Multidimensional HPLC of Polymers

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Publisher : Springer Science & Business Media
ISBN 13 : 3642360807
Total Pages : 291 pages
Book Rating : 4.6/5 (423 download)

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Book Synopsis Multidimensional HPLC of Polymers by : Harald Pasch

Download or read book Multidimensional HPLC of Polymers written by Harald Pasch and published by Springer Science & Business Media. This book was released on 2013-06-12 with total page 291 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents the principle ideas of combining different analytical techniques in multi-dimensional analysis schemes. It reviews the basic principles and instrumentation of multi-dimensional chromatography and the hyphenation of liquid chromatography with selective spectroscopic detectors and presents experimental protocols for the analysis of complex polymers. It is the consequent continuation of "HPLC of Polymers" from 1999 by the same authors. Like its 'predecessor', this book discusses the theoretical background, equipment, experimental procedures and applications for each separation technique, but in contrast treats multi-dimensional and coupled techniques. "Multidimensional HPLC of Polymers" intends to review the state of the art in polymer chromatography and to summarize the developments in the field during the last 15 years. With its tutorial and laboratory manual style it is written for beginners as well as for experienced chromatographers, and will enable its readers (polymer chemists, physicists and material scientists, as well as students of polymer and analytical sciences) to optimize the experimental conditions for their specific separation problems.

HPLC of Polymers

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Author :
Publisher : Springer Science & Business Media
ISBN 13 : 3642582656
Total Pages : 234 pages
Book Rating : 4.6/5 (425 download)

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Book Synopsis HPLC of Polymers by : Harald Pasch

Download or read book HPLC of Polymers written by Harald Pasch and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 234 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymers are mainly characterized by molar mass, chemical composition, functionality and architecture. The determination of the complex structure of polymers by chromatographic and spectroscopic methods is one of the major concerns of polymer analysis and characterization. This lab manual describes the experimental approach to the chromatographic analysis of polymers. Different chromatographic methods, their theoretical background, equipment, experimental procedures and applications are discussed. The book will enable polymer chemists, physicists and material scientists as well as students of macromolecular and analytical science to optimize chromatographic conditions for a specific separation problem. Special emphasis is given to the description of applications for homo- and copolymers and polymer blends.

Chromatographic Characterization of Polymers

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Publisher :
ISBN 13 :
Total Pages : 322 pages
Book Rating : 4.X/5 (2 download)

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Book Synopsis Chromatographic Characterization of Polymers by : Theodore Provder

Download or read book Chromatographic Characterization of Polymers written by Theodore Provder and published by . This book was released on 1995 with total page 322 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents an overview of the recent developments in the use of hyphenated multidimensional separation and detection techniques for the characterization of polymeric materials. Reports on successful multidimensional chromatographic methods and multiple detector systems. Includes an analysis of compositional heterogeneity in copolymers and blends.

Chromatography of Polymers

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Publisher :
ISBN 13 :
Total Pages : 368 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Chromatography of Polymers by : Theodore Provder

Download or read book Chromatography of Polymers written by Theodore Provder and published by . This book was released on 1999 with total page 368 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers recent advances in characterizing polymers by chromatographic techniques and with other types of detectors. It also examines applications of these techniques to the analysis of oligomers and other polymeric techniques.

Multidimensional Liquid Chromatography

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Publisher : John Wiley & Sons
ISBN 13 : 0470276258
Total Pages : 490 pages
Book Rating : 4.4/5 (72 download)

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Book Synopsis Multidimensional Liquid Chromatography by : Steven A. Cohen

Download or read book Multidimensional Liquid Chromatography written by Steven A. Cohen and published by John Wiley & Sons. This book was released on 2008-05-09 with total page 490 pages. Available in PDF, EPUB and Kindle. Book excerpt: Multidimensional Liquid Chromatography (MDLC) is a very powerful separation technique for analyzing exceptionally complex samples in one step. This authoritative reference presents a number of recent contributions that help define the current art and science of MDLC. Topics covered include instrumentation, theory, methods development, and applications of MDLC in the life sciences and in industrial chemistry. With the information to help you perform very difficult separations of complex samples, this reference includes chapters contributed by leading experts or teams of experts.

Liquid Chromatography of Synthetic Polymers

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Publisher : Springer Nature
ISBN 13 : 3031348354
Total Pages : 310 pages
Book Rating : 4.0/5 (313 download)

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Book Synopsis Liquid Chromatography of Synthetic Polymers by : Muhammad Imran Malik

Download or read book Liquid Chromatography of Synthetic Polymers written by Muhammad Imran Malik and published by Springer Nature. This book was released on 2023-11-03 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book elucidates the peculiar phenomenon of entropy/enthalpy compensation that takes place in high performance liquid chromatography (HPLC) of polymers. Numerous publications, including some books, are devoted to molecular characterization of synthetic polymers, materials presently produced in large and steadily growing quantities, applying methods of HPLC. A knowledge of the molecular characteristics of polymers is indispensable, not only for their proper applications but also for their recycling and remediation. Polymer scientists generally focus on synthesis and potential applications of polymers while not giving due attention to an important central link, their comprehensive characterization in context of development of structure-property correlations. To fill this gap is one of the aims of the present book. The process of entropy/enthalpy compensation plays a decisive role in the advanced method of polymer characterization such as liquid chromatography at critical conditions, eluent gradient interaction chromatography, and temperature gradient interaction chromatography. All chemists working on any aspect of polymer science will find this book a valuable resource for the development of structure-property correlations.

Multidimensional Chromatography

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Publisher : John Wiley & Sons
ISBN 13 : 9780471988694
Total Pages : 464 pages
Book Rating : 4.9/5 (886 download)

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Book Synopsis Multidimensional Chromatography by : Luigi Mondello

Download or read book Multidimensional Chromatography written by Luigi Mondello and published by John Wiley & Sons. This book was released on 2002-02-15 with total page 464 pages. Available in PDF, EPUB and Kindle. Book excerpt: Mehrdimensionale Chromatographie im analytischen Labor: Dieses Buch bespricht erstmals alle gängigen Verfahren sowie Anwendungen auf verschiedensten Gebieten, von der Pharmazie, Biologie und Chemie bis hin zur Umwelttechnik und erdölverarbeitender Industrie. Die Autoren sind selbst aktiv in der einschlägigen Forschung tätig.

Additives in Polymers

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Publisher : John Wiley & Sons
ISBN 13 : 0470012056
Total Pages : 836 pages
Book Rating : 4.4/5 (7 download)

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Book Synopsis Additives in Polymers by : Jan C. J. Bart

Download or read book Additives in Polymers written by Jan C. J. Bart and published by John Wiley & Sons. This book was released on 2005-04-08 with total page 836 pages. Available in PDF, EPUB and Kindle. Book excerpt: This industrially relevant resource covers all established and emerging analytical methods for the deformulation of polymeric materials, with emphasis on the non-polymeric components. Each technique is evaluated on its technical and industrial merits. Emphasis is on understanding (principles and characteristics) and industrial applicability. Extensively illustrated throughout with over 200 figures, 400 tables, and 3,000 references.

New Developments in Polymer Analytics I

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Publisher : Springer
ISBN 13 : 3540487646
Total Pages : 235 pages
Book Rating : 4.5/5 (44 download)

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Book Synopsis New Developments in Polymer Analytics I by : M. Schmidt

Download or read book New Developments in Polymer Analytics I written by M. Schmidt and published by Springer. This book was released on 2003-07-01 with total page 235 pages. Available in PDF, EPUB and Kindle. Book excerpt: The two companion volumes of "Advances in Polymer Science" - Volumes 150 and 151 - deal with recent progress in the characterization of polymers, mostly in solution but also at surfaces. The contributions comprise multidimensional chromatography for elucidation, the composition and the chain length distribution of copolymers, capillary electrophoresis of synthetic water-soluble polymers including polyelectrolytes, field flow fractionation techniques for quick and reliable separation and characterization of broad polymer samples and a novel application of thermal grating experiments for probing Brownian and thermal diffusion. Finally the rapid development of atomic forces techniques is reviewed with particular emphasis on the visualization of macromolecules and the patterning of surfaces.

Hyphenated and Alternative Methods of Detection in Chromatography

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Publisher : CRC Press
ISBN 13 : 1000654567
Total Pages : 311 pages
Book Rating : 4.0/5 (6 download)

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Book Synopsis Hyphenated and Alternative Methods of Detection in Chromatography by : R. Andrew Shalliker

Download or read book Hyphenated and Alternative Methods of Detection in Chromatography written by R. Andrew Shalliker and published by CRC Press. This book was released on 2011-12-14 with total page 311 pages. Available in PDF, EPUB and Kindle. Book excerpt: Widely employed for separating and detecting chemicals in solution, separation techniques are most often applied in tandem, subsequently referred to as hyphenated methods. Hyphenated and Alternative Methods of Detection in Chromatography details the development and application of mass spectral detection techniques coupled with gas phase and liquid

Thermal Field-Flow Fractionation of Polymers

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Publisher : Springer
ISBN 13 : 3030106500
Total Pages : 116 pages
Book Rating : 4.0/5 (31 download)

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Book Synopsis Thermal Field-Flow Fractionation of Polymers by : Guilaume Greyling

Download or read book Thermal Field-Flow Fractionation of Polymers written by Guilaume Greyling and published by Springer. This book was released on 2019-02-21 with total page 116 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book introduces the reader to thermal field-flow fractionation and discusses its advantages over the fundamental problems associated with traditional column-based analytical techniques commonly used to characterize polymers and macromolecules. The authors discuss the theoretical background, equipment, experimental procedures as well as the recent advances and applications of thermal field-flow fractionation. Complete with several practical examples and troubleshooting guidelines, the book is written for beginners and experienced separation scientists alike and will enable its readers to optimize their experimental conditions for their specific separation needs and problems.

Advanced Separation Techniques for Polyolefins

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Publisher : Springer
ISBN 13 : 3319086324
Total Pages : 179 pages
Book Rating : 4.3/5 (19 download)

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Book Synopsis Advanced Separation Techniques for Polyolefins by : Harald Pasch

Download or read book Advanced Separation Techniques for Polyolefins written by Harald Pasch and published by Springer. This book was released on 2014-08-27 with total page 179 pages. Available in PDF, EPUB and Kindle. Book excerpt: This Springer Laboratory volume introduces the reader to advanced techniques for the separation and fractionation of polyolefins. It includes detailed information on experimental protocols and procedures, addressing the experimental background of different polyolefin fractionation techniques in great detail. The book summarizes important applications in all major fractionation methods with emphasis on multidimensional analytical approaches. It comprises the most powerful modern techniques, such as high temperature size exclusion chromatography (HT-SEC) for molar mass analysis, temperature rising elution fractionation (TREF) and crystallization analysis fractionation (CRYSTAF) for the analysis of chemical composition and branching, high temperature two-dimensional liquid chromatography (HT-2D-LC), solvent and temperature gradient interaction chromatography (SGIC and TGIC) and crystallization elution fractionation (CEF). Beginners as well as experienced chromatographers will benefit from this concise introduction to a great variety in instrumentation, separation procedures and applications. With detailed descriptions of experimental approaches for the analysis of complex polyolefins, the readers are offered a toolbox to solve simple as well as sophisticated separation tasks. The book starts with an introduction into the molecular complexity of polyolefins - the most widely used synthetic polymers with rapidly growing production capacities. It systematically discusses crystallization based fractionation techniques including TREF, CRYSTAF and CEF and column chromatographic techniques for molar mass, chemical composition and microstructure, as well as the combination of different fractionations in multidimensional experimental setups. This book also includes basic information on the application of high-temperature field-flow fractionation.

Molecular Characterization of Polymers

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Publisher : Elsevier
ISBN 13 : 012822598X
Total Pages : 670 pages
Book Rating : 4.1/5 (282 download)

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Book Synopsis Molecular Characterization of Polymers by : Muhammad Imran Malik

Download or read book Molecular Characterization of Polymers written by Muhammad Imran Malik and published by Elsevier. This book was released on 2021-03-09 with total page 670 pages. Available in PDF, EPUB and Kindle. Book excerpt: Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material Establishes a strong link between basic principles, characterization techniques, and real-life applications

Liquid Chromatography of Polymers and Related Materials. III

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Publisher : CRC Press
ISBN 13 : 1000146138
Total Pages : 315 pages
Book Rating : 4.0/5 (1 download)

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Book Synopsis Liquid Chromatography of Polymers and Related Materials. III by : Jack Cazes

Download or read book Liquid Chromatography of Polymers and Related Materials. III written by Jack Cazes and published by CRC Press. This book was released on 2020-11-26 with total page 315 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book describes new gel permeation chromatography/liquid chromatography applications and techniques that will provide polymer scientists and practitioners with insight into the development of new polymers and plastics and improvement of existing materials.

Gradient HPLC of Copolymers and Chromatographic Cross-Fractionation

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Publisher : Springer Science & Business Media
ISBN 13 : 3642757995
Total Pages : 227 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Gradient HPLC of Copolymers and Chromatographic Cross-Fractionation by : Gottfried Glöckner

Download or read book Gradient HPLC of Copolymers and Chromatographic Cross-Fractionation written by Gottfried Glöckner and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 227 pages. Available in PDF, EPUB and Kindle. Book excerpt: "The problems involved in separating complex macromolecules require under standing not only the chromatographic process but also the physicochemical behavior of the solutes." This sentence from the pen of Phyllis R. Brown 1, University of Rhode Island, can certainly be applied to synthetic copolymers whose structure is very complex indeed. Thus it may be forgiven that a book on copolymer HPLC has been written not by a trained chromatographer but by someone from the polymer side. The HPLC of synthetic polymers is often understood to mean only a synonym for size exclusion chromatography. The latter method separates polymers according to the size of the macromolecules and enables the molecular weight distribution of a sample to be evaluated. But as early as 1936, Mark and Saito attempted chromatographic fractionation of cellulose acetate on a charcoal-like adsorbent made from blood. HPLC adsorption chromatography was first applied to copolymer analysis by Teramachi et al. in 1979. Since then, another branch of polymer HPLC has arisen which has the capacity of separating copolymers by composition and enables the chemical composition distribution to be evaluated. The technique requires a suitable elution program and is mainly carried out as gradient elution.

Rubber Analysis

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Publisher : Walter de Gruyter GmbH & Co KG
ISBN 13 : 3110640287
Total Pages : 358 pages
Book Rating : 4.1/5 (16 download)

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Book Synopsis Rubber Analysis by : Martin J. Forrest

Download or read book Rubber Analysis written by Martin J. Forrest and published by Walter de Gruyter GmbH & Co KG. This book was released on 2019-04-01 with total page 358 pages. Available in PDF, EPUB and Kindle. Book excerpt: Rubber analysis plays a vital part in ensuring that manufactured products are fit for purpose. This comprehensive, application-based book with up-to-date referencing covers all important applications and subject area associated with the analysis of rubber compounds and rubber products. Includes characterization of rubber polymers, rubber fumes, identification of extractables and leachables, as well as reverse engineering on compounded products.

Multidimensional Spectroscopy of Polymers

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Publisher : Wiley-VCH
ISBN 13 :
Total Pages : 624 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Multidimensional Spectroscopy of Polymers by : Marek W. Urban

Download or read book Multidimensional Spectroscopy of Polymers written by Marek W. Urban and published by Wiley-VCH. This book was released on 1995-08-31 with total page 624 pages. Available in PDF, EPUB and Kindle. Book excerpt: Focuses on advances in three areas of multidimensional spectroscopy: NMR, vibrational, and fluorescence. Discusses important areas in polymer analysis, including diffusion, free volume, adhesion, absorption, polymer interactions, and miscibility. Includes introductory chapters as well as chapters covering both theory and application. Valuable material for researchers in polymer science and in analytical laboratories specializing in NMR, FT-IR and fluorescence spectroscopy.