Hydrothermal Synthesis Of Shape Size Controlled Cerium Based Oxides

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Hydrothermal Synthesis of Shape/size-controlled Cerium-based Oxides

Author : Samuel Itumo Mutinda
Publisher :
ISBN 13 :
Total Pages : 200 pages
Book Rating : 4.:/5 (864 download)

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Book Synopsis Hydrothermal Synthesis of Shape/size-controlled Cerium-based Oxides by : Samuel Itumo Mutinda

Download or read book Hydrothermal Synthesis of Shape/size-controlled Cerium-based Oxides written by Samuel Itumo Mutinda and published by . This book was released on 2013 with total page 200 pages. Available in PDF, EPUB and Kindle. Book excerpt: A low energy band gap between Ce3+ and Ce4+ states in cerium oxide along with its high oxygen mobility and high oxygen storage capacity are properties that qualify it as one of the most widely used heterogeneous catalysts and catalyst oxide supports. This thesis report is an account of studies that were carried out on the synthesis and catalytic properties of pure, metal-doped and noble-metal impregnated cerium oxide nanoparticles. Our results revealed that synthesis temperature, during hydrothermal reactions, plays a critical role in controlling the shape, size, oxygen vacancy concentration, and low temperature reducibility in CeO2 nanoparticles. In addition, OH− ion concentration was found to play an important role in engineering the lattice constants and oxygen vacancy concentrations of ceria nanoparticles within the same particle morphology and synthesis temperature. Secondly, our studies demonstrated that hydrothermal synthesis is a facile one-step approach to the preparation of compositionally homogeneous Ce[subscript x]Zr[subscript 1-x]O2 (0≤x≤1) nanocrystals, in which CeO2-ZrO2 mixed oxides present a superior low-temperature oxygen release capability compared to pure CeO2. The Ce[subscript 0.5]Zr[subscript 0.5]O2 system proved to have good thermal stability up to 1000°C under reducing and oxidizing atmosphere. We have also seen that at above 1000°C, phase transformation occurs from psudocubic to cation ordered pyrochlore or tetragonal phase under reducing and oxidizing atmosphere, respectively. This method may be easily extended to other cerium-based mixed oxides or synthesis of analogous mixed oxides. Lastly, our results established that the impregnation of 1 wt. % platinum and gold on CeO2 nanorods and on nanocubes causes an enhanced reduction on their surface reduction temperatures with negligible effect on their bulk reducibility. It was also shown that both pure and impregnated CeO2 nanorods have a lower surface reduction temperature compared to that of pure and impregnated CeO2 nanocubes. We have also demonstrated that gold nanoparticles proved to have a higher catalytic performance in oxidizing molecular hydrogen at low temperatures as compared to platinum nanoparticles.

Nanomaterials in Biomass Conversion

Author : Komal Rizwan
Publisher : Elsevier
ISBN 13 : 0443135010
Total Pages : 534 pages
Book Rating : 4.4/5 (431 download)

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Book Synopsis Nanomaterials in Biomass Conversion by : Komal Rizwan

Download or read book Nanomaterials in Biomass Conversion written by Komal Rizwan and published by Elsevier. This book was released on 2024-03-01 with total page 534 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanomaterials in Biomass Conversion: Advances and Applications for Bioenergy, Biofuels and Bio-based Products critically reviews the basic principles through to the latest advances in the emerging field of nanotechnology for the production of biofuels and bioenergy. Divided into 3 parts, the first five chapters explain the fundamentals of nanomaterials, their properties, characterization, and basic processes for synthesis. Part 2, which constitutes the majority of the book, reviews the various methods and technologies for the conversion of biomass to bioenergy, biofuels, and value-added products using nanomaterials. This includes homogeneous and heterogeneous nano-catalytic systems, nano-photocatalytic conversion, nanomaterial-assisted anaerobic digestion, nanoparticles-immobilized enzymes conversion, the production of biogas, volatile fatty acids, and value-added products, and in carbon capture and conversion to sustainable energy products, as well as the potential of nano-biochar, nano-cellulose, and other nanomaterials in microbial fuel cells, bioelectrochemical systems, and batteries. Finally, Part 3 addresses the techno-economics and financial viability in the context of the circular economy, risk related to toxicology, stability, and environmental impacts, and considers the various challenges and future opportunities of biomass conversion through nanomaterials. Nanomaterials in Biomass Conversion is an invaluable resource for researchers and engineers involved in the production of bioenergy, biofuel, and bioproducts, and will also be of benefit to those interested in environmental remediation, pollution management, and cleaner energy production. Critically examines the role of nanomaterials in the management of waste biomass as applied to bioenergy and biofuels Explains various nanotechnological methods for the conversion of waste biomass into value-added products Discusses the basic principles, operational aspects, ongoing developments, and future perspectives related to the applications of nanotechnologies and nanomaterials in biomass conversion Provides solutions to the key challenges of nanotechnologies and nanomaterials in the conversion of biomass, along with future challenges and risks

Engineered Nanomaterials and Phytonanotechnology: Challenges for Plant Sustainability

Author : Ashok Kumar Das
Publisher :
ISBN 13 : 0128213205
Total Pages : 342 pages
Book Rating : 4.1/5 (282 download)

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Book Synopsis Engineered Nanomaterials and Phytonanotechnology: Challenges for Plant Sustainability by : Ashok Kumar Das

Download or read book Engineered Nanomaterials and Phytonanotechnology: Challenges for Plant Sustainability written by Ashok Kumar Das and published by . This book was released on 2019-11-27 with total page 342 pages. Available in PDF, EPUB and Kindle. Book excerpt: Engineered Nanomaterials and Phytonanotechnology: Challenges for Plant Sustainability, Volume 87 in the Comprehensive Analytical Chemistry series, highlights new advances in the field, with this new volume presenting interesting chapters on the Current status of environmental monitoring, Physical principles of infrared, Chemical principles of infrared, Instrumentation and hardware, Data analysis, Sampling, Applications in water, Application in soil and sediments, Applications in ecology of animals and plants, Applications in air monitoring, Applications in contamination, Applications in marine environments, Advantages and pitfalls, and more. Provides the authority and expertise of leading contributors from an international board of authors Presents the latest release in the Comprehensive Analytical Chemistry series Updated release includes the latest information on the field of engineered nanomaterials in plants

Functionalized Nanomaterials

Author : Muhammad Akhyar Farrukh
Publisher : BoD – Books on Demand
ISBN 13 : 9535128558
Total Pages : 176 pages
Book Rating : 4.5/5 (351 download)

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Book Synopsis Functionalized Nanomaterials by : Muhammad Akhyar Farrukh

Download or read book Functionalized Nanomaterials written by Muhammad Akhyar Farrukh and published by BoD – Books on Demand. This book was released on 2016-12-28 with total page 176 pages. Available in PDF, EPUB and Kindle. Book excerpt: Generally the nanometer scale covers from 1 to 100 nm while discussing the nanomaterials. Nanomaterials have very high potency and emerge with large applications piercing through all the discipline of knowledge, leading to industrial and technological growth. Nanotechnology is a multidisciplinary science that has its roots in fields such as colloidal science, device physics, and biomedical and supramolecular chemistry. The main objective of the book is to cover maximum areas focusing on synthesis, characterization with various microscopic techniques, and multiple applications. This book is divided into two sections with Non-carbon Compounds and Carbon Compounds. The synthesis, characterization, and applications of metal, metal oxides, and metal hydroxide nanoparticles are covered in the section Non-carbon Compounds, while the section Carbon Compounds focuses on the carbon nanotubes, graphite oxide, graphene oxide, etc.

Synthesis and Support Shape Effects on the Catalytic Activities of CuO[subscript X]/CeO2 Nanomaterials

Author : Elizabeth Theresa Zell
Publisher :
ISBN 13 :
Total Pages : 398 pages
Book Rating : 4.:/5 (15 download)

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Book Synopsis Synthesis and Support Shape Effects on the Catalytic Activities of CuO[subscript X]/CeO2 Nanomaterials by : Elizabeth Theresa Zell

Download or read book Synthesis and Support Shape Effects on the Catalytic Activities of CuO[subscript X]/CeO2 Nanomaterials written by Elizabeth Theresa Zell and published by . This book was released on 2018 with total page 398 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this dissertation, the research focused on the preparation of shape-controlled cerium oxide (CeO2), a known active catalyst support, to investigate the structure-property relationship for CO oxidation reaction. The use of surfactants during synthesis of shape-controlled oxide supports can have an adverse effect on the catalytic activity. Thus, CeO2 of different morphologies (nanorods, nanocubes, and nano-octahedra) were synthesized using a hydrothermal method without an addition of surfactants in the solution. Since the size has a strong effect on differences in geometric and/or electronic properties of catalyst supports effects on the adsorption and activation of CO (carbon monoxide) and molecular oxygen are also known to take place. We strive to understand if there is a correlation with the nano-catalyst's shapes with different termination planes and the catalytic activity. Furthermore, the research focused on the impregnation of cost-effective metal catalysts with a higher known abundance on the planet. The different morphologies of CeO2 supports were impregnated with copper oxide (CuO) at varying wt.% (1, 5 and 10 wt.%) using a wet incipient method. The samples were oxidized and reduced in order to garner a better understanding of the reducibility effect. The catalysts were then investigated to correlate the increased catalytic activities with the various shapes and defects. CuO/CeO2 and CuOx/CeO2 were characterized using Raman spectroscopy, X-ray Photoelectron Spectroscopy (XPS), X-ray Diffraction (XRD) and Transmission Electron Microscopy (TEM). The catalytic activities were measured using Temperature Programmed Reduction (TPR), Temperature Programmed Oxidation (TPO), Temperature Programmed Desorption (TPD), and CO oxidation reaction. The results showed that CeO2 nanorods were the superior shape regarding enhancing the catalytic v activity due to its increased surface area and surface defects. CuO catalyst impregnated on CeO2 nanorods with increased surface defects demonstrated improved CO oxidation and low reduction temperatures. Additionally, a systematic study of various bimetal oxides and bimetallic nano-catalysts (Fe-CuO, Ni-CuO, Mn-CuO and Ag-CuO[subscript x]) impregnated on shape-controlled CeO2 was investigated to understand the effects of the binary catalyst system on the catalytic efficiencies. This was done while keeping copper as one of the binary metal catalysts, since CuO catalysts showed enhanced catalytic activity. The collected data determined that each of the bimetallic catalyst systems showed an improvement in catalytic activity and an enhancement of the stability as compared to CuO/CeO2 catalysts. To make an in-depth investigation of the interfacial interaction and structure of the CuO[subscript x]/CeO2, TEM and HRTEM techniques were to characterize CuO[subscript x]/CeO2 nanorods. The H2-TPR profiles were re-evaluated and offered information on the possible structural analysis as well as indicating reduction temperatures.

Cerium Oxide (CeO2): Synthesis, Properties and Applications

Author : Salvatore Scire
Publisher : Elsevier
ISBN 13 : 0128156627
Total Pages : 402 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Cerium Oxide (CeO2): Synthesis, Properties and Applications by : Salvatore Scire

Download or read book Cerium Oxide (CeO2): Synthesis, Properties and Applications written by Salvatore Scire and published by Elsevier. This book was released on 2019-08-21 with total page 402 pages. Available in PDF, EPUB and Kindle. Book excerpt: Cerium Oxide (CeO2): Synthesis, Properties and Applications provides an updated and comprehensive account of the research in the field of cerium oxide based materials. The book is divided into three main blocks that deal with its properties, synthesis and applications. Special attention is devoted to the growing number of applications of ceria based materials, including their usage in industrial and environmental catalysis and photocatalysis, energy production and storage, sensors, cosmetics, radioprotection, glass technology, pigments, stainless steel and toxicology. A brief historical introduction gives users background, and a final chapter addresses future perspectives and outlooks to stimulate future research. The book is intended for a wide audience, including students, academics and industrial researchers working in materials science, chemistry and physics. Addresses a wide range of applications of ceria-based materials, including catalysis, energy production and storage, sensors, cosmetics and toxicology Provides the fundamentals of ceria-based materials, including synthesis methods, materials properties, toxicology and surface chemistry Includes nanostructured ceria-based materials and a discussion of future prospects and outlooks

Catalysis by Ceria and Related Materials

Author : Alessandro Trovarelli
Publisher : World Scientific
ISBN 13 : 1848169647
Total Pages : 909 pages
Book Rating : 4.8/5 (481 download)

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Book Synopsis Catalysis by Ceria and Related Materials by : Alessandro Trovarelli

Download or read book Catalysis by Ceria and Related Materials written by Alessandro Trovarelli and published by World Scientific. This book was released on 2013 with total page 909 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book follows the 2002 edition of Catalysis by Ceria and Related Materials, which was the first book entirely devoted to ceria and its catalytic properties. In the ten years since the first edition a massive amount of work has been carried out in the field, and ceria has gained a prominent position in catalysis as one of the most valuable material for several applications. This second edition covers fundamental and applied aspects of the latest advances in ceria-based materials with a special focus on structural, redox and catalytic features. Special emphasis is given to nano-engineered and nano-shaped systems which are a key factor in the predictive and rational design of ceria with novel properties.In addition, the book presents recent advances in emerging and traditional large-scale applications of ceria in catalysis, such as the treatment of emissions from mobile sources (including diesel and gasoline engines). The primary readership includes catalysis and material science researchers from academy and industry and postdoctorate and graduate students in chemistry, chemical engineering and physics.

Binary Rare Earth Oxides

Author : G. Adachi
Publisher : Springer Science & Business Media
ISBN 13 : 9781402025686
Total Pages : 278 pages
Book Rating : 4.0/5 (256 download)

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Book Synopsis Binary Rare Earth Oxides by : G. Adachi

Download or read book Binary Rare Earth Oxides written by G. Adachi and published by Springer Science & Business Media. This book was released on 2004-09 with total page 278 pages. Available in PDF, EPUB and Kindle. Book excerpt: Binary Rare Earth Oxides is the first book in the field of rare earth oxides that provides coverage from the basic science through to recent advances. This book introduces the unique characteristics of the binary rare earth oxides with their chemistry, physics and applications. It provides a comprehensive review of all the characteristics of rare earth oxides, essential for scientists and engineers involved with rare earths, oxides, inorganic materials, ceramics, and structures. The binary rare earth oxides bring us a variety of interesting characteristics. Understanding their fundamental mechanisms builds a bridge between solid-state chemistry and materials science. The book begins with a brief introduction to binary rare earth oxides, their physical and chemical stabilities, polymorphism, crystal structures and phase transformation and the association with current applications. The book goes on to present the band structure of the oxides using several quantum chemical calculations, which belong to a newly developed area in the binary rare earth oxides. Central to this chapter are the characterizations of electrical, magnetic and optical properties, as well as details of single crystal growth and particle preparation methods that have progressed in recent years. Later chapters concentrate on thermo-chemical properties and trace determination techniques. The final chapter contains a variety of useful applications in various fields such as phosphors, glass abrasives, automotive catalysts, fuel cells, solid electrolytes, sunscreens, iron steels, and biological materials. This book is an invaluable resource for materials scientists and solid-state physicists and chemists with an interest in rare earth oxides, as well as advanced students and graduates who require an approach to familiarize them with this field. This book provides guidance through a comprehensive review of all the characteristics of binary rare earth oxides.

Doped-Ceria Electrolytes

Author : Luca Spiridigliozzi
Publisher : Springer
ISBN 13 : 331999395X
Total Pages : 85 pages
Book Rating : 4.3/5 (199 download)

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Book Synopsis Doped-Ceria Electrolytes by : Luca Spiridigliozzi

Download or read book Doped-Ceria Electrolytes written by Luca Spiridigliozzi and published by Springer. This book was released on 2018-08-16 with total page 85 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides an overview of fuel cell technology and, in particular, of Solid Oxide Electrolysis Cells (SOFCs). Each chapter highlights the effects of different synthesis parameters and/or adopted sintering method, clarifying both advantages and disadvantages pointed out by different experimental campaigns. The book focuses on Doped-Ceria Electrolytes, presenting an engineered production process of GDC/SDC electrolytes by using a combination of wet chemical synthesis and/or alternative sintering techniques, capable of enhancing electrolytes microstructural features and electrical properties at reduced temperature and time. The author proposes useful guidelines to produce dense and high-preforming ceria-based electrolytes for IT-SOFCs.

Nanocatalysts

Author : Indrajit Sinha
Publisher : BoD – Books on Demand
ISBN 13 : 1789841593
Total Pages : 170 pages
Book Rating : 4.7/5 (898 download)

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Book Synopsis Nanocatalysts by : Indrajit Sinha

Download or read book Nanocatalysts written by Indrajit Sinha and published by BoD – Books on Demand. This book was released on 2019-07-31 with total page 170 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanocatalysis is a topical area of research that has huge potential. It attempts to merge the advantages of heterogeneous and homogeneous catalysis. The collection of articles in this book treats the topics of specificity, activity, reusability, and stability of the catalyst and presents a compilation of articles that focuses on different aspects of these issues.

Cerium-Based Materials: Synthesis, Properties and Applications

Author : Ramesh Chandra
Publisher : Bentham Science Publishers
ISBN 13 : 9815080091
Total Pages : 127 pages
Book Rating : 4.8/5 (15 download)

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Book Synopsis Cerium-Based Materials: Synthesis, Properties and Applications by : Ramesh Chandra

Download or read book Cerium-Based Materials: Synthesis, Properties and Applications written by Ramesh Chandra and published by Bentham Science Publishers. This book was released on 2023-05-23 with total page 127 pages. Available in PDF, EPUB and Kindle. Book excerpt: Cerium is the most abundant metal of rare-earth elements. It can be used to make materials such as phosphors and alloys, that have applications in various applied fields (like electronics, magnetics and heterogeneous catalysis) and devices (like catalytic converters and gas mantles). Cerium-Based Materials: Synthesis, Properties and Applications presents detailed knowledge about cerium materials. Starting with the history of cerium-based materials, it gives an introduction to the synthesis of chemicals like cerium oxides and composites. This is followed by information about characterization of cerium nanoparticles and industrial applications of cerium-based materials, with a focus on catalysis, biomedical engineering and pharmaceutical chemistry. This book is an essential reference for researchers and chemical engineers who want a summary of cerium materials and its applications.

Hydrothermal Synthesis of Cerium-containing Oxides for Use in Catalysis

Author : Christopher Stuart Wright
Publisher :
ISBN 13 :
Total Pages : 0 pages
Book Rating : 4.:/5 (142 download)

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Book Synopsis Hydrothermal Synthesis of Cerium-containing Oxides for Use in Catalysis by : Christopher Stuart Wright

Download or read book Hydrothermal Synthesis of Cerium-containing Oxides for Use in Catalysis written by Christopher Stuart Wright and published by . This book was released on 2006 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:

3rd International Multidisciplinary Microscopy and Microanalysis Congress (InterM)

Author : Ahmet Yavuz Oral
Publisher : Springer
ISBN 13 : 3319466011
Total Pages : 258 pages
Book Rating : 4.3/5 (194 download)

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Book Synopsis 3rd International Multidisciplinary Microscopy and Microanalysis Congress (InterM) by : Ahmet Yavuz Oral

Download or read book 3rd International Multidisciplinary Microscopy and Microanalysis Congress (InterM) written by Ahmet Yavuz Oral and published by Springer. This book was released on 2016-11-09 with total page 258 pages. Available in PDF, EPUB and Kindle. Book excerpt: The 3rd International Multidisciplinary Microscopy Congress (InterM2015), held from 19 to 23 October 2015, focused on the latest developments concerning applications of microscopy in the biological, physical and chemical sciences at all dimensional scales, advances in instrumentation, techniques in and educational materials on microscopy. These proceedings gather 17 peer-reviewed technical papers submitted by leading academic and research institutions from nine countries and representing some of the most cutting-edge research available.

Nanocatalysis

Author : Ulrich Heiz
Publisher : Springer Science & Business Media
ISBN 13 : 3540326464
Total Pages : 514 pages
Book Rating : 4.5/5 (43 download)

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Book Synopsis Nanocatalysis by : Ulrich Heiz

Download or read book Nanocatalysis written by Ulrich Heiz and published by Springer Science & Business Media. This book was released on 2007-01-10 with total page 514 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanocatalysis, a subdiscipline of nanoscience, seeks to control chemical reactions by changing the size, dimensionality, chemical composition, and morphology of the reaction center and by changing the kinetics using nanopatterning of the reaction center. This book offers a detailed pedagogical and methodological overview of the field. Readers discover many examples of current research, helping them explore new and emerging applications.

Synthesis of Lanthanide and Actinide Compounds

Author : G. Meyer
Publisher : Springer Science & Business Media
ISBN 13 : 9401137587
Total Pages : 377 pages
Book Rating : 4.4/5 (11 download)

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Book Synopsis Synthesis of Lanthanide and Actinide Compounds by : G. Meyer

Download or read book Synthesis of Lanthanide and Actinide Compounds written by G. Meyer and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 377 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Nanocasting

Author : An-Hui Lu
Publisher : Royal Society of Chemistry
ISBN 13 : 0854041885
Total Pages : 279 pages
Book Rating : 4.8/5 (54 download)

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Book Synopsis Nanocasting by : An-Hui Lu

Download or read book Nanocasting written by An-Hui Lu and published by Royal Society of Chemistry. This book was released on 2010 with total page 279 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanostructured materials with tailored properties are regarded as a fundamental element in the development of future science and technology. Research is still ongoing into the nanosized construction elements required to create functional solids. The recently developed technique, nanocasting, has great advantage over others in terms of the synthesis of special nanostructured materials by the careful choice of suitable elements and nanoengineering steps. This new book summarizes the recent developments in nanocasting, including the principles of nanocasting, syntheses of novel nanostructured materials, characterization methods, detailed synthetic recipes and further possible development in this area. The book focuses on the synthesis of porous solids from the viewpoint of methodology and introduces the science of nanocasting from fundamental principles to their use in synthesis of various materials. It starts by outlining the principles of nanocasting, requirements to the templates and precursors and the tools needed to probe matter at the nanoscale level. It describes how to synthesize nano structured porous solids with defined characteristics and finally discusses the functionalization and application of porous solids. Special attention is given to new developments in this field and future perspectives. A useful appendix covering the detailed synthetic recipes of various templates including porous silica, porous carbon and colloidal spheres is included which will be invaluable to researchers wanting to follow and reproduce nanocast materials. Topics covered in the book include: * inorganic chemistry * organic chemistry * solution chemistry * sol-gel and interface science * acid-base equilibria * electrochemistry * biochemistry * confined synthesis The book gives readers not only an overview of nanocasting technology, but also sufficient information and knowledge for those wanting to prepare various nanostructured materials without needing to search the available literature.

Cerium Oxide

Author : Sher Bahadar Khan
Publisher : BoD – Books on Demand
ISBN 13 : 1789850231
Total Pages : 123 pages
Book Rating : 4.7/5 (898 download)

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Book Synopsis Cerium Oxide by : Sher Bahadar Khan

Download or read book Cerium Oxide written by Sher Bahadar Khan and published by BoD – Books on Demand. This book was released on 2019-01-23 with total page 123 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book focuses on the chemical structure and applications of CeO2. It covers the recent developments in a wide range of CeO2 applications, particularly catalysis corrosion protection, fuel cells, sensors, and UV-blocking. It also provides a concise but thorough coverage of the chemical structure and applications of CeO2. Thus, this book provides an overview of chemical structure, applications, and recent attributes of CeO2 for a broad audience, including beginners, graduate students, and specialists in both academic and industrial sectors.