Hplc Of Polymers

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HPLC of Polymers

Author : Harald Pasch
Publisher : Springer Science & Business Media
ISBN 13 : 3642582656
Total Pages : 234 pages
Book Rating : 4.6/5 (425 download)

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Book Synopsis HPLC of Polymers by : Harald Pasch

Download or read book HPLC of Polymers written by Harald Pasch and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 234 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymers are mainly characterized by molar mass, chemical composition, functionality and architecture. The determination of the complex structure of polymers by chromatographic and spectroscopic methods is one of the major concerns of polymer analysis and characterization. This lab manual describes the experimental approach to the chromatographic analysis of polymers. Different chromatographic methods, their theoretical background, equipment, experimental procedures and applications are discussed. The book will enable polymer chemists, physicists and material scientists as well as students of macromolecular and analytical science to optimize chromatographic conditions for a specific separation problem. Special emphasis is given to the description of applications for homo- and copolymers and polymer blends.

Multidimensional HPLC of Polymers

Author : Harald Pasch
Publisher : Springer Science & Business Media
ISBN 13 : 3642360807
Total Pages : 291 pages
Book Rating : 4.6/5 (423 download)

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Book Synopsis Multidimensional HPLC of Polymers by : Harald Pasch

Download or read book Multidimensional HPLC of Polymers written by Harald Pasch and published by Springer Science & Business Media. This book was released on 2013-06-12 with total page 291 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents the principle ideas of combining different analytical techniques in multi-dimensional analysis schemes. It reviews the basic principles and instrumentation of multi-dimensional chromatography and the hyphenation of liquid chromatography with selective spectroscopic detectors and presents experimental protocols for the analysis of complex polymers. It is the consequent continuation of "HPLC of Polymers" from 1999 by the same authors. Like its 'predecessor', this book discusses the theoretical background, equipment, experimental procedures and applications for each separation technique, but in contrast treats multi-dimensional and coupled techniques. "Multidimensional HPLC of Polymers" intends to review the state of the art in polymer chromatography and to summarize the developments in the field during the last 15 years. With its tutorial and laboratory manual style it is written for beginners as well as for experienced chromatographers, and will enable its readers (polymer chemists, physicists and material scientists, as well as students of polymer and analytical sciences) to optimize the experimental conditions for their specific separation problems.

Polymer Characterization by Liquid Chromatography

Author : G. Glöckner
Publisher : Elsevier
ISBN 13 : 9780080858371
Total Pages : 585 pages
Book Rating : 4.8/5 (583 download)

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Book Synopsis Polymer Characterization by Liquid Chromatography by : G. Glöckner

Download or read book Polymer Characterization by Liquid Chromatography written by G. Glöckner and published by Elsevier. This book was released on 1987-02-01 with total page 585 pages. Available in PDF, EPUB and Kindle. Book excerpt: The main subject of this book is the characterization of plastics. To a high degree the properties of these polymers depend on the distribution of the molar mass and of other structural features, and small deviations frequently have a great effect. Therefore the characterization of polymers cannot be restricted to the determination of mean values but must yield information on these distributions. Using classical methods, the analytical fractionation of polymer homologues and structurally isomeric polymers is extremely time-consuming. Therefore, efficient chromatographic techniques are being increasingly employed in modern polymer characterization. In the first place, high-performance liquid chromatography is applied, in the form of size exclusion chromatography. It is also possible, however, to use other separation modes. More space is devoted to these other possibilities in this volume than is merited by their current range of applications, as the author believes that many separation problems will be solved by separation techniques of the non-exclusion type. Nevertheless, much emphasis is placed on size exclusion chromatography. Not only because of its current wide range of applications, but also because its relative importance, as a complement to other chromatographic techniques may even increase in the forthcoming years. This book is the first to cover all phenomena related to the above considerations. Starting with an introduction to basic liquid chromatography and to polymer science, it deals with the adsorption behaviour of polymers, with gradient techniques, with the kinetic band broadening in liquid chromatography, with instrumental features and packing materials. The book consists of four balanced sections and related information from about 1800 references is compiled in the tables. Some 250 figures and 30 tables will help give the reader a clear insight of the topics discussed. The book is aimed at helping the analyst or polymer chemist who is looking for information about chromatographic methods for the characterization of polymers.

Liquid Chromatography of Synthetic Polymers

Author : Muhammad Imran Malik
Publisher : Springer Nature
ISBN 13 : 3031348354
Total Pages : 310 pages
Book Rating : 4.0/5 (313 download)

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Book Synopsis Liquid Chromatography of Synthetic Polymers by : Muhammad Imran Malik

Download or read book Liquid Chromatography of Synthetic Polymers written by Muhammad Imran Malik and published by Springer Nature. This book was released on 2023-11-03 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book elucidates the peculiar phenomenon of entropy/enthalpy compensation that takes place in high performance liquid chromatography (HPLC) of polymers. Numerous publications, including some books, are devoted to molecular characterization of synthetic polymers, materials presently produced in large and steadily growing quantities, applying methods of HPLC. A knowledge of the molecular characteristics of polymers is indispensable, not only for their proper applications but also for their recycling and remediation. Polymer scientists generally focus on synthesis and potential applications of polymers while not giving due attention to an important central link, their comprehensive characterization in context of development of structure-property correlations. To fill this gap is one of the aims of the present book. The process of entropy/enthalpy compensation plays a decisive role in the advanced method of polymer characterization such as liquid chromatography at critical conditions, eluent gradient interaction chromatography, and temperature gradient interaction chromatography. All chemists working on any aspect of polymer science will find this book a valuable resource for the development of structure-property correlations.

Gradient HPLC of Copolymers and Chromatographic Cross-Fractionation

Author : Gottfried Glöckner
Publisher : Springer Science & Business Media
ISBN 13 : 3642757995
Total Pages : 227 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Gradient HPLC of Copolymers and Chromatographic Cross-Fractionation by : Gottfried Glöckner

Download or read book Gradient HPLC of Copolymers and Chromatographic Cross-Fractionation written by Gottfried Glöckner and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 227 pages. Available in PDF, EPUB and Kindle. Book excerpt: "The problems involved in separating complex macromolecules require under standing not only the chromatographic process but also the physicochemical behavior of the solutes." This sentence from the pen of Phyllis R. Brown 1, University of Rhode Island, can certainly be applied to synthetic copolymers whose structure is very complex indeed. Thus it may be forgiven that a book on copolymer HPLC has been written not by a trained chromatographer but by someone from the polymer side. The HPLC of synthetic polymers is often understood to mean only a synonym for size exclusion chromatography. The latter method separates polymers according to the size of the macromolecules and enables the molecular weight distribution of a sample to be evaluated. But as early as 1936, Mark and Saito attempted chromatographic fractionation of cellulose acetate on a charcoal-like adsorbent made from blood. HPLC adsorption chromatography was first applied to copolymer analysis by Teramachi et al. in 1979. Since then, another branch of polymer HPLC has arisen which has the capacity of separating copolymers by composition and enables the chemical composition distribution to be evaluated. The technique requires a suitable elution program and is mainly carried out as gradient elution.

Liquid Chromatography of Polymers and Related Materials

Author : Jack Cazes
Publisher :
ISBN 13 :
Total Pages : 200 pages
Book Rating : 4.:/5 (319 download)

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Book Synopsis Liquid Chromatography of Polymers and Related Materials by : Jack Cazes

Download or read book Liquid Chromatography of Polymers and Related Materials written by Jack Cazes and published by . This book was released on 1977 with total page 200 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Liquid Chromatography

Author : W. Radke
Publisher : Elsevier Inc. Chapters
ISBN 13 : 0128071109
Total Pages : 688 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Liquid Chromatography by : W. Radke

Download or read book Liquid Chromatography written by W. Radke and published by Elsevier Inc. Chapters. This book was released on 2013-01-08 with total page 688 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the last decade, the use of interaction chromatography and hyphenated techniques has become increasingly important for the characterization of polymeric materials. Interaction chromatography allows separation by other structural features than molar mass, while hyphenation with mass spectroscopy or spectroscopic techniques provides detailed characterization of the separated chromatographic fractions. This chapter gives an overview of the principles and applications of interaction chromatography and the information that can be determined by hyphenation of polymer chromatography with mass spectrometry and spectroscopic techniques.

Chemical Analysis of Polymers

Author : G. Lawson
Publisher : iSmithers Rapra Publishing
ISBN 13 : 9780080417424
Total Pages : 136 pages
Book Rating : 4.4/5 (174 download)

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Book Synopsis Chemical Analysis of Polymers by : G. Lawson

Download or read book Chemical Analysis of Polymers written by G. Lawson and published by iSmithers Rapra Publishing. This book was released on 1991-12 with total page 136 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Gas Chromatography of Polymers

Author :
Publisher : Elsevier
ISBN 13 : 9780080858104
Total Pages : 224 pages
Book Rating : 4.8/5 (581 download)

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Book Synopsis Gas Chromatography of Polymers by :

Download or read book Gas Chromatography of Polymers written by and published by Elsevier. This book was released on 2011-09-22 with total page 224 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas Chromatography of Polymers

Liquid Chromatography of Polymers and Related Materials. III

Author : Jack Cazes
Publisher : CRC Press
ISBN 13 : 1000146138
Total Pages : 315 pages
Book Rating : 4.0/5 (1 download)

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Book Synopsis Liquid Chromatography of Polymers and Related Materials. III by : Jack Cazes

Download or read book Liquid Chromatography of Polymers and Related Materials. III written by Jack Cazes and published by CRC Press. This book was released on 2020-11-26 with total page 315 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book describes new gel permeation chromatography/liquid chromatography applications and techniques that will provide polymer scientists and practitioners with insight into the development of new polymers and plastics and improvement of existing materials.

Molecular Characterization of Polymers

Author : Muhammad Imran Malik
Publisher : Elsevier
ISBN 13 : 012822598X
Total Pages : 670 pages
Book Rating : 4.1/5 (282 download)

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Book Synopsis Molecular Characterization of Polymers by : Muhammad Imran Malik

Download or read book Molecular Characterization of Polymers written by Muhammad Imran Malik and published by Elsevier. This book was released on 2021-03-09 with total page 670 pages. Available in PDF, EPUB and Kindle. Book excerpt: Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material Establishes a strong link between basic principles, characterization techniques, and real-life applications

Chromatography Mass Spectroscopy in Polymer Analysis

Author : T. R Crompton
Publisher : Smithers Rapra
ISBN 13 : 184735484X
Total Pages : 248 pages
Book Rating : 4.8/5 (473 download)

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Book Synopsis Chromatography Mass Spectroscopy in Polymer Analysis by : T. R Crompton

Download or read book Chromatography Mass Spectroscopy in Polymer Analysis written by T. R Crompton and published by Smithers Rapra. This book was released on 2010-12-02 with total page 248 pages. Available in PDF, EPUB and Kindle. Book excerpt: The combination of chromatography with mass spectroscopy is a very useful technique which is being increasingly used by polymer chemists to improve existing polymers and to discover new ones with specific physical properties such as thermal stability and retention of properties over a long service life.This technique is extremely powerful for the analysis and characterisation of polymers and is often based on the use of controlled chromatography - mass spectroscopy to measure a polymer's decomposition with techniques such as pyrolysis, followed by chromatography to separate any breakdown product, and, finally, mass spectroscopy, to achieve an unequivocal identification of the pyrolysis products obtained. The detail that can be obtained by such methods includes structure of the polymer backbone, branching, end groups, isomeric detail and fine detail in the structure of copolymers.The first three chapters of the book discuss the various chromatographic and mass spectroscopic techniques now available.Chapters 3-8 cover the complementary methods, based on the combination of mass spectroscopy with various chromatographic techniques such as high-performance liquid chromatography, gas chromatography and supercritical fluid chromatography.Pyrolysis chromatography-mass spectroscopy is a method of studying the structure of polymers which involves subjecting the polymer pyrolysis products to a chromatographic technique to simplify subsequent analysis and, finally mass spectroscopy to identify the pyrolysis products with the possibility of deducing finer details of polymer structure than were previously attainable by classical methods (Chapters 9-11).By providing a thorough up-to-date review of work in this field it is hoped that the book will be of interest to all those engaged in polymer research and development, and polymer users in general.

Polymer Characterization by Liquid Chromatography

Author : Gottfried Glöckner
Publisher :
ISBN 13 : 9780444416162
Total Pages : 330 pages
Book Rating : 4.4/5 (161 download)

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Book Synopsis Polymer Characterization by Liquid Chromatography by : Gottfried Glöckner

Download or read book Polymer Characterization by Liquid Chromatography written by Gottfried Glöckner and published by . This book was released on 1986 with total page 330 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Liquid Chromatography of Polymers and Related Materials, II

Author : Jack Cazes
Publisher : CRC Press
ISBN 13 : 1000110508
Total Pages : 273 pages
Book Rating : 4.0/5 (1 download)

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Book Synopsis Liquid Chromatography of Polymers and Related Materials, II by : Jack Cazes

Download or read book Liquid Chromatography of Polymers and Related Materials, II written by Jack Cazes and published by CRC Press. This book was released on 2020-11-25 with total page 273 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers a range of topics of interest to those involved in the fractionation and characterization of polymeric substances. It deals with problems that are encountered in modern gel permeation chromatography with dual detection when calculating average molecular weights.

Modern Methods of Polymer Characterization

Author : Howard G. Barth
Publisher : John Wiley & Sons
ISBN 13 : 9780471828143
Total Pages : 582 pages
Book Rating : 4.8/5 (281 download)

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Book Synopsis Modern Methods of Polymer Characterization by : Howard G. Barth

Download or read book Modern Methods of Polymer Characterization written by Howard G. Barth and published by John Wiley & Sons. This book was released on 1991-09-03 with total page 582 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents the methods used for characterization of polymers. In addition to theory and basic principles, the instrumentation and apparatus necessary for methods used to study the kinetic and thermodynamic interactions of a polymer with its environment are covered in detail. Some of the methods examined include polymer separations and characterization by size exclusion and high performance chromatography, inverse gas chromatography, osmometry, viscometry, ultracentrifugation, light scattering and spectroscopy.

Liquid Chromatography of Polymers and Related Materials. III

Author : Jack Cazes
Publisher : CRC Press
ISBN 13 : 9780824715144
Total Pages : 316 pages
Book Rating : 4.7/5 (151 download)

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Book Synopsis Liquid Chromatography of Polymers and Related Materials. III by : Jack Cazes

Download or read book Liquid Chromatography of Polymers and Related Materials. III written by Jack Cazes and published by CRC Press. This book was released on 1981-08-01 with total page 316 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book describes new gel permeation chromatography/liquid chromatography applications and techniques that will provide polymer scientists and practitioners with insight into the development of new polymers and plastics and improvement of existing materials.

Handbook of HPLC

Author : Danilo Corradini
Publisher : CRC Press
ISBN 13 : 9780203909751
Total Pages : 1018 pages
Book Rating : 4.9/5 (97 download)

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Book Synopsis Handbook of HPLC by : Danilo Corradini

Download or read book Handbook of HPLC written by Danilo Corradini and published by CRC Press. This book was released on 2011-01-03 with total page 1018 pages. Available in PDF, EPUB and Kindle. Book excerpt: Delineating its usage in separation, purification and detection processes across a variety of disciplines, from industry to applied research, this work discusses the principles, techniques and instrumentation involving HPLC within a detailed framework. Over 100 tables present previously scattered experimental data.