Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials

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Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials

Author : Peter Kusch
Publisher : World Scientific
ISBN 13 : 1786345773
Total Pages : 268 pages
Book Rating : 4.7/5 (863 download)

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Book Synopsis Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials by : Peter Kusch

Download or read book Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials written by Peter Kusch and published by World Scientific. This book was released on 2018-10-08 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt: The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.

Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition)

Author : Peter Kusch
Publisher : World Scientific
ISBN 13 : 1800613008
Total Pages : 383 pages
Book Rating : 4.8/5 (6 download)

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Book Synopsis Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) by : Peter Kusch

Download or read book Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) written by Peter Kusch and published by World Scientific. This book was released on 2023-08-28 with total page 383 pages. Available in PDF, EPUB and Kindle. Book excerpt: Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.

Pyrolysis - GC/MS Data Book of Synthetic Polymers

Author : Shin Tsuge
Publisher : Elsevier
ISBN 13 : 0444538933
Total Pages : 420 pages
Book Rating : 4.4/5 (445 download)

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Book Synopsis Pyrolysis - GC/MS Data Book of Synthetic Polymers by : Shin Tsuge

Download or read book Pyrolysis - GC/MS Data Book of Synthetic Polymers written by Shin Tsuge and published by Elsevier. This book was released on 2011-08-02 with total page 420 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample

Pyrolysis - GC/MS Data Book of Synthetic Polymers

Author : Shin Tsuge
Publisher : Elsevier
ISBN 13 : 0444538925
Total Pages : 406 pages
Book Rating : 4.4/5 (445 download)

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Book Synopsis Pyrolysis - GC/MS Data Book of Synthetic Polymers by : Shin Tsuge

Download or read book Pyrolysis - GC/MS Data Book of Synthetic Polymers written by Shin Tsuge and published by Elsevier. This book was released on 2011-10-13 with total page 406 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample

Advanced Gas Chromatography

Author : Mustafa Ali Mohd
Publisher : BoD – Books on Demand
ISBN 13 : 9535102982
Total Pages : 474 pages
Book Rating : 4.5/5 (351 download)

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Book Synopsis Advanced Gas Chromatography by : Mustafa Ali Mohd

Download or read book Advanced Gas Chromatography written by Mustafa Ali Mohd and published by BoD – Books on Demand. This book was released on 2012-03-21 with total page 474 pages. Available in PDF, EPUB and Kindle. Book excerpt: Progress in agricultural, biomedical and industrial applications' is a compilation of recent advances and developments in gas chromatography and its applications. The chapters cover various aspects of applications ranging from basic biological, biomedical applications to industrial applications. Book chapters analyze new developments in chromatographic columns, microextraction techniques, derivatisation techniques and pyrolysis techniques. The book also includes several aspects of basic chromatography techniques and is suitable for both young and advanced chromatographers. It includes some new developments in chromatography such as multidimensional chromatography, inverse chromatography and some discussions on two-dimensional chromatography. The topics covered include analysis of volatiles, toxicants, indoor air, petroleum hydrocarbons, organometallic compounds and natural products. The chapters were written by experts from various fields and clearly assisted by simple diagrams and tables. This book is highly recommended for chemists as well as non-chemists working in gas chromatography.

Analytical Pyrolysis

Author : C.E.R. Jones
Publisher : Elsevier
ISBN 13 : 0444601406
Total Pages : 435 pages
Book Rating : 4.4/5 (446 download)

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Book Synopsis Analytical Pyrolysis by : C.E.R. Jones

Download or read book Analytical Pyrolysis written by C.E.R. Jones and published by Elsevier. This book was released on 2012-12-02 with total page 435 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Pyrolysis presents the Proceedings of the Third International Symposium on Analytical Pyrolysis, held in Amsterdam on September 7-9, 1976. It looks at newly emergent techniques in analytical pyrolysis, including pyrolysis mass spectrometry, gas chromatography, thin-layer chromatography, and pyrolysis-gas liquid chromatography. The book also covers topics ranging from automation and microbiology to forensic science and pharmacology, reproducibility and specificity, biochemistry, laser-induced pyrolysis, pyrolytic reaction mechanisms, and polymers. Comprised of 50 chapters, this book begins with a discussion of automatic analysis of tire rubber blends using computer-linked pyrolysis gas chromatography, thermal procedures in coupling with thin-layer chromatography, the role of pyrolysis-gas liquid chromatography in biomedical studies, and the identification of microorganisms by pyrolysis gas-liquid chromatography. It then examines forensic applications of analytical pyrolysis techniques, structure and degradation behavior of synthetic polymers using pyrolysis in combination with field ion mass spectrometry, determination of polysaccharides in fulvic acids by pyrolysis gas chromatography, and application of Curie-point pyrolysis mass spectrometry in fungal taxonomy. The reader is also introduced to pyrolysis mass spectrometry of model compounds labeled with stable isotopes, the use of pyrolysis/gas chromatography to determine the quality of porous polymers of styrene cross-linked with divinyl benzene, and application of pyrohydrolysis for a rapid and accurate determination of halides in silicate rocks and minerals. This volume will benefit students, researchers, chemists, and scientists working in the field of analytical pyrolysis.

Analytical Pyrolysis

Author : Peter Kusch
Publisher : BoD – Books on Demand
ISBN 13 : 1789849586
Total Pages : 104 pages
Book Rating : 4.7/5 (898 download)

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Book Synopsis Analytical Pyrolysis by : Peter Kusch

Download or read book Analytical Pyrolysis written by Peter Kusch and published by BoD – Books on Demand. This book was released on 2019-02-13 with total page 104 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical pyrolysis deals with the structural identification and quantitation of pyrolysis products with the ultimate aim of establishing the identity of the original material and the mechanisms of its thermal decomposition. The pyrolytic process is carried out in a pyrolyzer interfaced with analytical instrumentation such as gas chromatography (GC), mass spectrometry (MS), gas chromatography coupled with mass spectrometry (GC/MS), or with Fourier-transform infrared spectroscopy (GC/FTIR). By measurement and identification of pyrolysis products, the molecular composition of the original sample can often be reconstructed.This book is the outcome of contributions by experts in the field of pyrolysis and includes applications of the analytical pyrolysis-GC/MS to characterize the structure of synthetic organic polymers and lignocellulosic materials as well as cellulosic pulps and isolated lignins, solid wood, waste particle board, and bio-oil. The thermal degradation of cellulose and biomass is examined by scanning electron micrography, FTIR spectroscopy, thermogravimetry (TG), differential thermal analysis, and TG/MS. The calorimetric determination of high heating values of different raw biomass, plastic waste, and biomass/plastic waste mixtures and their by-products resulting from pyrolysis is described.

Analytical Pyrolysis of Natural Organic Polymers

Author : S.C. Moldoveanu
Publisher : Elsevier
ISBN 13 : 9780080527161
Total Pages : 510 pages
Book Rating : 4.5/5 (271 download)

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Book Synopsis Analytical Pyrolysis of Natural Organic Polymers by : S.C. Moldoveanu

Download or read book Analytical Pyrolysis of Natural Organic Polymers written by S.C. Moldoveanu and published by Elsevier. This book was released on 1998-11-11 with total page 510 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical pyrolysis is one of the many tools utilized for the study of natural organic polymers. This books describes in three parts the methodology of analytical pyrolysis, the results of pyrolysis for a variety of biopolymers, and several practical applications of analytical pyrolysis on natural organic polymers and their composite materials. Analytical pyrolysis methodology covers two distinct subjects, the instrumentation used for pyrolysis and the analytical methods that are applied for the analysis of the pyrolysis products. A variety of pyrolytic techniques and of analytical instruments commonly coupled with pyrolysis devices are given. The description of the results of pyrolysis for biopolymers and some chemically modified natural organic polymers is the core of the book. The main pyrolysis products of numerous compounds as well as the proposed mechanisms for their pyrolysis are described. In this part an attempt is made to present as much as possible the chemistry of the pyrolytic process of natural organic polymers. The applications of analytical pyrolysis include topics such as polymer detection used for example in forensic science, structure elucidation of specific polymers, and identification of small molecules present in polymers (anti-oxidants, plasticizers, etc.). Also, the degradation during heating is a subject of major interest in many practical applications regarding the physical properties of polymers. The applications to composite polymeric materials are in the fields of classification of microorganisms, study of a variety of biological samples, study of fossil materials, etc. Analytical pyrolysis can also be used for obtaining information on the burning area generate pyrolysates that have complex compositions. Their analysis is important in connection with health issues, environmental problems, and taste of food and cigarettes. Features of this book: • Presents analytical pyrolysis as a uniform subject and not as a conglomerate of scientific papers. • Puts together in an organized manner a large volume of available information in this specific field. • Provides original results which address subjects with relatively scarce information in literature. • Gives original views on subjects such as the parallel between the pyrolytic process and the ion fragmentation in mass spectrometry. • Includes the role of pyrolysis in the burning process. The three parts of the book are covered in 18 chapters, each divided into sections. Some sections are further divided by particular subjects. References are given for each chapter, and an effort has been made to include as much as possible from the available representative information. A few unpublished personal results are also included.

Mass Spectrometry of Polymers

Author : Giorgio Montaudo
Publisher : CRC Press
ISBN 13 : 1420037757
Total Pages : 601 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Mass Spectrometry of Polymers by : Giorgio Montaudo

Download or read book Mass Spectrometry of Polymers written by Giorgio Montaudo and published by CRC Press. This book was released on 2001-10-29 with total page 601 pages. Available in PDF, EPUB and Kindle. Book excerpt: Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results

Analytical Pyrolysis of Synthetic Organic Polymers

Author : Serban C. Moldoveanu
Publisher : Elsevier
ISBN 13 : 0080455867
Total Pages : 714 pages
Book Rating : 4.0/5 (84 download)

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Book Synopsis Analytical Pyrolysis of Synthetic Organic Polymers by : Serban C. Moldoveanu

Download or read book Analytical Pyrolysis of Synthetic Organic Polymers written by Serban C. Moldoveanu and published by Elsevier. This book was released on 2005-01-20 with total page 714 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Pyrolysis of Synthetic Organic Polymers is a follow-up to Analytical Pyrolysis of Natural Organic Polymers, which is volume 20 of the series. The main focus of the book is on practical applications of analytical pyrolysis in synthetic organic polymer identification and characterization. The first part of the book has five chapters including an introduction, a discussion on physico-chemistry of thermal degradation of synthetic polymers and on instrumentation used in analytical pyrolysis, a chapter discussing what type of information can be obtained from analytical pyrolysis, and a chapter dedicated to the analysis and characterization of synthetic polymers. The second part systematically covers the analytical pyrolysis of various classes of synthetic polymers. Some theoretical background for the understanding of polymer structure using analytical pyrolysis is also discussed. * Includes broad coverage of organic synthetic macromolecules * Focuses on physico-chemistry of thermal degradation, and the analytical pyrolysis of various classes of synthetic polymers * Is well written and suitable for both researchers and chemists working in analytical chemistry or in synthetic polymers

Thermal Degradation of Polymeric Materials

Author : Krzysztof Pielichowski
Publisher : iSmithers Rapra Publishing
ISBN 13 : 9781859574980
Total Pages : 324 pages
Book Rating : 4.5/5 (749 download)

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Book Synopsis Thermal Degradation of Polymeric Materials by : Krzysztof Pielichowski

Download or read book Thermal Degradation of Polymeric Materials written by Krzysztof Pielichowski and published by iSmithers Rapra Publishing. This book was released on 2005 with total page 324 pages. Available in PDF, EPUB and Kindle. Book excerpt: Understanding the thermal degradation of polymers is of paramount importance for developing a rational technology of polymer processing and higher-temperature applications. Controlling degradation requires understanding of many different phenomena, including chemical mechanisms, the influence of polymer morphology, the complexities of oxidation chemistry, and the effects of stabilisers, fillers and other additives. This book offers a wealth of information for polymer researchers and processors requiring an understanding of the implications of thermal degradation on material and product performance.

Methods in Lignin Chemistry

Author : Stephen Y. Lin
Publisher : Springer Science & Business Media
ISBN 13 : 3642740650
Total Pages : 595 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Methods in Lignin Chemistry by : Stephen Y. Lin

Download or read book Methods in Lignin Chemistry written by Stephen Y. Lin and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 595 pages. Available in PDF, EPUB and Kindle. Book excerpt: An up-to-date compilation of the theoretical background and practical procedures involved in lignin characterization. Whenever possible, the procedures are presented in sufficient detail to enable the reader to perform the analysis solely by following the step-by-step description. The advantages and limitations of individual methods are discussed and, more importantly, illustrated by typical analytical data in comparison to results obtained from other methods. This handbook serves the need of researchers and other professionals in academia, the pulp and paper industry as well as allied industries. It is equally useful for those with no previous experience in lignin or lignocellulosics.

Horizons in Polymer Research

Author : Robert K. Bregg
Publisher : Nova Publishers
ISBN 13 : 9781594544125
Total Pages : 214 pages
Book Rating : 4.5/5 (441 download)

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Book Synopsis Horizons in Polymer Research by : Robert K. Bregg

Download or read book Horizons in Polymer Research written by Robert K. Bregg and published by Nova Publishers. This book was released on 2005 with total page 214 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymers are substances containing a large number of structural units joined by the same type of linkage. These substances often form into a chain-like structure. Starch, cellulose, and rubber all possess polymeric properties. Today, the polymer industry has grown to be larger than the aluminum, copper and steel industries combined. Polymers already have a range of applications that far exceeds that of any other class of material available to man. Current applications extend from adhesives, coatings, foams, and packaging materials to textile and industrial fibers, elastomers, and structural plastics. Polymers are also used for most composites, electronic devices, biomedical devices, optical devices, and precursors for many newly developed high-tech ceramics. This new book presents leading-edge research in this rapidly-changing and evolving field.

Analytical Methods for Polymer Characterization

Author : Rui Yang
Publisher : CRC Press
ISBN 13 : 135121313X
Total Pages : 342 pages
Book Rating : 4.3/5 (512 download)

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Book Synopsis Analytical Methods for Polymer Characterization by : Rui Yang

Download or read book Analytical Methods for Polymer Characterization written by Rui Yang and published by CRC Press. This book was released on 2018-01-09 with total page 342 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Methods for Polymer Characterization presents a collection of methods for polymer analysis. Topics include chromatographic methods (gas chromatography, inverse gas chromatography, and pyrolysis gas chromatography), mass spectrometry, spectroscopic methods (ultraviolet-visible spectroscopy, infrared spectroscopy, Raman spectroscopy, and nuclear magnetic resonance), thermal analysis (differential scanning calorimetry and thermogravimetry), microscopy methods (scanning electron microscopy, transmission electron microscopy, and atomic force microscopy), and x-ray diffraction. The author also discusses mechanical and dynamic mechanical properties.

Practical Gas Chromatography

Author : Katja Dettmer-Wilde
Publisher : Springer
ISBN 13 : 3642546404
Total Pages : 904 pages
Book Rating : 4.6/5 (425 download)

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Book Synopsis Practical Gas Chromatography by : Katja Dettmer-Wilde

Download or read book Practical Gas Chromatography written by Katja Dettmer-Wilde and published by Springer. This book was released on 2014-11-05 with total page 904 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.

Sample Preparation in Chromatography

Author : S.C. Moldoveanu
Publisher : Elsevier
ISBN 13 : 0080540708
Total Pages : 949 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Sample Preparation in Chromatography by : S.C. Moldoveanu

Download or read book Sample Preparation in Chromatography written by S.C. Moldoveanu and published by Elsevier. This book was released on 2002-05-08 with total page 949 pages. Available in PDF, EPUB and Kindle. Book excerpt: Sample preparation is an essential step in many analyses. This book approaches the topic of sample preparation in chromatography in a methodical way, viewing it as a logical connection between sample collection and analytical chromatography. Providing a guide for choosing the appropriate sample preparation for a given analysis, this book describes various ways to process the sample, explaining the principle, discussing the advantages and disadvantages, describing the applicability to different types of samples, and showing the fitness to specific chromatographic determinations. The first part of the book contains an overview of sample preparation showing its relation to sample collection and to the core chromatographic analysis. The second part covers procedures that do not use chemical modifications of the analyte and includes methods for sample dissolution, concentration and cleanup designed mainly for modifying the initial matrix of the sample. This part starts with conventional separations such as filtration and distillation and finishes with more advanced techniques such as solid phase extraction and electroseparations. The third part gives a description of the chemical modifications that can be performed on a sample either for fractionation purposes or to improve a specific property of the analyte. This part includes derivatizations, polymer chemical degradations, and pyrolysis.

Polymer Characterisation

Author : B.J. Hunt
Publisher : Springer Science & Business Media
ISBN 13 : 9401121605
Total Pages : 376 pages
Book Rating : 4.4/5 (11 download)

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Book Synopsis Polymer Characterisation by : B.J. Hunt

Download or read book Polymer Characterisation written by B.J. Hunt and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 376 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymers continue to play an ever increasing role in the modern world. In fact it is quite inconceivable to most people that we could ever have existed of the increased volume and variety of materials without them. As a result currently available, and the diversity of their application, characterisation has become an essential requirement of industrial and academic laboratories in volved with polymeric materials. On the one hand requirements may come from polymer specialists involved in the design and synthesis of new materials who require a detailed understanding of the relationship between the precise molecular architecture and the properties of the polymer in order to improve its capabilities and range of applications. On the other hand, many analysts who are not polymer specialists are faced with the problems of analysing and testing a wide range of polymeric materials for quality control or material specification purposes. We hope this book will be a useful reference for all scientists and techno or industrial laboratories, logists involved with polymers, whether in academic and irrespective of their scientific discipline. We have attempted to include in one volume all of the most important techniques. Obviously it is not possible to do this in any great depth but we have encouraged the use of specific examples to illustrate the range of possibilities. In addition numerous references are given to more detailed texts on specific subjects, to direct the reader where appropriate. The book is divided into II chapters.