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Study On Reactor Structures For Bulk Polymerization Of Styrene
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Book Synopsis Study on Reactor Structures for Bulk Polymerization of Styrene by : Ashvin Kamaraju
Download or read book Study on Reactor Structures for Bulk Polymerization of Styrene written by Ashvin Kamaraju and published by . This book was released on 1983 with total page 184 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Rapid High Temperature Bulk Polymerization of Styrene in a Tubular Reactor by : Lefteris N. Valsamis
Download or read book Rapid High Temperature Bulk Polymerization of Styrene in a Tubular Reactor written by Lefteris N. Valsamis and published by . This book was released on 1977 with total page 320 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Experimental Studies and Mathematical Modeling of Aqueous Suspension Polymerization Reactors by : Georgios A. Kalfas
Download or read book Experimental Studies and Mathematical Modeling of Aqueous Suspension Polymerization Reactors written by Georgios A. Kalfas and published by . This book was released on 1992 with total page 670 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Preliminary Design of a Tubular Reactor for the Continuous Bulk Polymerization of Styrene by : Lefteris N. Valsamis
Download or read book Preliminary Design of a Tubular Reactor for the Continuous Bulk Polymerization of Styrene written by Lefteris N. Valsamis and published by . This book was released on 1975 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Masters Theses in the Pure and Applied Sciences by : Wade H. Shafer
Download or read book Masters Theses in the Pure and Applied Sciences written by Wade H. Shafer and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 407 pages. Available in PDF, EPUB and Kindle. Book excerpt: Masters Theses in the Pure and Applied Sciences was first conceived, published, and disseminated by the Center for Information and Numerical Data Analysis and Synthesis (CINDAS) * at Purdue University in 1 957, starting its coverage of theses with the academic year 1955. Beginning with Volume 13, the printing and dissemination phases of the activity were transferred to University Microfilms/Xerox of Ann Arbor, Michigan, with the thought that such an arrangement would be more beneficial to the academic and general scientific and technical community. After five years of this joint undertaking we had concluded that it was in the interest of all con cerned if the printing and distribution of the volumes were handled by an interna tional publishing house to assure improved service and broader dissemination. Hence, starting with Volume 18, Masters Theses in the Pure and Applied Sciences has been disseminated on a worldwide basis by Plenum Publishing Cor poration of New York, and in the same year the coverage was broadened to include Canadian universities. All back issues can also be ordered from Plenum. We have reported in Volume 29 (thesis year 1984) a total of 12,637 theses titles from 23 Canadian and 202 United States universities. We are sure that this broader base for these titles reported will greatly enhance the value of this important annual reference work. While Volume 29 reports theses submitted in 1984, on occasion, certain univer sities do report theses submitted in previous years but not reported at the time.
Book Synopsis Control of Polymerization Reactors by : Joseph Schork
Download or read book Control of Polymerization Reactors written by Joseph Schork and published by Routledge. This book was released on 2017-09-20 with total page 378 pages. Available in PDF, EPUB and Kindle. Book excerpt: This reference and text provides an in-depth description of developments in control techniques and their application to polymerization reactors and offers important introductory background information on polymerization reaction engineering.;Discussing modelling, identification, linear, nonlinear and multivariable schemes, Control of Polymerization Reactors: presents all available techniques that can be used to control reactors properly for optimal performance; shows how to manipulate pivotal variables that affect reactor control; examines methods for deriving dynamic process models to improve reactor efficiency; reviews reactor control problems and points out end-use properties; supplies methods for measuring process variables, and ways to estimate variables that can't be measured; and explains how single-input, single-output (SISO) strategies can be effectively used for control.;Filled with illustrative examples to clarify concepts, including more than 730 figures, tables and equations, Control of Polymerization Reactors is intended for use as a reference for chemical, process development, process design, research and development, control systems, and polymer engineers; and polymer chemists and physicists; as well as a text for upper-level undergraduate and graduate students in polymerization reactor control courses.
Book Synopsis Synthesis of Polymers by : Dieter A. Schlüter
Download or read book Synthesis of Polymers written by Dieter A. Schlüter and published by John Wiley & Sons. This book was released on 2012-05-23 with total page 1229 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymers are huge macromolecules composed of repeating structural units. While polymer in popular usage suggests plastic, the term actually refers to a large class of natural and synthetic materials. Due to the extraordinary range of properties accessible, polymers have come to play an essential and ubiquitous role in everyday life - from plastics and elastomers on the one hand to natural biopolymers such as DNA and proteins on the other hand. The study of polymer science begins with understanding the methods in which these materials are synthesized. Polymer synthesis is a complex procedure and can take place in a variety of ways. This book brings together the "Who is who" of polymer science to give the readers an overview of the large field of polymer synthesis. It is a one-stop reference and a must-have for all Chemists, Polymer Chemists, Chemists in Industry, and Materials Scientists.
Book Synopsis Modern Styrenic Polymers by : John Scheirs
Download or read book Modern Styrenic Polymers written by John Scheirs and published by John Wiley & Sons. This book was released on 2003-03-28 with total page 796 pages. Available in PDF, EPUB and Kindle. Book excerpt: This title addresses the latest developments in the field, covering the major advances that have occurred over the past five years in the polymerization and structure of new generation polystyrenes that are broadening its scope of application. It covers the advent of branched polystyrenes, syndiotactic polystyrene, high-molecular weight general purpose PS, styrenic interpolymers, and clear SBS copolymers Presents voluminous research previously only reported at conferences in one reference Unique coverage of a topic not found in the field
Book Synopsis Modelling and Control of the Polymerisation of Styrene by : T. M. Raja
Download or read book Modelling and Control of the Polymerisation of Styrene written by T. M. Raja and published by . This book was released on 1995 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Modelling and Experimental Studies of Free Radical Polymerization Reactors by : Xiaomang Zhang
Download or read book Modelling and Experimental Studies of Free Radical Polymerization Reactors written by Xiaomang Zhang and published by . This book was released on 1996 with total page 416 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Modelling and Control of the Polymerisation of Styrene by : Tariq M. Raja
Download or read book Modelling and Control of the Polymerisation of Styrene written by Tariq M. Raja and published by . This book was released on 1995 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: The thesis describes a study of polymerisation with the intention of demonstrating the generic feasibility of some control techniques for the production of polymers with prescribed molecular weight distributions. The polymerisation of styrene using thermal and catalytic initiation was used as an exemplar for the purposes of developing the strategies. A number of mathematical models have been developed, including the kinetics of the free-radical bulk polymerisation of styrene initiated thermally and by 2,2'azobisisobutyronitrile (AIBN) catalyst without consideration of the environment in which the reactions occur. The dynamics of the polymerisation process are described in terms of the first three moments of the distribution of dead polymer. These moments were used to characterise the molecular weight distribution of the polymer for the purposes of control. Further, the constraints of carrying out the polymerisation in batch and semi-batch reactors, continuous stirred tank reactors and a tubular reactor have been modelled. Dynamic optimisation using Pontryagin's minimum principle and the kinetic model was used to solve the minimum batch time problem by considering separately and simultaneously the two optimal policies, for initiator and temperature. These policies yield the minimum batch time to produce a polymer product which satisfies a set of target specifications for the molecular weight distribution. Using the kinetic and reactor models together, and the optimal temperature policy as a reference level, a model based predictive controller was employed to assess whether a realistic implementation of the policy could be achieved. A difficulty in the practical, real time control of polymerisation is the lack of on-line measurement of molecular weight. A preliminary study of a model based, non-linear observer was conducted to estimate molecular weight distribution on-line. It was shown that the estimate is robust in the face of disturbances and uncertainty in the initial conditions.
Book Synopsis Continuous Polymerization Reactors by : American Institute of Chemical Engineers
Download or read book Continuous Polymerization Reactors written by American Institute of Chemical Engineers and published by . This book was released on 1976 with total page 148 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Continuous Polymerization of Styrene in a Tubular Reactor by : David William Foster
Download or read book Continuous Polymerization of Styrene in a Tubular Reactor written by David William Foster and published by . This book was released on 1973 with total page 150 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Scientific and Technical Aerospace Reports by :
Download or read book Scientific and Technical Aerospace Reports written by and published by . This book was released on 1970 with total page 1338 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Dynamic Modelling and Optimization of Polymerization Processes in Batch and Semi-batch Reactors by : W. H. B. W. Ibrahim
Download or read book Dynamic Modelling and Optimization of Polymerization Processes in Batch and Semi-batch Reactors written by W. H. B. W. Ibrahim and published by . This book was released on 2012 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Dynamic modelling and optimization of three different processes namely (a) bulk polymerization of styrene, (b) solution polymerization of methyl methacrylate (MMA) and (c) emulsion copolymerization of Styrene and MMA in batch and semi-batch reactors are the focus of this work. In this work, models are presented as sets of differential-algebraic equations describing the process. Different optimization problems such as (a) maximum conversion (Xn), (b) maximum number average molecular weight (Mn) and (c) minimum time to achieve the desired polymer molecular properties (defined as pre-specified values of monomer conversion and number average molecular weight) are formulated. Reactor temperature, jacket temperature, initial initiator concentration, monomer feed rate, initiator feed rate and surfactant feed rate are used as optimization variables in the optimization formulations. The dynamic optimization problems were converted into nonlinear programming problem using the CVP techniques which were solved using efficient SQP (Successive Quadratic Programming) method available within the gPROMS (general PROcess Modelling System) software. The process model used for bulk polystyrene polymerization in batch reactors, using 2, 2 azobisisobutyronitrile catalyst (AIBN) as initiator was improved by including the gel and glass effects. The results obtained from this work when compared with the previous study by other researcher which disregarded the gel and glass effect in their study which show that the batch time operation are significantly reduced while the amount of the initial initiator concentration required increases. Also, the termination rate constant decreases as the concentration of the mixture increases, resulting rapid monomer conversion. The process model used for solution polymerization of methyl methacrylate (MMA) in batch reactors, using AIBN as the initiator and Toluene as the solvent was improved by including the free volume theory to calculate the initiator efficiency, f. The effects of different f was examined and compared with previous work which used a constant value of f 0.53. The results of these studies show that initiator efficiency, f is not constant but decreases with the increase of monomer conversion along the process. The determination of optimal control trajectories for emulsion copolymerization of Styrene and MMA with the objective of maximizing the number average molecular weight (Mn) and overall conversion (Xn) were carried out in batch and semi-batch reactors. The initiator used in this work is Persulfate K2S2O8 and the surfactant is Sodium Dodecyl Sulfate (SDS). Reduction of the pre-batch time increases the Mn but decreases the conversion (Xn). The sooner the addition of monomer into the reactor, the earlier the growth of the polymer chain leading to higher Mn. Besides that, Mn also can be increased by decreasing the initial initiator concentration (Ci0). Less oligomeric radicals will be produced with low Ci0, leading to reduced polymerization loci thus lowering the overall conversion. On the other hand, increases of reaction temperature (Tr) will decrease the Mn since transfer coefficient is increased at higher Tr leading to increase of the monomeric radicals resulting in an increase in termination reaction.
Book Synopsis Polymerization Reactors and Processes by : James Neil Henderson
Download or read book Polymerization Reactors and Processes written by James Neil Henderson and published by . This book was released on 1979 with total page 430 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis An Experimental Study of Multiple Steady States in a Photopolymerization Reactor by : Chih-Ning Kuan
Download or read book An Experimental Study of Multiple Steady States in a Photopolymerization Reactor written by Chih-Ning Kuan and published by . This book was released on 1982 with total page 388 pages. Available in PDF, EPUB and Kindle. Book excerpt: