Hydrogenation of the Alpha, Beta-Unsaturated Aldehydes Acrolein, Crotonaldehyde, and Prenal Over Pt Single Crystals

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ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (16 download)

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Book Synopsis Hydrogenation of the Alpha, Beta-Unsaturated Aldehydes Acrolein, Crotonaldehyde, and Prenal Over Pt Single Crystals by :

Download or read book Hydrogenation of the Alpha, Beta-Unsaturated Aldehydes Acrolein, Crotonaldehyde, and Prenal Over Pt Single Crystals written by and published by . This book was released on 2008 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Sum-frequency generation vibrational spectroscopy (SFG-VS) and kinetic measurements using gas chromatography have been used to study the surface reaction intermediates during the hydrogenation of three?,?-unsaturated aldehydes, acrolein, crotonaldehyde, and prenal, over Pt(111) at Torr pressures (1 Torr aldehyde, 100 Torr hydrogen) in the temperature range of 295K to 415K. SFG-VS data showed that acrolein has mixed adsorption species of?2-di-?(CC)-trans,?2-di-?(CC)-cis as well as highly coordinated?3 or?4 species. Crotonaldehyde adsorbed to Pt(111) as?2 surface intermediates. SFG-VS during prenal hydrogenation also suggested the presence of the?2 adsorption species, and became more highly coordinated as the temperature was raised to 415K, in agreement with its enhanced C=O hydrogenation. The effect of catalyst surface structure was clarified by carrying out the hydrogenation of crotonaldehyde over both Pt(111) and Pt(100) single crystals while acquiring the SFG-VS spectra in situ. Both the kinetics and SFG-VS showed little structure sensitivity. Pt(100) generated more decarbonylation 'cracking' product while Pt(111) had a higher selectivity for the formation of the desired unsaturated alcohol, crotylalcohol.

Hydrogenation

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Publisher : Walter de Gruyter GmbH & Co KG
ISBN 13 : 3110545217
Total Pages : 204 pages
Book Rating : 4.1/5 (15 download)

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Book Synopsis Hydrogenation by : S. David Jackson

Download or read book Hydrogenation written by S. David Jackson and published by Walter de Gruyter GmbH & Co KG. This book was released on 2018-09-24 with total page 204 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book gives a comprehensive overview of modern hydrogenation methods used in organic synthesis. In clearly structured chapters, the authors cover the catalysts, scope and limitations of their application, and the techniques for hydrogenation of carbon-carbon, carbon-heteroatom and heteroatom-heteroatom multiple bonds.

In-situ Studies of the Reactions of Bifunctional and Heterocyclic Molecules Over Noble Metal Single Crystal and Nanoparticle Catalysts Studied with Kinetics and Sum-Frequency Generation Vibrational Spectroscopy

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Total Pages : pages
Book Rating : 4.:/5 (893 download)

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Book Synopsis In-situ Studies of the Reactions of Bifunctional and Heterocyclic Molecules Over Noble Metal Single Crystal and Nanoparticle Catalysts Studied with Kinetics and Sum-Frequency Generation Vibrational Spectroscopy by :

Download or read book In-situ Studies of the Reactions of Bifunctional and Heterocyclic Molecules Over Noble Metal Single Crystal and Nanoparticle Catalysts Studied with Kinetics and Sum-Frequency Generation Vibrational Spectroscopy written by and published by . This book was released on 2009 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Sum frequency generation surface vibrational spectroscopy (SFG-VS) in combination with gas chromatography (GC) was used in-situ to monitor surface bound reaction intermediates and reaction selectivities for the hydrogenation reactions of pyrrole, furan, pyridine, acrolein, crotonaldehyde, and prenal over Pt(111), Pt(100), Rh(111), and platinum nanoparticles under Torr reactant pressures and temperatures of 300K to 450K. The focus of this work is the correlation between the SFG-VS observed surface bound reaction intermediates and adsorption modes with the reaction selectivity, and how this is affected by catalyst structure and temperature. Pyrrole hydrogenation was investigated over Pt(111) and Rh(111) single crystals at Torr pressures. It was found that pyrrole adsorbs to Pt(111) perpendicularly by cleaving the N-H bond and binding through the nitrogen. However, over Rh(111) pyrrole adsorbs in a tilted geometry binding through the [pi]-aromatic orbitals. A surface-bound pyrroline reaction intermediate was detected over both surfaces with SFG-VS. It was found that the ring-cracking product butylamine is a reaction poison over both surfaces studied. Furan hydrogenation was studied over Pt(111), Pt(100), 10 nm cubic platinum nanoparticles and 1 nm platinum nanoparticles. The product distribution was observed to be highly structure sensitive and the acquired SFG-VS spectra reflected this sensitivity. Pt(100) exhibited more ring-cracking to form butanol than Pt(111), while the nanoparticles yielded higher selectivities for the partially saturated ring dihydrofuran. Pyridine hydrogenation was investigated over Pt(111) and Pt(100). The [alpha]-pyridyl surface adsorption mode was observed with SFG-VS over both surfaces. 1,4-dihydropyridine was seen as a surface intermediate over Pt(100) but not Pt(111). Upon heating the surfaces to 350K, the adsorbed pyridine changes to a flat-lying adsorption mode. No evidence was found for the pyridinium cation. The hydrogenation of the [alpha], [beta]-unsaturated aldehydes acrolein, crotonaldehyde, and prenal were investigated over Pt(111) and Pt(100). The selectivity for the hydrogenation of the C=C bond was found to depend on the number of methyl groups added to the bond. The adsorption modes of the three aldehydes were determined. The hydrogenation of crotonaldehyde was found to be nearly structure insensitive as the TOF and selectivity were very close to the same over Pt(111) and Pt(100). SFG-VS indicated identical surface intermediates over the two crystal faces during crotonaldehyde hydrogenation.

Advances in Catalysis

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Publisher : Academic Press
ISBN 13 : 0124202330
Total Pages : 401 pages
Book Rating : 4.1/5 (242 download)

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Book Synopsis Advances in Catalysis by :

Download or read book Advances in Catalysis written by and published by Academic Press. This book was released on 2013-11-28 with total page 401 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advances in Catalysis fills the gap between the journal papers and the textbooks across the diverse areas of catalysis research. For more than 60 years Advances in Catalysis has been dedicated to recording progress in the field of catalysis and providing the scientific community with comprehensive and authoritative reviews. This series in invaluable to chemical engineers, physical chemists, biochemists, researchers and industrial chemists working in the fields of catalysis and materials chemistry. In-depth, critical, state-of-the-art reviews Comprehensive, covers of all aspects of catalysis research

Heterogeneous Catalysis in Organic Transformations

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Publisher : CRC Press
ISBN 13 : 100055550X
Total Pages : 214 pages
Book Rating : 4.0/5 (5 download)

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Book Synopsis Heterogeneous Catalysis in Organic Transformations by : Varun Rawat

Download or read book Heterogeneous Catalysis in Organic Transformations written by Varun Rawat and published by CRC Press. This book was released on 2022-04-26 with total page 214 pages. Available in PDF, EPUB and Kindle. Book excerpt: As the broad challenges around energy and the environment have become the focus of much research, scientists and experts have dedicated their efforts to developing more active and selective catalytic systems for key chemical transformations. For many decades environmentally viable protocols for the synthesis of fine chemicals have been the crux of academic and industrial research. Heterogeneous Catalysis in Organic Transformations serves as an overview of this work, providing a complete description of role of heterogeneous catalysis in organic transformations and offering a review of the current and near future technologies and applications. Discusses the fundamentals of catalysis and compares the advantages and disadvantages of different types of catalyst systems Examines oxide nanoparticles and noble metal nanoparticles Consider organometallic compounds, solid-supported catalysts, and mesoporous materials Describes recent advances in metal-based heterogeneous catalysts and new reactions with possible mechanistic pathways Providing a comprehensive review of heterogeneous catalysis from the basics through recent advances, this book will be of keen interest to undergraduates, graduates, and researchers in chemistry, chemical engineering, and associated fields.

Phenolic Resins: A Century of Progress

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Publisher : Springer Science & Business Media
ISBN 13 : 3642047149
Total Pages : 543 pages
Book Rating : 4.6/5 (42 download)

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Book Synopsis Phenolic Resins: A Century of Progress by : Louis Pilato

Download or read book Phenolic Resins: A Century of Progress written by Louis Pilato and published by Springer Science & Business Media. This book was released on 2010-03-10 with total page 543 pages. Available in PDF, EPUB and Kindle. Book excerpt: The legacy of Leo Hendrik Baekeland and his development of phenol formal- hyde resins are recognized as the cornerstone of the Plastics Industry in the early twentieth century, and phenolic resins continue to ?ourish after a century of robust growth. On July 13, 1907, Baekeland ?led his “heat and pressure” patent related to the processing of phenol formaldehyde resins and identi?ed their unique utility in a plethora of applications. The year 2010 marks the Centennial Year of the prod- tion of phenolic resins by Leo Baekeland. In 1910, Baekeland formed Bakelite GmbH and launched the manufacture of phenolic resins in Erkner in May 1910. In October 1910, General Bakelite began producing resins in Perth Amboy, New Jersey. Lastly, Baekeland collaborated with Dr. Takamine to manufacture phenolic resins in Japan in 1911. These events were instrumental in establishing the Plastics Industry and in tracing the identity to the brilliance of Dr. Leo Baekeland. Phenolic resins remain as a versatile resin system featuring either a stable, thermoplastic novolak composition that cures with a latent source of formaldehyde (hexa) or a heat reactive and perishable resole composition that cures thermally or under acidic or special basic conditions. Phenolic resins are a very large volume resin system with a worldwide volume in excess of 5 million tons/year, and its growth is related to the gross national product (GNP) growth rate globally.

Deep Nutrition

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Publisher : Macmillan
ISBN 13 : 1250113822
Total Pages : 512 pages
Book Rating : 4.2/5 (51 download)

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Book Synopsis Deep Nutrition by : Catherine Shanahan, M.D.

Download or read book Deep Nutrition written by Catherine Shanahan, M.D. and published by Macmillan. This book was released on 2017-01-03 with total page 512 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Shanahan examined diets around the world known to help people live longer, healthier lives--diets like the Mediterranean, Okinawa, and 'Blue Zone'--and identified the four common nutritional habits, developed over millennia, that unfailingly produce strong, healthy, intelligent children, and active, vital elders, generation after generation. Dr. Cate shows how all calories are not created equal; food is information that directs our cellular growth. Our family history does not determine our destiny: what you eat and how you live can alter your DNA in ways that affect your health and the health of your future children. She offers a prescriptive plan for how anyone can begin eating The Human Diet."--

XAFS Techniques for Catalysts, Nanomaterials, and Surfaces

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Publisher : Springer
ISBN 13 : 3319438662
Total Pages : 545 pages
Book Rating : 4.3/5 (194 download)

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Book Synopsis XAFS Techniques for Catalysts, Nanomaterials, and Surfaces by : Yasuhiro Iwasawa

Download or read book XAFS Techniques for Catalysts, Nanomaterials, and Surfaces written by Yasuhiro Iwasawa and published by Springer. This book was released on 2016-10-19 with total page 545 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is a comprehensive, theoretical, practical, and thorough guide to XAFS spectroscopy. The book addresses XAFS fundamentals such as experiments, theory and data analysis, advanced XAFS methods such as operando XAFS, time-resolved XAFS, spatially resolved XAFS, total-reflection XAFS, high energy resolution XAFS, and practical applications to a variety of catalysts, nanomaterials and surfaces. This book is accessible to a broad audience in academia and industry, and will be a useful guide for researchers entering the subject and graduate students in a wide variety of disciplines.

Comprehensive Inorganic Chemistry II

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Publisher : Newnes
ISBN 13 : 0080965296
Total Pages : 7694 pages
Book Rating : 4.0/5 (89 download)

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Book Synopsis Comprehensive Inorganic Chemistry II by :

Download or read book Comprehensive Inorganic Chemistry II written by and published by Newnes. This book was released on 2013-07-23 with total page 7694 pages. Available in PDF, EPUB and Kindle. Book excerpt: Comprehensive Inorganic Chemistry II, Nine Volume Set reviews and examines topics of relevance to today’s inorganic chemists. Covering more interdisciplinary and high impact areas, Comprehensive Inorganic Chemistry II includes biological inorganic chemistry, solid state chemistry, materials chemistry, and nanoscience. The work is designed to follow on, with a different viewpoint and format, from our 1973 work, Comprehensive Inorganic Chemistry, edited by Bailar, Emeléus, Nyholm, and Trotman-Dickenson, which has received over 2,000 citations. The new work will also complement other recent Elsevier works in this area, Comprehensive Coordination Chemistry and Comprehensive Organometallic Chemistry, to form a trio of works covering the whole of modern inorganic chemistry. Chapters are designed to provide a valuable, long-standing scientific resource for both advanced students new to an area and researchers who need further background or answers to a particular problem on the elements, their compounds, or applications. Chapters are written by teams of leading experts, under the guidance of the Volume Editors and the Editors-in-Chief. The articles are written at a level that allows undergraduate students to understand the material, while providing active researchers with a ready reference resource for information in the field. The chapters will not provide basic data on the elements, which is available from many sources (and the original work), but instead concentrate on applications of the elements and their compounds. Provides a comprehensive review which serves to put many advances in perspective and allows the reader to make connections to related fields, such as: biological inorganic chemistry, materials chemistry, solid state chemistry and nanoscience Inorganic chemistry is rapidly developing, which brings about the need for a reference resource such as this that summarise recent developments and simultaneously provide background information Forms the new definitive source for researchers interested in elements and their applications; completely replacing the highly cited first edition, which published in 1973

Protected Metal Clusters: From Fundamentals to Applications

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Publisher : Elsevier
ISBN 13 : 0444635025
Total Pages : 394 pages
Book Rating : 4.4/5 (446 download)

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Book Synopsis Protected Metal Clusters: From Fundamentals to Applications by :

Download or read book Protected Metal Clusters: From Fundamentals to Applications written by and published by Elsevier. This book was released on 2015-09-06 with total page 394 pages. Available in PDF, EPUB and Kindle. Book excerpt: Protected Metal Clusters: From Fundamentals to Applications surveys the fundamental concepts and potential applications of atomically precise metal clusters protected by organic ligands. As this class of materials is now emerging as a result of breakthroughs in synthesis and characterization that have taken place over the last few years, the book provides the first reference with a focus on these exciting novel nanomaterials, explaining their formation, and how, and why, they play an important role in the future of molecular electronics, catalysis, sensing, biological imaging, and medical diagnosis and therapy. Surveys the fundamental concepts and potential applications of atomically precise metal clusters protected by organic ligands. Provides well-organized, tutorial style chapters that are ideal for teaching and self-study In-depth descriptions by top scientists in the field Presents the state-of-the art of protected metal clusters and their future prospects

Silver Catalysis in Organic Synthesis

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Publisher : John Wiley & Sons
ISBN 13 : 3527807691
Total Pages : 400 pages
Book Rating : 4.5/5 (278 download)

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Book Synopsis Silver Catalysis in Organic Synthesis by : Chao-Jun Li

Download or read book Silver Catalysis in Organic Synthesis written by Chao-Jun Li and published by John Wiley & Sons. This book was released on 2018-12-07 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt: Covers all the aspects of the recent achievements in silver catalyzed reactions Silver catalysis has emerged as a powerful tool in the field of organic synthesis. This comprehensive book systematically explores the unique performance of silver catalysis, introducing all the recent progress of silver catalysis in organic synthesis. It clearly emphasizes the unique features of silver catalysis and provides the reaction mechanism involved. This two-volume book also provides vivid schematics and tables throughout to enhance the accessibility to the relevant theory and mechanisms. Silver Catalysis in Organic Synthesis begins with an introduction to Silver Chemistry before moving on to chapters covering: Silver-Catalyzed Cycloaddition Reactions; Silver-Catalyzed Cyclizations; Silver-Mediated Radical Reactions; Silver-Mediated Fluorination, Perfluoroalkylation and Trifluoromethylthiolation Reactions; Coupling Reactions and C-H Functionalization; Silver-Catalyzed CO2 Incorporation; Silver-Catalyzed Carbene, Nitrene, and Silylene Transfer Reactions; Asymmetric Silver-Catalyzed Reactions; Silver-Catalyzed Reduction and Oxidation of Aldehydes and Their Derivatives; Silver Complexes in Organic Transformations; and Silver Nanoparticles in Organic Transformations. -Covers recently developed organic reactions catalyzed by silver, along with their reaction mechanism -Introduces many new reactions and mechanisms related to silver catalysis -Offers professionals and newcomers in the related fields a survey of new advances in silver catalysis in organic synthesis Silver Catalysis in Organic Synthesis will appeal to a wide readership including chemists, biochemists, pharmaceutical scientists, biomedical researchers, agriculture scientists, and graduate students in the related fields.

Chemisorption and Reactivity on Supported Clusters and Thin Films:

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Publisher : Springer Science & Business Media
ISBN 13 : 9401589119
Total Pages : 534 pages
Book Rating : 4.4/5 (15 download)

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Book Synopsis Chemisorption and Reactivity on Supported Clusters and Thin Films: by : R.M. Lambert

Download or read book Chemisorption and Reactivity on Supported Clusters and Thin Films: written by R.M. Lambert and published by Springer Science & Business Media. This book was released on 2013-04-17 with total page 534 pages. Available in PDF, EPUB and Kindle. Book excerpt: Heterogeneous catalysis provides the backbone of the world's chemical and oil industries. The innate complexity of practical catalytic systems suggests that useful progress should be achievable by investigating key aspects of catalysis by experimental studies on idealised model systems. Thin films and supported clusters are two promising types of model system that can be used for this purpose, since they mimic important aspects of the properties of practical dispersed catalysts. Similarly, appropriate theoretical studies of chemisorption and surface reaction clusters or extended slab systems can provide valuable information on the factors that underlie bonding and catalytic activity. This volume describes such experimental and theoretical approaches to the surface chemistry and catalytic behaviour of metals, metal oxides and metal/metal oxide systems. An introduction to the principles and main themes of heterogeneous catalysis is followed by detailed accounts of the application of modern experimental and theoretical techniques to fundamental problems. The application of advanced experimental methods is complemented by a full description of theoretical procedures, including Hartree-Fock, density functional and similar techniques. The relative merits of the various approaches are considered and directions for future progress are indicated.

Comprehensive Organic Functional Group Transformations II

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Publisher : Elsevier
ISBN 13 : 0080523471
Total Pages : 9196 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Comprehensive Organic Functional Group Transformations II by :

Download or read book Comprehensive Organic Functional Group Transformations II written by and published by Elsevier. This book was released on 2004-12-16 with total page 9196 pages. Available in PDF, EPUB and Kindle. Book excerpt: Comprehensive Organic Functional Group Transformations II (COFGT-II) will provide the first point of entry to the literature for all scientists interested in chemical transformations. Presenting the vast subject of organic synthesis in terms of the introduction and interconversion of all known functional groups, COFGT-II provides a unique information source documenting all methods of efficiently performing a particular transformation. Organised by the functional group formed, COFGT-II consists of 144 specialist reviews, written by leading scientists who evaluate and summarise the methods available for each functional group transformation. Also available online via ScienceDirect – featuring extensive browsing, searching, and internal cross-referencing between articles in the work, plus dynamic linking to journal articles and abstract databases, making navigation flexible and easy. For more information, pricing options and availability visit www.info.sciencedirect.com. By systematically treating each functional group in turn the work also identifies what is not known, thus pointing the way to new research areas Follows the systematic layout of the successful 1995 COFGT reference work, based on the arrangement and bonding of hetero-atoms around a central carbon atom The work will save researchers valuable time in their research as each chapter is written by experts who have critically read and reviewed the literature and presented the best methods of forming every known functional group

Comprehensive Organometallic Chemistry

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Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (8 download)

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Book Synopsis Comprehensive Organometallic Chemistry by : Geoffrey Wilkinson

Download or read book Comprehensive Organometallic Chemistry written by Geoffrey Wilkinson and published by . This book was released on 1982 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

The Chemistry of Enols

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ISBN 13 :
Total Pages : 848 pages
Book Rating : 4.X/5 (1 download)

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Book Synopsis The Chemistry of Enols by : Zvi Rappoport

Download or read book The Chemistry of Enols written by Zvi Rappoport and published by . This book was released on 1990-09-07 with total page 848 pages. Available in PDF, EPUB and Kindle. Book excerpt: From the series covering all aspects of the chemistry of one of the important groups in organic chemistry, this volume concentrates on the chemistry of enols.

Electrosorption

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Publisher : Springer Science & Business Media
ISBN 13 : 1468417312
Total Pages : 234 pages
Book Rating : 4.4/5 (684 download)

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Book Synopsis Electrosorption by : Eliezer Gileadi

Download or read book Electrosorption written by Eliezer Gileadi and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 234 pages. Available in PDF, EPUB and Kindle. Book excerpt: The gradual emergence during the last decade of the study of the mechanism of electrode reactions from the dark ages has given stimulus to a consideration of the double layer at metal-solution interfaces, which extends far outside the classical experimental studies of the capacitance of the mercury solution interface made during the 1950's by D. C. Grahame at Amherst College, Massachusetts. The central aspect of the study of an electrode reaction is the elucidation of its path and rate-determining step. Two fields are, however, prerequisites for such studies. First, it must be known what species are in the bulk of the solution, for these will seldom be simple ones such as H30~ and this study ("complex ions") has been made with both extent and depth. Second, the occupancy of the surface of the electrocatalyst and the associated field gradients must be known as a function of position in the double layer. Such "maps of the double layer" can be given with reasonable certainty up to concentrations of about 1 N for mercury in contact with solutions of inorganic ions. However, this is-or was until very recently-the extent of the know ledge. The problems confronting a fundamental approach to the rational development of, e.g., fuel cell catalysis were therefore considerable.

Adhesives Technology for Electronic Applications

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Publisher : William Andrew
ISBN 13 : 1437778909
Total Pages : 415 pages
Book Rating : 4.4/5 (377 download)

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Book Synopsis Adhesives Technology for Electronic Applications by : James J. Licari

Download or read book Adhesives Technology for Electronic Applications written by James J. Licari and published by William Andrew. This book was released on 2011-06-24 with total page 415 pages. Available in PDF, EPUB and Kindle. Book excerpt: Approx.512 pages Approx.512 pages