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Principles And Practice Of X Ray Spectrometric Analysis
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Book Synopsis Principles and Practice of X-ray Spectrometric Analysis by : Eugene P. Bertin
Download or read book Principles and Practice of X-ray Spectrometric Analysis written by Eugene P. Bertin and published by Springer. This book was released on 1970 with total page 712 pages. Available in PDF, EPUB and Kindle. Book excerpt: Excitation and nature of X-rays; X-ray spectra -- Properties of X-ray -- X-ray secondary-emission (fluorescence) spectrometry; general introduction -- Excitation -- Dispersion -- Detection -- Measurement -- Pulse-height analysis; nondispersive analysis -- Laboratory, automated, and special X-ray spectrometers -- Qualitative and semiquantitative analysis -- Precision and error; counting statistics -- Absorption-enhancement effects -- Sensitivity and resolution; spectral-line interference -- Methods of quantitative analysis -- Mathematical correction of absorption-enhancement effects -- Specimen preparation and presentation--general, solids, powders, briquets, fusion products -- Specimen preparation and presentation--liquids; supported specimens -- Measurement of thickness of films and platings -- Selected-area analysis -- Other analytical methods based on emission, absorption, and scatter of X-rays; other spectrometric methods involving X-rays -- The electron-probe microanalyzer.
Book Synopsis Introduction to X-Ray Spectrometric Analysis by : Eugene P. Bertin
Download or read book Introduction to X-Ray Spectrometric Analysis written by Eugene P. Bertin and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 494 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-ray fluorescence spectrometry has been an established, widely practiced method of instrumental chemical analysis for about 30 years. However, although many colleges and universities offer full-semester courses in optical spectrometric methods of instrumental analysis and in x-ray dif fraction, very few offer full courses in x-ray spectrometric analysis. Those courses that are given are at the graduate level. Consequently, proficiency in this method must still be acquired by: self-instruction; on-the-job training and experience; "workshops" held by the x-ray instrument manu facturers; the one- or two-week summer courses offered by a few uni versities; and certain university courses in analytical and clinical chemistry, metallurgy, mineralogy. geology, ceramics. etc. that devote a small portion of their time to applications of x-ray spectrometry to those respective disciplines. Moreover, with all due respect to the books on x-ray spectrometric analysis now in print, in my opinion none is really suitable as a text or manual for beginners in the discipline. In 1968, when I undertook the writing of the first edition of my previous book, Principles and Practice of X-Ray Spectrometric Analysis,* my objective was to provide a student text. However, when all the material was compiled, I decided to provide a more comprehensive book, which was also lacking at that time. Although that book explains principles, instrumentation, and methods at the begin ner's level, this material is distributed throughout a mass of detail and more advanced material.
Book Synopsis Principles and Practice of X-Ray Spectrometric Analysis by : E.P. Bertin
Download or read book Principles and Practice of X-Ray Spectrometric Analysis written by E.P. Bertin and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 1098 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the first edition of this book was published early in 1970, three major developments have occurred in the field of x-ray spectrochemical analysis. First, wavelength-dispersive spectrometry, in 1970 already securely established among instrumental analytical methods, has matured. Highly sophisticated, miniaturized, modular, solid-state circuitry has replaced elec tron-tube circuitry in the readout system. Computers are now widely used to program and control fully automated spectrometers and to store, process, and compute analytical concentrations directly and immediately from ac cumulated count data. Matrix effects have largely yielded to mathematical treatment. The problems associated with the ultralong-wavelength region have been largely surmounted. Indirect (association) methods have extended the applicability of x-ray spectrometry to the entire periodic table and even to certain classes of compounds. Modern commercial, computerized, auto matic, simultaneous x-ray spectrometers can index up to 60 specimens in turn into the measurement position and for each collect count data for up to 30 elements and read out the analytical results in 1--4 min-all corrected for absorption-enhancement and particle-size or surface-texture effects and wholly unattended. Sample preparation has long been the time-limiting step in x-ray spectrochemical analysis. Second, energy-dispersive spectrometry, in 1970 only beginning to assume its place among instrumental analytical methods, has undergone phenomenal development and application and, some believe, may supplant wavelength spectrometry for most applications in the foreseeable future.
Book Synopsis Principles and Practice of X-Ray Spectrometric Analysis by : E.P. Bertin
Download or read book Principles and Practice of X-Ray Spectrometric Analysis written by E.P. Bertin and published by Springer. This book was released on 2012-10-12 with total page 1080 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the first edition of this book was published early in 1970, three major developments have occurred in the field of x-ray spectrochemical analysis. First, wavelength-dispersive spectrometry, in 1970 already securely established among instrumental analytical methods, has matured. Highly sophisticated, miniaturized, modular, solid-state circuitry has replaced elec tron-tube circuitry in the readout system. Computers are now widely used to program and control fully automated spectrometers and to store, process, and compute analytical concentrations directly and immediately from ac cumulated count data. Matrix effects have largely yielded to mathematical treatment. The problems associated with the ultralong-wavelength region have been largely surmounted. Indirect (association) methods have extended the applicability of x-ray spectrometry to the entire periodic table and even to certain classes of compounds. Modern commercial, computerized, auto matic, simultaneous x-ray spectrometers can index up to 60 specimens in turn into the measurement position and for each collect count data for up to 30 elements and read out the analytical results in 1--4 min-all corrected for absorption-enhancement and particle-size or surface-texture effects and wholly unattended. Sample preparation has long been the time-limiting step in x-ray spectrochemical analysis. Second, energy-dispersive spectrometry, in 1970 only beginning to assume its place among instrumental analytical methods, has undergone phenomenal development and application and, some believe, may supplant wavelength spectrometry for most applications in the foreseeable future.
Book Synopsis X-ray Photoelectron Spectroscopy by : Paul van der Heide
Download or read book X-ray Photoelectron Spectroscopy written by Paul van der Heide and published by John Wiley & Sons. This book was released on 2011-11-01 with total page 275 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book introduces readers interested in the field of X-ray Photoelectron Spectroscopy (XPS) to the practical concepts in this field. The book first introduces the reader to the language and concepts used in this field and then demonstrates how these concepts are applied. Including how the spectra are produced, factors that can influence the spectra (all initial and final state effects are discussed), how to derive speciation, volume analysed and how one controls this (includes depth profiling), and quantification along with background substraction and curve fitting methodologies. This is presented in a concise yet comprehensive manner and each section is prepared such that they can be read independently of each other, and all equations are presented using the most commonly used units. Greater emphasis has been placed on spectral understanding/interpretation. For completeness sake, a description of commonly used instrumentation is also presented. Finally, some complementary surface analytical techniques and associated concepts are reviewed for comparative purposes in stand-alone appendix sections.
Book Synopsis A Handbook of Silicate Rock Analysis by : P.J. Potts
Download or read book A Handbook of Silicate Rock Analysis written by P.J. Potts and published by Springer Science & Business Media. This book was released on 2013-11-11 with total page 633 pages. Available in PDF, EPUB and Kindle. Book excerpt: without an appreciation of what happens in between. The techniques available for the chemical analysis of silicate rocks have undergone a revolution over the last 30 years. However, to use an analytical technique most effectively, No longer is the analytical balance the only instrument used it is essential to understand its analytical characteristics, in for quantitative measurement, as it was in the days of classi particular the excitation mechanism and the response of the cal gravimetric procedures. A wide variety of instrumental signal detection system. In this book, these characteristics techniques is now commonly used for silicate rock analysis, have been described within a framework of practical ana lytical aplications, especially for the routine multi-element including some that incorporate excitation sources and detec tion systems that have been developed only in the last few analysis of silicate rocks. All analytical techniques available years. These instrumental developments now permit a wide for routine silicate rock analysis are discussed, including range of trace elements to be determined on a routine basis. some more specialized procedures. Sufficient detail is In parallel with these exciting advances, users have tended included to provide practitioners of geochemistry with a firm to become more remote from the data production process. base from which to assess current performance, and in some This is, in part, an inevitable result of the widespread intro cases, future developments.
Book Synopsis X-Ray Fluorescence Spectrometry by : Ron Jenkins
Download or read book X-Ray Fluorescence Spectrometry written by Ron Jenkins and published by Wiley-Interscience. This book was released on 1988-10-03 with total page 192 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-Ray Fluorescence Spectrometry, Ron Jenkins Written by the principal scientist for JCPDS, the International Centre for Diffraction Data, Swarthmore, Pennsylvania, this book focuses on the scientific and technological developments achieved in the field during the past decade. It offers comprehensive coverage of all crucial topics, including: the properties and uses of X-ray emission spectrometry in material analysis; its industrial applications; X-ray diffraction; instrumentation for X-ray fluorescence spectrometry; a comparison of wavelength and energy dispersive spectrometers; and use of X-ray spectrometry for qualitative analysis.
Book Synopsis Handbook of X-Ray Data by : Günter H. Zschornack
Download or read book Handbook of X-Ray Data written by Günter H. Zschornack and published by Springer Science & Business Media. This book was released on 2007-01-24 with total page 969 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the only handbook available on X-ray data. In a concise and informative manner, the most important data connected with the emission of characteristic X-ray lines are tabulated for all elements up to Z = 95 (Americium). The tabulated data are characterized and, in most cases, evaluated. Furthermore, all important processes and phenomena connected with the production, emission and detection of characteristic X-rays are discussed.
Book Synopsis Elemental Analysis by : Gerhard Schlemmer
Download or read book Elemental Analysis written by Gerhard Schlemmer and published by Walter de Gruyter GmbH & Co KG. This book was released on 2019-08-05 with total page 414 pages. Available in PDF, EPUB and Kindle. Book excerpt: Elemental Analysis is an excellent guide introducing cutting-edge methods for the qualitative and quantitative analysis of elements. Each chapter of the book gives an overview of a certain technique, such as AAS, AFS, ICP-OES, MIP-OES, ICP-MS and XRF. Readers will benefit from a balanced combination of theoretical basics, operational principles of instruments and their practical applications.
Book Synopsis Handbook of Practical X-Ray Fluorescence Analysis by : Burkhard Beckhoff
Download or read book Handbook of Practical X-Ray Fluorescence Analysis written by Burkhard Beckhoff and published by Springer Science & Business Media. This book was released on 2007-05-18 with total page 897 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-Ray fluorescence analysis is an established technique for non-destructive elemental materials analysis. This book gives a user-oriented practical guidance to the application of this method. The book gives a survey of the theoretical fundamentals, analytical instrumentation, software for data processing, various excitation regimes including gracing incidents and microfocus measurements, quantitative analysis, applications in routine and micro analysis, mineralogy, biology, medicine, criminal investigations, archeology, metallurgy, abrasion, microelectronics, environmental air and water analysis. This book is the bible of X-Ray fluorescence analysis. It gives the basic knowledge on this technique, information on analytical equipment and guides the reader to the various applications. It appeals to researchers, analytically active engineers and advanced students.
Book Synopsis Quantitative X-Ray Spectrometry by : Ron Jenkins
Download or read book Quantitative X-Ray Spectrometry written by Ron Jenkins and published by CRC Press. This book was released on 1995-04-26 with total page 502 pages. Available in PDF, EPUB and Kindle. Book excerpt: This work covers important aspects of X-ray spectrometry, from basic principles to the selection of instrument parameters and sample preparation. This edition explicates the use of combined X-ray fluorescence and X-ray diffraction data, and features new applications in environmental studies, forensic science, archeometry and the analysis of metals
Book Synopsis Principles of Quantitative X-ray Fluorescence Analysis by : R. Tertian
Download or read book Principles of Quantitative X-ray Fluorescence Analysis written by R. Tertian and published by John Wiley & Sons. This book was released on 1982 with total page 412 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Handbook of X-Ray Spectrometry by : Rene Van Grieken
Download or read book Handbook of X-Ray Spectrometry written by Rene Van Grieken and published by CRC Press. This book was released on 2001-11-27 with total page 1016 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Updates fundamentals and applications of all modes of x-ray spectrometry, including total reflection and polarized beam x-ray fluorescence analysis, and synchrotron radiation induced x-ray emission. Promotes the accurate measurement of samples while reducing the scattered background in the x-ray spectrum."
Book Synopsis Laboratory Micro-X-Ray Fluorescence Spectroscopy by : Michael Haschke
Download or read book Laboratory Micro-X-Ray Fluorescence Spectroscopy written by Michael Haschke and published by Springer Science & Business Media. This book was released on 2014-05-08 with total page 367 pages. Available in PDF, EPUB and Kindle. Book excerpt: Micro-X-ray fluorescence offers the possibility for a position- sensitive and non-destructive analysis that can be used for the analysis of non-homogeneous materials and layer systems. This analytical technique has shown a dynamic development in the last 15 years and is used for the analysis of small particles, inclusions, of elemental distributions for a wide range of different applications both in research and quality control. The first experiments were performed on synchrotrons but there is a requirement for laboratory instruments which offers a fast and immediate access for analytical results. The book discuss the main components of a μ-XRF instrument and the different measurement modes, it gives an overview about the various instruments types, considers the special requirements for quantification of non-homogeneous materials and presents a wide range of application for single point and multi-point analysis as well as for distribution analysis in one, two and three dimensions.
Book Synopsis Trace Elemental Analysis of Metals by : Thomas R. Dulski
Download or read book Trace Elemental Analysis of Metals written by Thomas R. Dulski and published by Routledge. This book was released on 2017-10-06 with total page 602 pages. Available in PDF, EPUB and Kindle. Book excerpt: This work details minor, trace and ultratrace methods; addresses the essential stages that precede measurement; and highlights the measurement systems most likey to be used by the pragmatic analyst. It features key material on inclusion and phase isolation. The book is designed to provide useful maps and signposts for metals analysts who must verify that stringent trace level compositional specifications have been met.
Book Synopsis Analysis of the Composition and Structure of Glass and Glass Ceramics by : Hans Bach
Download or read book Analysis of the Composition and Structure of Glass and Glass Ceramics written by Hans Bach and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 541 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first book completely devoted to the subject, this volume describes the analysis of the composition and structure of glass and glass ceramics. Although conceived as a monograph, the individual chapters are written by leading Schott experts on the corresponding subjects.
Book Synopsis Advances in Portable X-ray Fluorescence Spectrometry by : B Lee Drake
Download or read book Advances in Portable X-ray Fluorescence Spectrometry written by B Lee Drake and published by Royal Society of Chemistry. This book was released on 2022-10-19 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: Over the last two decades, advances in the design, miniaturization, and analytical capabilities of portable X-ray fluorescence (pXRF) instrumentation have led to its rapid and widespread adoption in a remarkably diverse range of applications in research and industrial fields. The impetus for this volume was that, as pXRF continues to grow into mainstream use, analysts should be increasingly empowered with the right information to safely and effectively employ pXRF as part of their analytical toolkit. This volume provides introductory and advanced-level users alike with readings on topics ranging from basic principles of pXRF and qualitative and quantitative approaches, through to machine learning and artificial intelligence for enhanced applications. It also includes fundamental guidance on calibrations, the mathematics of calculating uncertainties, and an extensive reference index of all elements and their interactions with X-rays. Contributing authors have provided a wealth of information and case studies in industry-specific chapters. These sections delve into detail on current standard practices in industry and research, including examples from agricultural and geo-exploration sectors, research in art and archaeology, and metals industrial and regulatory applications. As pXRF continues to grow in use in industrial and academic settings, it is essential that practitioners continue to learn, share, and implement informed and effective use of this technique. This volume serves as an accessible guidebook and go-to reference manual for new and experienced users in pXRF to achieve this goal.
