Microwave Chemistry

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Publisher : Walter de Gruyter GmbH & Co KG
ISBN 13 : 3110479931
Total Pages : 552 pages
Book Rating : 4.1/5 (14 download)

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Book Synopsis Microwave Chemistry by : Giancarlo Cravotto

Download or read book Microwave Chemistry written by Giancarlo Cravotto and published by Walter de Gruyter GmbH & Co KG. This book was released on 2017-09-25 with total page 552 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microwave Chemistry has changed the way to work in chemical laboratories and is an established state-of-the-art technology to accelarate and enhance chemical processes. This book not only gives an overview of the technology, its historical development and theoretical background, but also presents its exceptionally broad spectrum of applications. Microwave Chemistry enables graduate students and scientist to learn and apply its methods successfully.

Microwave Chemical and Materials Processing

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Author :
Publisher : Springer
ISBN 13 : 9789819757947
Total Pages : 0 pages
Book Rating : 4.7/5 (579 download)

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Book Synopsis Microwave Chemical and Materials Processing by : Satoshi Horikoshi

Download or read book Microwave Chemical and Materials Processing written by Satoshi Horikoshi and published by Springer. This book was released on 2024-10-29 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book adds remarkable advances in microwave chemistry, methods, equipment, and practical examples since the first edition was published in 2018. Moreover, practical examples of the use of microwave energy have been upgraded. It also includes how to easily predict microwave heating using material constants. In addition, coupling analysis simulation with electromagnetic fields and heat transfer which greatly support researchers' experiments is covered. The principal aim of this book hasn’t changed: to introduce chemists through a tutorial approach to the use of microwaves by examining several experiments of microwave chemistry and materials processing. It subsequently enables chemists to fashion their own experiments in microwave chemistry or materials processing. This book helps chemists who take an interest in the use of microwave radiation to overcome difficulties to understand the nature of electromagnetism, microwave engineering, and thermodynamics.

Aqueous Microwave Assisted Chemistry

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Publisher : Royal Society of Chemistry
ISBN 13 : 1849730997
Total Pages : 243 pages
Book Rating : 4.8/5 (497 download)

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Book Synopsis Aqueous Microwave Assisted Chemistry by : Vivek Polshettiwar

Download or read book Aqueous Microwave Assisted Chemistry written by Vivek Polshettiwar and published by Royal Society of Chemistry. This book was released on 2010-05-20 with total page 243 pages. Available in PDF, EPUB and Kindle. Book excerpt: The demands for green and sustainable synthetic methods in the fields of healthcare and fine chemicals, combined with the pressure to produce these substances expeditiously and in an environmentally benign fashion, pose significant challenges to the synthetic chemical community. Green chemistry can avoid pollution by utilizing techniques that are environmentally friendly by design and one of the best green techniques is the use of microwave (MW) assisted aqueous synthetic protocols. Fusing MW technique with water (as a benign reaction medium) can offer an extraordinary synergistic effect with greater potential than these two individual components in isolation. Selective microwave heating can be exploited to develop a high yield protocol and the use of water expedites the MW-protocol with more energy efficiency. This book provides an overview of the various processes developed using aqueous microwave chemistry and is written for chemists, chemical engineers and researchers in the early stages who want to develop sustainable and green processes. Written by well known microwave experts, the book is a comprehensive examination of the field and is the first book that deals strictly with aqueous microwave chemistry and represents a significant effort towards green chemistry. It covers all the microwave-assisted aqueous reactions in depth, including heterocycle synthesis, metal catalysis, enzyme catalysis, polymer synthesis, nanomaterials synthesis and nano-catalysis. Each chapter contains representative experimental procedures, helping the reader quickly replicate some of the experiments to gain hands-on experience.

Synthetic Applications

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Publisher : Walter de Gruyter GmbH & Co KG
ISBN 13 : 3110730472
Total Pages : 578 pages
Book Rating : 4.1/5 (17 download)

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Book Synopsis Synthetic Applications by : Rajender S. Varma

Download or read book Synthetic Applications written by Rajender S. Varma and published by Walter de Gruyter GmbH & Co KG. This book was released on 2022-05-09 with total page 578 pages. Available in PDF, EPUB and Kindle. Book excerpt: Magnetic nanocatalysts are becoming an important tool for greener catalytic processes in chemical transformations in view of the ease of their removal from a reaction medium. This book explores assorted magnetic nanocatalysts, their deployment in synthesis, chemical transformation and their recovery and reuse. Various thematic topics embodied include magnetic nanocatalysts for S-S bond formation, N-heterocycle formation, C-heteroatom bond formation, silica-supported catalysts, multicomponent reactions, including their recyclability; another available volume emphasizes the utility of magnetic nanocatalysts in industrial appliances.

Microwave Assisted Organic Synthesis

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Publisher : John Wiley & Sons
ISBN 13 : 1405168447
Total Pages : 296 pages
Book Rating : 4.4/5 (51 download)

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Book Synopsis Microwave Assisted Organic Synthesis by : Jason Tierney

Download or read book Microwave Assisted Organic Synthesis written by Jason Tierney and published by John Wiley & Sons. This book was released on 2009-02-12 with total page 296 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first reports on the application of microwaves in organicsynthesis date back to 1986, but it was not until the recentintroduction of specifically designed and constructed equipment,which countered the safety and reproducibility concerns, thatsynthetic application of microwaves has become established as alaboratory technique. Microwave assisted synthesis is now beingadopted in many industrial and academic laboratories to takeadvantage of the novel chemistry that can be carried out using avariety of organic reaction types. This book demonstrates the underlying principles of microwavedielectric heating and, by reference to a range of organic reactiontypes, it's effective use in synthetic organic chemistry. Toillustrate the impact microwave assisted organic synthesis can haveon chemical research, case studies drawn mainly from thepharmaceutical industry are presented.

Practical Microwave Synthesis for Organic Chemists

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Author :
Publisher : John Wiley & Sons
ISBN 13 : 3527623914
Total Pages : 310 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Practical Microwave Synthesis for Organic Chemists by : C. Oliver Kappe

Download or read book Practical Microwave Synthesis for Organic Chemists written by C. Oliver Kappe and published by John Wiley & Sons. This book was released on 2008-11-21 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt: With the novice user in mind, this beginner's guide explains thebasics behind microwave technology, evaluates available instrumentsand reaction modes, and provides practical hints for everyeventuality. Includes 27 detailed protocols for often-usedreactions. From the contents: 1 Microwave Synthesis - An Introduction 2 Microwave Theory 3 Equipment Review 4 Microwave Processing Techniques 5 Starting With Microwave Chemistry 6 Experimental Protocols 6.1 General Small-Scale Sealed-Vessel Microwave Processing 6.2 Reaction Optimization 6.3 Library Generation 6.4 Reaction Scale-Up 6.5 Special Processing Techniques

Microwaves in Catalysis

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Publisher : John Wiley & Sons
ISBN 13 : 3527338152
Total Pages : 426 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Microwaves in Catalysis by : Satoshi Horikoshi

Download or read book Microwaves in Catalysis written by Satoshi Horikoshi and published by John Wiley & Sons. This book was released on 2015-12-14 with total page 426 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive overview covering the principles and preparation of catalysts, as well as reactor technology and applications in the field of organic synthesis, energy production, and environmental catalysis. Edited and authored by renowned and experienced scientists, this reference focuses on successful reaction procedures for applications in industry. Topics include catalyst preparation, the treatment of waste water and air, biomass and waste valorisation, hydrogen production, oil refining as well as organic synthesis in the presence of heterogeneous and homogeneous catalysts and continuous-flow reactions. With its practical relevance and successful methodologies, this is a valuable guide for chemists at universities working in the field of catalysis, organic synthesis, pharmaceutical or green chemistry, as well as researchers and engineers in the chemical industry.

Microwaves in Organic and Medicinal Chemistry

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Author :
Publisher : John Wiley & Sons
ISBN 13 : 3527606831
Total Pages : 422 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Microwaves in Organic and Medicinal Chemistry by : C. Oliver Kappe

Download or read book Microwaves in Organic and Medicinal Chemistry written by C. Oliver Kappe and published by John Wiley & Sons. This book was released on 2006-05-12 with total page 422 pages. Available in PDF, EPUB and Kindle. Book excerpt: The authors of this guide are experts on the use of microwaves for drug synthesis as well as having much experience in teaching courses held under the auspices of the American Chemical Society and the IUPAC. In this handy source of information for any practicing synthetic chemist they focus on common reaction types in medicinal chemistry, including solid-phase and combinatorial methods. They consider the underlying theory, latest developments in microwave applications and include a variety of examples from recent literature, as well as less common applications that are equally relevant for organic and medicinal chemists. An indispensable reference for researchers with an affinity to modern methods.

Microwave-enhanced Chemistry

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Author :
Publisher :
ISBN 13 :
Total Pages : 808 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Microwave-enhanced Chemistry by : Howard M. Kingston

Download or read book Microwave-enhanced Chemistry written by Howard M. Kingston and published by . This book was released on 1997 with total page 808 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is an indication of the breadth of microwave-enhanced chemistry as a new branch of chemical science. Microwave radiation can be used in many fields of chemistry in addition to sample preparation, decomposition, and extraction. It is now commonly used in the synthesis of organic, organometallic, and inorganic compounds or catalysts. Microwave-assisted sample preparation has become a standard method in thousands of analytical chemical laboratories, and many other chemical manipulations are in the process of standardizing procedures that depend on microwave technology. This book will be helpful to many chemists around the world because it has been constructed to be an international reference text.

Microwave Synthesis

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Publisher :
ISBN 13 :
Total Pages : 300 pages
Book Rating : 4.3/5 (97 download)

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Book Synopsis Microwave Synthesis by : Brittany L. Hayes

Download or read book Microwave Synthesis written by Brittany L. Hayes and published by . This book was released on 2002 with total page 300 pages. Available in PDF, EPUB and Kindle. Book excerpt: 1. Introduction to microwave chemistry 11; 2. Solvents 29; 3. Chemical reactions in the presence and absence of solvent 77; 4. Synthetic applications 95; 5. Getting started with microwave synthesis 157; 6. Microwave safety considerations 175; 7. Microwave hardware 181.

Milestones in Microwave Chemistry

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Publisher : Springer
ISBN 13 : 3319306324
Total Pages : 117 pages
Book Rating : 4.3/5 (193 download)

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Book Synopsis Milestones in Microwave Chemistry by : György Keglevich

Download or read book Milestones in Microwave Chemistry written by György Keglevich and published by Springer. This book was released on 2016-03-22 with total page 117 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book looks back on thirty-five years of microwave (MW) chemistry and explains how the application of the MW technique became an integral part of R&D, eventually becoming recognized in industry. Further, it details how MW chemistry has undergone a dynamic development in the past three decades, one driven by the advent of increasingly sophisticated professional MW reactors in place of the kitchen MW ovens used in earlier years. A major part of the book shows how substitutions, esterifications, amidations, hydrolyses, alkylations, eliminations, dehydrations, condensations, cyclizations, C–C couplings and the modification of heterocycles can be performed advantageously under MW irradiation, as the reaction times are shorter, while the selectivity and yields are higher; it also explains why in most cases, the reactions can be performed under solvent-free conditions. MW irradiation within the sphere of organophosphorus chemistry is showcased and typical reactions, such as the direct derivatization of phosphinic acids, alkylating esterifications, Diels–Alder reactions, the inverse Wittig-type reaction, fragmentations, the Arbuzov reaction, the synthesis of α-hydroxyphosphonates and α-aminophosphonates (the Kabachnik–Fields condensation), deoxygenations and P–C coupling reactions are described under MW conditions. In closing, the advantages of MW chemistry such as faster reactions and the possibility of simplifying the catalytic systems are addressed.

Advances in Microwave Chemistry

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Publisher : CRC Press
ISBN 13 : 1351240471
Total Pages : 438 pages
Book Rating : 4.3/5 (512 download)

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Book Synopsis Advances in Microwave Chemistry by : Bimal K Banik

Download or read book Advances in Microwave Chemistry written by Bimal K Banik and published by CRC Press. This book was released on 2018-12-07 with total page 438 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advances in Microwave Chemistry discusses the novel bond formation methodologies, synergistic effects of microwaves with other entities, sample preparation including digestion, combustion, and extraction techniques, as well as selectivity in chemical processes. Recent updates are provided on microwave-assisted syntheses of pharmacologically significant aza-, oxo- and other heterocycles, including lactams, nucleosides, bile acids and sterols, the preparation of nanomaterials, composites, and absorber layer materials for thin film. This book also incorporates comparative discussions involving microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry. Key Features: Provides a comparative discussion on microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry Presents recent applications of microwave radiation in biocatalysis Offers a complete package correlating various aspects of microwaves in organic syntheses, the biological impact of products formed in reactions, pharmacological features, and environmental sustainability of the procedures Explains microwave-induced reactions on structurally complex bile acids and sterols Stands as a valuable and unique addition to the well-established book series, New Directions in Organic and Biological Chemistry

Dynamics in Microwave Chemistry

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Publisher : Springer Nature
ISBN 13 : 9811596557
Total Pages : 167 pages
Book Rating : 4.8/5 (115 download)

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Book Synopsis Dynamics in Microwave Chemistry by : Kama Huang

Download or read book Dynamics in Microwave Chemistry written by Kama Huang and published by Springer Nature. This book was released on 2021-01-04 with total page 167 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book addresses microwave chemistry at both the physical and molecular level. Its main goal is to elaborate the highly complex scientific issues involved in the fundamental theory of microwave chemistry, and in industrialized applications in the near future.The book provides detailed insights into the characterization and measurement of dielectric properties under complex conditions, such as chemical reactions, high-temperature environments, etc. Considerable attention is paid to the theory of dynamics in microwave chemistry, from the view of both physical level and molecular level. Microwave-Material Interactions simulation is used for physical dynamical analysis, while a Microwave-Molecules Interactions methodology is proposed for molecular dynamical analysis. In turn, calculational examples are introduced for better description and validation, respectively. Lastly, the book proposes design strategies and calculational examples for large-scale application. Richly illustrated and including a wealth of worked-out examples, this book is ideal for all researchers, students and engineers who are just getting started in the dynamics of microwave chemistry.

Advances in Microwave Chemistry

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Author :
Publisher : CRC Press
ISBN 13 : 135124048X
Total Pages : 522 pages
Book Rating : 4.3/5 (512 download)

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Book Synopsis Advances in Microwave Chemistry by : Bimal K Banik

Download or read book Advances in Microwave Chemistry written by Bimal K Banik and published by CRC Press. This book was released on 2018-12-07 with total page 522 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advances in Microwave Chemistry discusses the novel bond formation methodologies, synergistic effects of microwaves with other entities, sample preparation including digestion, combustion, and extraction techniques, as well as selectivity in chemical processes. Recent updates are provided on microwave-assisted syntheses of pharmacologically significant aza-, oxo- and other heterocycles, including lactams, nucleosides, bile acids and sterols, the preparation of nanomaterials, composites, and absorber layer materials for thin film. This book also incorporates comparative discussions involving microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry. Key Features: Provides a comparative discussion on microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry Presents recent applications of microwave radiation in biocatalysis Offers a complete package correlating various aspects of microwaves in organic syntheses, the biological impact of products formed in reactions, pharmacological features, and environmental sustainability of the procedures Explains microwave-induced reactions on structurally complex bile acids and sterols Stands as a valuable and unique addition to the well-established book series, New Directions in Organic and Biological Chemistry

Microwave Chemical and Materials Processing

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Author :
Publisher : Springer
ISBN 13 : 9811064660
Total Pages : 402 pages
Book Rating : 4.8/5 (11 download)

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Book Synopsis Microwave Chemical and Materials Processing by : Satoshi Horikoshi

Download or read book Microwave Chemical and Materials Processing written by Satoshi Horikoshi and published by Springer. This book was released on 2017-11-28 with total page 402 pages. Available in PDF, EPUB and Kindle. Book excerpt: The principal aim of this book is to introduce chemists through a tutorial approach to the use of microwaves by examining several experiments of microwave chemistry and materials processing. It will subsequently enable chemists to fashion their own experiments in microwave chemistry or materials processing. Microwave heating has become a popular methodology in introducing thermal energy in chemical reactions and material processing in laboratory-scale experiments. Several research cases where microwave heating has been used in a wide range of fields have been reported, including organic synthesis, polymers, nanomaterials, biomaterials, and ceramic sintering, among others. In most cases, microwave equipment is used as a simple heat source. Therefore the principal benefits of microwave radiation have seldom been taken advantage of. One reason is the necessity to understand the nature of electromagnetism, microwave engineering, and thermodynamics. However, it is difficult for a chemist to appreciate these in a short time, so they act as barriers for the chemist who might take an interest in the use of microwave radiation. This book helps to overcome these barriers by using figures and diagrams instead of equations as much as possible.

Microwave Methods in Organic Synthesis

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Author :
Publisher : Springer Science & Business Media
ISBN 13 : 3540367578
Total Pages : 297 pages
Book Rating : 4.5/5 (43 download)

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Book Synopsis Microwave Methods in Organic Synthesis by : Mats Larhed

Download or read book Microwave Methods in Organic Synthesis written by Mats Larhed and published by Springer Science & Business Media. This book was released on 2006-10-09 with total page 297 pages. Available in PDF, EPUB and Kindle. Book excerpt: We are delighted to present this volume with contributions from some of the most renowned and experienced microwavechemists today. The delivery and introduction of energy has been closely connected with the discovery and investigation of new chemistry. It is with pleasure that we have seen an increased use of microwave irradiation over the years and we hope that this volume will re?ect the current interest in expanding the scopeofmicrowaveapplicationsinbothorganicandmedicinalchemistry. One important explanation behind the growth of microwave-enhanced chemistry has been the introductionof dedicated microwavereactors. As a result of this development we are proud to present a diverse set of - views. Apart fromchapters spanning the scope that is usually associated with microwavemethods, such as heterocyclic chemistry - an intriguing, but fr- tratingly diverse?eld that is excellently presented in one of the reviews - and transition metal-catalyzed reactions, we also present a review on microwa- assisted natural product chemistry, a topic that is of high interest and neither often nor widely covered. A contribution on microwave-accelerated synt- sis of protease inhibitors underlines the usefulness of microwave heating in medicinal chemistryandareview of?uorousmicrowavechemistryhighlights the importance of the combination of high-speed reactions and quick sepa- tions. Two separate chaptersonscaled-up microwavereactionsandgreen and sustainablechemistrygiveanoverviewofaspectsofmicrowavechemistrythat mightbeofgreatuseinbothindustrialandsmall-scaleapplications. We would like to take this opportunity to express our sincere gratitude to the contributors of this volume for their valuable time and efforts. We believe that the presented workwill further promotethe use of controlledmicrowave heating in both academia and industry.

Catalysis

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Publisher : Royal Society of Chemistry
ISBN 13 : 1839163127
Total Pages : 494 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Catalysis by : James J Spivey

Download or read book Catalysis written by James J Spivey and published by Royal Society of Chemistry. This book was released on 2021-06-14 with total page 494 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume looks at modern approaches to catalysis and reviews the extensive literature. Chapters highlight application of 2D materials in biomass conversion catalysis, plasmonic photocatalysis, catalytic demonstration of mesoporosity in the hierarchical zeolite and the effect of surface phase oxides on supported metals and catalysis. Looking to the future a chapter on ab initio machine learning for accelerating catalytic materials discovery is included. Appealing broadly to researchers in academia and industry, these illustrative chapters bridge the gap from academic studies in the laboratory to practical applications in industry not only for catalysis field but also for environmental protection. Other chapters with an industrial perspective include heterogeneous and homogeneous catalytic routes for vinyl acetate synthesis, catalysis for production of jet fuel from renewable sources by HDO/HDC and microwave-assisted catalysis for fuel conversion. Chemical reactions in ball mills is also explored. The book will be of great benefit to any researcher wanting a succinct reference on developments in this area now and looking to the future.