biology, chemistry, medicine and the life sciences who are working to develop new methods and technologies to combat cancer.
Download or read book Mesoporous Silica written by Shunai Che and published by Walter de Gruyter GmbH & Co KG. This book was released on 2020-12-17 with total page 216 pages. Available in PDF, EPUB and Kindle. Book excerpt: Mesoporous silica has large-scale industrial applications such as catalysis, drug delivery and bio/chemical absorptions. This book is devoted to all aspects and types of this material, focusing synthesis of mesoporous silica with anionic amphiphilic molecules. Characterization, properties, and applications are also discussed, making the book an essential reference for material scientists, chemists, and chemical Engineer.
Book Synopsis Synthesis and Application of Mesoporous Silica by : Xining Chen
Download or read book Synthesis and Application of Mesoporous Silica written by Xining Chen and published by LAP Lambert Academic Publishing. This book was released on 2014-09-17 with total page 224 pages. Available in PDF, EPUB and Kindle. Book excerpt: Mesoporous materials with well-defined pore size and structure have applications in a wide range of topics from catalysis, environment and medicine to electronics. This work presents the methods and procedures for preparing functional mesoporous materials for applications in the environment from removal of toxic metals to clean synthesis of fine chemicals. Magnetic mesoporous silica (magMCM-41) of large surface area (800 m2 g-1) and high magnetization (8.30 emu g-1) was prepared by grafting 10 nm magnetic iron oxide nanoparticles in the silica matrix, and this highly dispersible material can be easily separated from aqueous solution by a magnetic field. Functionalization of the surface with selected ligands and metal complexes creates powerful capabilities for chemical separation and catalysis. Fe3+-magMCM-41 prepared by grafting aminopropyls and then adsorbing Fe3+ was found to be a highly selective adsorbent which adsorbed only As(V) and Cr(VI) oxyanions (70 and 100 mg g-1, respectively) without any Cu(II). A series of salt-tolerant sorbents with designed functionalized groups were capable of removing 97 99% toxic heavy metals with a high Kd (distribution coefficient) value.
Book Synopsis Chemistry of Silica and Zeolite-Based Materials by : Abderrazzak Douhal
Download or read book Chemistry of Silica and Zeolite-Based Materials written by Abderrazzak Douhal and published by Elsevier. This book was released on 2019-07-04 with total page 464 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemistry of Silica and Zeolite-Based Materials covers a wide range of topics related to silica-based materials from design and synthesis to applications in different fields of science and technology. Since silica is transparent and inert to the light, it is a very attractive host material for constructing artificial photosynthesis systems. As an earth-abundant oxide, silica is an ideal and basic material for application of various oxides, and the science and technology of silica-based materials are fundamentally important for understanding other oxide-based materials. The book examines nanosolvation and confined molecules in silica hosts, catalysis and photocatalysis, photonics, photosensors, photovoltaics, energy, environmental sciences, drug delivery, and health. Written by a highly experienced and internationally renowned team from around the world, Chemistry of Silica and Zeolite-Based Materials is ideal for chemists, materials scientists, chemical engineers, physicists, biologists, biomedical sciences, environmental scientists, toxicologists, and pharma scientists. --- "The enormous versatility of silica for building a large variety of materials with unique properties has been very well illustrated in this book.... The reader will be exposed to numerous potential applications of these materials – from photocatalytic, optical and electronic applications, to chemical reactivity in confined spaces and biological applications. This book is of clear interest not only to PhD students and postdocs, but also to researchers in this field seeking an understanding of the possible applications of meso and microporous silica-derived materials." - Professor Avelino Corma, Institute of Chemical Technology (ITQ-CSIC) and Polytechnical University of Valencia, Spain Discusses the most important advances in various fields using silica materials, including nanosolvation and confined molecules in silica hosts, catalysis and photocatalysis, and other topics Written by a global team of experts from a variety of science and technology disciplines Ideal resource for chemists, materials scientists, and chemical engineers working with oxide-based materials
Book Synopsis Ordered Mesoporous Materials by : Dongyuan Zhao
Download or read book Ordered Mesoporous Materials written by Dongyuan Zhao and published by John Wiley & Sons. This book was released on 2012-11-28 with total page 544 pages. Available in PDF, EPUB and Kindle. Book excerpt: Mesoporous materials are a class of molecules with a large and uniform pore size, highly regular nanopores, and a large surface area. This book is devoted to all aspects and types of these materials and describes, in an in-depth and systematic manner, the step-by-step synthesis and its mechanism, as well as the characterization, morphology control, hybridization, and applications, of mesoporous molecular sieves. In so doing, it covers silicates, metal-doped silicates, nonsilicates, and organic-inorganic hybrids. Although the emphasis is on synthesis, the expert authors also discuss characterization and applications, ranging from catalysis and biochemistry to optics and the use of these materials as templates for nanomaterial synthesis. Both the fundamentals and the latest research results are covered, ensuring that this monograph serves as a reference for researchers in and newcomers to the field.
Book Synopsis Periodic Mesoporous Organosilicas by : Chang-Sik Ha
Download or read book Periodic Mesoporous Organosilicas written by Chang-Sik Ha and published by Springer. This book was released on 2018-11-07 with total page 333 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a comprehensive overview of the fundamental properties, preparation routes and applications of a novel class of organic–inorganic nanocomposites known as periodic mesoporous organosilicas (PMOs). Mesoporous silicas are amorphous inorganic materials which have silicon and oxygen atoms in their framework with pore size ranging from 2 to 50 nm. They can be synthesized from surfactants as templates for the polycondensation of various silicon sources such as tetraalkoxysilane. In general, mesoporous silica materials possess high surface areas, tunable pore diameters, high pore volumes and well uniformly organized porosity. The stable chemical property and the variable ability for chemical modification makes them ideal for many applications such as drug carrier, sensor, separation, catalyst, and adsorbent. Among such mesoporous silicas, in 1999, three groups in Canada, Germany, and Japan independently developed a novel class of organic–inorganic nanocomposites known as periodic mesoporous organosilicas (PMOs). The organic functional groups in the frameworks of these solids allow tuning of their surface properties and modification of the bulk properties of the material. The book discusses the properties of PMOs, their preparation, different functionalities and morphology, before going on to applications in fields such as catalysis, drug delivery, sensing, optics, electronic devices, environmental applications (gas sensing and gas adsorption), biomolecule adsorption and chromatography. The book provides fundamental understanding of PMOs and their advanced applications for general materials chemists and is an excellent guide to these promising novel materials for graduate students majoring in chemical engineering, chemistry, polymer science and materials science and engineering.
Book Synopsis Ordered mesoporous silica COK-12: mesoscale tailoring, upscaling, continuous synthesis and application in the oxidative coupling of methane by : Colmenares, Maria
Download or read book Ordered mesoporous silica COK-12: mesoscale tailoring, upscaling, continuous synthesis and application in the oxidative coupling of methane written by Colmenares, Maria and published by Universitätsverlag der TU Berlin. This book was released on 2018-07-19 with total page 203 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ordered mesoporous silica (OMS) materials are a family of silica nanomaterials with pores ranging in size from 2 to 50 nm which are arranged periodically within the silica matrix. They have expanding applications in various fields of research, such as drug delivery, adsorption, separation and catalysis. COK-12 is an OMS produced by the soft-templating method, using the block copolymer P123 as a structure-directing agent. The synthesis takes place at room temperature under mild reaction conditions. In comparison with the most widely known OMS, the synthesis of COK-12 is more time efficient, inexpensive and environmentally friendly, yielding a material analogous to the well-known SBA-15. This thesis encompasses investigations regarding the production of the ordered mesoporous silica material (OMS) known as COK-12, in terms of upscaling of the synthesis and tailoring of the size and shape of its characteristic hexagonal pore structure. Batch upscaling of the synthesis yielded a material with nearly identical properties to that of the original COK-12. Upscaling of the COK-12 synthesis was also studied in continuous mode. The installation and operation of a continuous COK-12 production unit was carried out with the aim to determine the possibility of large-scale production of COK-12 with consistent material properties. COK-12 was produced in continuous mode by varying the time of aging of the COK-12 slurry and the flow rate of the feed streams, yielding materials with properties nearly identical to those of the original COK-12. COK-12 was used as a support for the Na2WO4-Mn/SiO2 catalyst for the oxidative coupling of methane reaction in various forms (powder, granular produced by pressing and monolithic), showing promising results comparable to the enhanced activity of the catalyst supported on the SBA-15. The advantage of using COK-12 over other OMS materials is that the facile nature of COK-12 synthesis makes it a viable candidate for industrial production of the Na2WO4-Mn/SiO2 catalyst, if paired with appropriate pelletizing and preparation method. The introduction of hexane and polypropylene glycol (PPG) as micellar swelling agents into the original COK-12 synthesis was studied in order to tailor the mesoporous structure of the system. Hexane was used as a micelle expander and as an agent to produce silica mesocellular foams, with “ink-bottle” shaped pores with a larger diameter than that of the original COK-12. By adding PPG into the synthesis, the shift of the mesostructure of COK-12 from 2D hexagonal to a multilamellar vesicular configuration was studied, resulting in the progressive formation of this type of material with increasing concentration of PPG. The flexibility of the COK-12 synthesis in terms of upscaling and tailoring of the mesostructure was examined throughout this work, with an aim to contribute to the existing and expanding knowledge regarding more versatile, sustainable and possibly industrial OMS production. Ordered Mesoporous Silica (OMS) gehört zu der Familie der Silica-Nanomaterialien mit periodisch angeordneten Mesoporen im Größenbereich zwischen 2 und 50 nm. Diese werden zunehmend in unterschiedlichen Forschungsfeldern wie Medikamentenfreisetzung, Adsorption, Separation und Katalyse eingesetzt. COK-12 ist ein OMS, das über eine Soft-Templating-Methode unter Nutzung des Blockcopolymers P123 als strukturbestimmenden Zusatz erzeugt wird. Die Synthese erfolgt bei Raumtemperatur unter milden Reaktionsbedingungen. Im Vergleich zu den am weitesten bekannten OMS-Materialien ist die Synthese von COK-12 zeiteffizient, günstig und umweltfreundlich. Dabei wird ein OMS-Material analog zu dem bereits etablierten SBA-15 erzeugt. Die vorliegende Dissertation umfasst die Synthese eines als COK-12 bekannten OMS-Materials, dem Scale-Up der Synthese sowie die Anpassung und Modifizierung der ursprünglich hexagonal-angeordneten Mesoporen bezüglich Porengrößen und Porenform. Das diskontinuierliche Scale-Up im Batchprozess führt zu nahezu identischen Materialeigenschaften im Vergleich zu dem ursprünglichen COK-12. Ein Scale-Up der COK-12-Synthese wurde zusätzlich im kontinuierlichen Prozess erprobt. Dessen Installation und Operation wurde mit dem Ziel durchgeführt, um die Möglichkeit einer Produktion von großen Mengen an COK-12 mit einheitlichen Materialeigenschaften zu validieren. Durch eine Variation der Alterungszeit als auch der Fließrate der Lösungen konnte COK-12 im kontinuierlichen Prozess mit nahezu identischen Eigenschaften wie das ursprüngliche COK-12 erzeugt werden. COK-12 wurde erfolgreich in verschiedenen Formen (Pulver, Pressgranulate und Monolithe) als Trägermaterial für Na2WO4-Mn/SiO2-Katalysatoren für die Oxidative Kopplung von Methan eingesetzt. Die resultierenden Aktivitäten ist sind vergleichbar mit denen des auf SBA-15-geträgerten Katalysators Der Vorteil der Nutzung von COK-12 im Vergleich zu anderen OMS-Materialien liegt in der vergleichsweise simplen COK-12-Synthese, weshalb es ein interessanter Kandidat für eine mögliche industrielle Produktion des Na2WO4-Mn/SiO2-Katalysators ist, wenn wenn geeignete Pelletierungs- und Herstellungsmethoden angewendet werden. Die Zugabe von Hexan und Polypropylenglykol (PPG) zur Aufweitung der Mizellen in der ursprünglichen COK-12-Synthese wurde untersucht, um die mesoporöse Struktur des Systems zu variieren. Hexan wurde eingesetzt zur Aufweitung der Mizellen und als Hilfsmittel zur Produktion mesozellulärer Silica-Schäume mit „ink-bottle“-förmigen Poren sowie vergrößertem Porendurchmesser im Vergleich zu denen des ursprünglichen COK-12. Durch die Zugabe von PPG in die Synthese verändert sich die Mesoporenstruktur der ursprünglichen hexagonalen 2D-Struktur zu einer multilamellaren vesikulären Anordnung, die mit zunehmender PPG-Konzentration verstärkt wird. Die Flexibilität der COK-12-Synthese wurde in dieser Arbeit in Bezug auf ein Scale-Up und eine Porenmodifikation weitreichend untersucht, mit dem Ziel das existierende Wissen in Bezug auf eine vielseitige, nachhaltige sowie eine potentielle Industrieproduktion der COK-12-Synthese zu entwickeln.
Book Synopsis Micro-Mesoporous Metallosilicates by : Peng Wu
Download or read book Micro-Mesoporous Metallosilicates written by Peng Wu and published by John Wiley & Sons. This book was released on 2024-05-28 with total page 501 pages. Available in PDF, EPUB and Kindle. Book excerpt: Micro-Mesoporous Metallosilicates Up-to-date and in-depth text bridging the technology gap between fundamental research and industry-scale applications of porous materials for catalysis Micro-Mesoporous Metallosilicates: Synthesis, Characterization, and Catalytic Applications comprehensively introduces the chemistry and catalytic technologies of metallosilicates, an important family of microporous crystalline zeolite and heteroatom-containing mesoporous materials, with a primary focus on design synthesis, characterization, theoretical studies, and catalytic applications of titanosilicates, tin-silicates, germanosilicates and Ti-mesosilica, and more. The text covers recent advances in the synthesis of titanosilicates, including hydrothermal synthesis, dry-gel conversion, fluoride-assisted synthesis, and post-synthesis methods, along with the synthesis of metallosilicates with two-dimensional lamellar structures and their structural modifications as well as applications in selective oxidation reactions. The text also discusses synthesis of germanosilicates with specially designed organic structure-directing agents, synthesis and catalytic applications of heteroatom-containing mesoporous silica, and dendritic mesoporous silica nanoparticles with unique wrinkled center-radial structures. Overall, every important porous metallosilicate and its synthesis, characterization, pore engineering, catalytic application, and industrial technique and process are covered. Specific sample topics discussed in Micro-Mesoporous Metallosilicates include: Chemical post-modifications of titanosilicates, in terms of the effects on transfer, adsorption/desorption, and surface reactions X-Ray based techniques, ultraviolet-visible-near infrared spectroscopy, Raman spectroscopy, and solid-state NMR spectroscopy Theoretical calculation as an effective tool and supplement to understand the catalytic active center, structural character, and Brønsted/Lewis acidity Titanosilicates in the liquid-phase epoxidation reaction of propylene and propylene chloride to corresponding epoxides Effects of particle sizes, oxidation state, and location sites of Au nanoparticles, and epoxidation performance of Ti-containing materials Delivering cutting-edge research and bridging the technology gap between fundamental research and industrial applications, Micro-Mesoporous Metallosilicates is a valuable resource for chemists, materials scientists, chemical engineers, and experienced researchers in related fields.
Book Synopsis Smart Nanovesicles for Drug Targeting and Delivery by : Maria Carafa
Download or read book Smart Nanovesicles for Drug Targeting and Delivery written by Maria Carafa and published by MDPI. This book was released on 2019-05-20 with total page 198 pages. Available in PDF, EPUB and Kindle. Book excerpt: We can use the short text on the SI page for the description, or you make slight modifications on it. The description/summary is only for promotion (flyer, distribution channels), and will not be included in the book You can use the short text on the SI page for the description Nanovesicles are highly-promising systems for the delivery and/or targeting of drugs, biomolecules and contrast agents. Despite the fact that initial studies in this area were performed on phospholipid vesicles, there is an ever-increasing interest in the use of other molecules to obtain smart vesicular carriers focusing on strategies for targeted delivery. These systems can be obtained using newly synthesized smart molecules, or by intelligent design of opportune carriers to achieve specific delivery to the site of action. The drug/contrast agent-containing vesicles need to be directed to precise locations within the body to obtain desired magnitude and duration of the therapeutic or diagnostic effect. This spatial control in the delivery might open new avenues to modulate drug activity while avoiding side-effects and to optimize contrast agent properties while avoiding a broad distribution in the organism. However, delivering and targeting active substances into specific tissues and cells is still a challenge in designing novel therapeutic approaches against untreatable disorders, such as tumors and degenerative diseases.
Book Synopsis Wrinkled Mesoporous Silica Synthesis and Applications by : Jason Lin
Download or read book Wrinkled Mesoporous Silica Synthesis and Applications written by Jason Lin and published by . This book was released on 2020 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Porous materials have been widely used for various applications. Due to their high surface area, tunable pore size, and adjustable pore structure, porous materials have played an important role in modern world scientific research. Recently, a new material, wrinkled mesoporous silica has attracted considerable attention due to the porosity, biocompatibility, and the morphology. In the past decade, wrinkled mesoporous silicas have been developed for catalysis, energy storage, absorption, and drug delivery. In this study, various types of wrinkled mesoporous silica have been synthesized and characterized. Biphenyl bridged wrinkled mesoporous silicas have also been used for iodine absorption and drug delivery.
Download or read book Porous Materials written by Kozo Ishizaki and published by Springer Science & Business Media. This book was released on 2013-11-27 with total page 249 pages. Available in PDF, EPUB and Kindle. Book excerpt: Approximately four million years of human history has passed. We have been using materials to make a variety of tools. The first materials used were naturally occurring materials such as animal bones, stones, wood etc.; and some of these familiar materials are porous. Porous materials are so familiar that they are sometimes forgotten or ignored. The taste experience of ice cream is created not only by adjusting ingre dients, but also by including air as an ingredient, i.e. pores that give the smooth texture of ice cream. This book is designed to describe and explain about pores, the synthesis of materials with pores (porous materials), and applications of porous materi als. This book is intended for engineers and scientists of different disciplines and specialities, and is expected to be useful in the design and synthesis of porous materials for existing as well as potential new applications. Let us rediscover pores. K. Ishizaki, S. Komameni and M. Nanko January 1998 1 Introduction 1.1 WHAT ARE POROUS MATERIALS? Porous materials are dermed as solids containing pores. Figure 1.1 shows different porous materials. Generally speaking, porous materials have a porosity of 0.2-0.95. The porosity means the fraction of pore volume to the total volume. Porous materials have been used in various applications from daily necessities, such as purifying drinking water by activated carbon or porous ceramics, to uses in modern industries, for example removing dusts from high purity process gases for semiconductor production.
Book Synopsis Chemistry of Zeolites and Related Porous Materials by : Ruren Xu
Download or read book Chemistry of Zeolites and Related Porous Materials written by Ruren Xu and published by John Wiley & Sons. This book was released on 2009-05-29 with total page 616 pages. Available in PDF, EPUB and Kindle. Book excerpt: Widely used in adsorption, catalysis and ion exchange, the family of molecular sieves such as zeolites has been greatly extended and many advances have recently been achieved in the field of molecular sieves synthesis and related porous materials. Chemistry of Zeolites and Related Porous Materials focuses on the synthetic and structural chemistry of the major types of molecular sieves. It offers a systematic introduction to and an in-depth discussion of microporous, mesoporous, and macroporous materials and also includes metal-organic frameworks. Provides focused coverage of the key aspects of molecular sieves Features two frontier subjects: molecular engineering and host-guest advanced materials Comprehensively covers both theory and application with particular emphasis on industrial uses This book is essential reading for researches in the chemical and materials industries and research institutions. The book is also indispensable for researches and engineers in R&D (for catalysis) divisions of companies in petroleum refining and the petrochemical and fine chemical industries.
Book Synopsis Mesoporous Zeolites by : Javier García-Martínez
Download or read book Mesoporous Zeolites written by Javier García-Martínez and published by John Wiley & Sons. This book was released on 2015-05-26 with total page 608 pages. Available in PDF, EPUB and Kindle. Book excerpt: Authored by a top-level team of both academic and industrial researchers in the field, this is an up-to-date review of mesoporous zeolites. The leading experts cover novel preparation methods that allow for a purpose-oriented fine-tuning of zeolite properties, as well as the related materials, discussing the specific characterization methods and the applications in close relation to each individual preparation approach. The result is a self-contained treatment of the different classes of mesoporous zeolites. With its academic insights and practical relevance this is a comprehensive handbook for researchers in the field and related areas, as well as for developers from the chemical industry.
