High Resolution NMR in Solids Selective Averaging

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Publisher : Elsevier
ISBN 13 : 0323160255
Total Pages : 205 pages
Book Rating : 4.3/5 (231 download)

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Book Synopsis High Resolution NMR in Solids Selective Averaging by : Ulrich Haeberlen

Download or read book High Resolution NMR in Solids Selective Averaging written by Ulrich Haeberlen and published by Elsevier. This book was released on 2012-12-02 with total page 205 pages. Available in PDF, EPUB and Kindle. Book excerpt: High Resolution NMR in Solids: Selective Averaging presents the principles and applications of the four approaches to high resolution NMR in solids — magic-angle sample spinning, multiple-pulse, proton-enhanced nuclear induction, and indirect detection methods. Divided into six chapters, this book initially describes the tensorial properties of nuclear spin interactions in both ordinary and spin spaces. It then deals with the manifestations of nuclear magnetic shielding in NMR spectra of both single-crystal and powder samples, and then discusses the techniques for analyzing spectra and rotation patterns in terms of shielding tensors. A wide range of NMR phenomena that are result of intentional or natural, selective or unselective averaging processes and the average Hamiltonian theory that yields the inclusion of correction are covered. This book also provides a detailed discussion on multiple-pulse sequences intended for high resolution NMR in solids. The concluding chapter examines the applications of multiple-pulse techniques, with particular emphasis on measurements of 19F and 1H shielding tensors. Discussions on rotations of angular momentum operators; time ordering and the Magnus expansion; off-resonance averaging of the second-order dipolar Hamiltonian; and phase transients are covered in the supplemental texts.

High resolution NMR in solids

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Publisher :
ISBN 13 :
Total Pages : 190 pages
Book Rating : 4.:/5 (251 download)

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Book Synopsis High resolution NMR in solids by :

Download or read book High resolution NMR in solids written by and published by . This book was released on 1976 with total page 190 pages. Available in PDF, EPUB and Kindle. Book excerpt:

High resolution NMR in solids

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Publisher :
ISBN 13 :
Total Pages : 0 pages
Book Rating : 4.:/5 (136 download)

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Book Synopsis High resolution NMR in solids by :

Download or read book High resolution NMR in solids written by and published by . This book was released on with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:

High Resolution NMR in Solids - Selective Averaging ; Supplement I , Advances in Magnetic Resonance

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ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (985 download)

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Book Synopsis High Resolution NMR in Solids - Selective Averaging ; Supplement I , Advances in Magnetic Resonance by : Haeberlen U.

Download or read book High Resolution NMR in Solids - Selective Averaging ; Supplement I , Advances in Magnetic Resonance written by Haeberlen U. and published by . This book was released on 1976 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Principles of High Resolution NMR in Solids

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Author :
Publisher : Springer Science & Business Media
ISBN 13 : 3642687563
Total Pages : 352 pages
Book Rating : 4.6/5 (426 download)

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Book Synopsis Principles of High Resolution NMR in Solids by : M. Mehring

Download or read book Principles of High Resolution NMR in Solids written by M. Mehring and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 352 pages. Available in PDF, EPUB and Kindle. Book excerpt: The field of Nuclear Magnetic Resonance (NMR) has developed at a fascinating pace during the last decade. It always has been an extremely valuable tool to the organic chemist by supplying molecular "finger print" spectra at the atomic level. Unfortunately the high resolution achievable in liquid solutions could not be obtained in solids and physicists and physical chemists had to live with unresolved lines open to a wealth of curve fitting procedures and a vast amount of speculations. High resolution NMR in solids seemed to be a paradoxon. Broad structure less lines are usually encountered when dealing with NMR in solids. Only with the recent advent of mUltiple pulse, magic angle, cross-polarization, two-dimen sional and multiple-quantum spectroscopy and other techniques during the last decade it became possible to resolve finer details of nuclear spin interactions in solids. I have felt that graduate students, researchers and others beginning to get involved with these techniques needed a book which treats the principles, theo retical foundations and applications of these rather sophisticated experimental techniques. Therefore I wrote a monograph on the subject in 1976. Very soon new ideas led to the developement of "two-dimensional spectroscopy" and "multiple-quantum spectroscopy", topics which were not covered in the first edition of my book. Moreover an exponential growth of literature appeared in this area of research leaving the beginner in an awkward situation of tracing back from a current article to the roots of the experiment.

High Resolution NMR Spectroscopy in Solids

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Publisher : Springer Science & Business Media
ISBN 13 : 3642963323
Total Pages : 257 pages
Book Rating : 4.6/5 (429 download)

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Book Synopsis High Resolution NMR Spectroscopy in Solids by : M. Mehring

Download or read book High Resolution NMR Spectroscopy in Solids written by M. Mehring and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 257 pages. Available in PDF, EPUB and Kindle. Book excerpt: Manipulation and Dilution Tools for Ruling Abundant Species "NMR is dead" was the slogan heard in the late 1960s at least among physicists, until John S. Waugh and his co-workers initiated a series of new NMR experiments, which employed the coherent modulation of interactions by strong radiofrequency fields. A wealth of new phenomena was observed, which are summarized in the introduction for the convenience of the unbiased reader, whereas Section 2 collects the basic spin interactions observed in solids. Line-narrowing effects in dipolar coupled solids by the application of multiple pulse experiments are extensively discussed in Section 3. Numerous extensions of the basic Waugh, Huber, and Haeberlen experiment have been developed by different groups and have been applied to the nuclei IH, 9Be, 19F, 27Al, 31p, 63CU in solids. Application of this technique to a variety of systems is still in progress and should reveal interesting insights into weak spin interactions in solids. It was soon realized that rare spins could be used as monitors for molecular fields in the solid state; however, rare spin observation is difficult because of the small signal-to-noise ratio. Pines, Gibby, and Waugh introduced a new concept of cross-polarization, based on ideas of Hahn and co-workers, which allows the detection ofrare spins with increased sensitivity. The dynamics involved are treated in detail. Other sections merely list results obtained by the techniques described and demonstrate their usefulness in the investigation of dynamical problems in molec ular and solid state physics.

Selective averaging, key to enhancement of resolution in NMR

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Publisher :
ISBN 13 :
Total Pages : 574 pages
Book Rating : 4.:/5 (72 download)

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Book Synopsis Selective averaging, key to enhancement of resolution in NMR by : Ulrich Haeberlen

Download or read book Selective averaging, key to enhancement of resolution in NMR written by Ulrich Haeberlen and published by . This book was released on 1975 with total page 574 pages. Available in PDF, EPUB and Kindle. Book excerpt:

High Resolution NMR

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Publisher : Elsevier
ISBN 13 : 0323161855
Total Pages : 369 pages
Book Rating : 4.3/5 (231 download)

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Book Synopsis High Resolution NMR by : Edwin D. Becker

Download or read book High Resolution NMR written by Edwin D. Becker and published by Elsevier. This book was released on 2012-12-02 with total page 369 pages. Available in PDF, EPUB and Kindle. Book excerpt: High Resolution NMR: Theory and Chemical Applications discusses the principles and theory of nuclear magnetic resonance and how this concept is used in the chemical sciences. This book is written at an intermediate level, with mathematics used to augment verbal descriptions of the phenomena. This text pays attention to developing and interrelating four approaches – the steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The style of this book is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. This book begins with a description of the basic physics, together with a brief account of the historical development of the field. It looks at the study of NMR in liquids, including high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. This book is intended to assist chemistry graduate students, advanced undergraduate students, or researchers to understand NMR at a fundamental level. This text also provides illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins.

Review of Progress in Quantitative Nondestructive Evaluation

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Publisher : Springer Science & Business Media
ISBN 13 : 1461528488
Total Pages : 2393 pages
Book Rating : 4.4/5 (615 download)

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Book Synopsis Review of Progress in Quantitative Nondestructive Evaluation by : Donald O. Thompson

Download or read book Review of Progress in Quantitative Nondestructive Evaluation written by Donald O. Thompson and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 2393 pages. Available in PDF, EPUB and Kindle. Book excerpt: These Proceedings, consisting of Parts A and B, contain the edited versions of most of the papers presented at the annual Review of Progress in Quantitative Nondestructive Evaluation held at the University of California San Diego, in La Jolla, California on July 19- July 24, 1992. The Review was organized by the Center for NDE at Iowa State University and the Ames Laboratory of the USDOE in cooperation with a number of organizations including the Air Force Wright Laboratory Materials Directorate, the American Society for Nondestructive Testing, the Center for NDE at Johns Hopkins University, the Department of Energy, the Federal Aviation Administration, the National Institute of Standards and Technology, the National Science Foundation IndustrylUniversity Cooperative Research Centers, and the Working Group in Quantitative NDE. This year's Review of Progress in QNDE was attended by approximately 475 participants from the U. S. and many foreign countries who presented over 380 papers. With such a large volume of work to review, the meeting was divided into 36 sessions with as many as four sessions running concurrently. The Review covered all phases of NDE research and development from fundamental investigations to engineering applications or inspection systems, and it included all methods of inspection science from acoustics to x-rays. During the last twenty years, the participants of the Review have contributed to its steady growth. Thanks to their efforts, the Review is today one of the largest and most significant gatherings of NDE researchers and engineers anywhere in the world.

Advances in Planar Lipid Bilayers and Liposomes

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Publisher : Academic Press
ISBN 13 : 0080554539
Total Pages : 283 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Advances in Planar Lipid Bilayers and Liposomes by : A. Leitmannova Liu

Download or read book Advances in Planar Lipid Bilayers and Liposomes written by A. Leitmannova Liu and published by Academic Press. This book was released on 2011-08-09 with total page 283 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advances in Planar Lipid Bilayers and Liposomes, Volume 6, continues to include invited chapters on a broad range of topics, covering both main arrangements of the reconstituted system, namely planar lipid bilayers and spherical liposomes. The invited authors present the latest results in this exciting multidisciplinary field of their own research group. Many of the contributors working in both fields over many decades were in close collaboration with the late Prof. H. Ti Tien, the founding editor of this book series. There are also chapters written by some of the younger generation of scientists included in this series. This volume keeps in mind the broader goal with both systems, planar lipid bilayers and spherical liposomes, which is the further development of this interdisciplinary field worldwide. Contributions from newcomers and established and experienced researchers Exploring theoretically and experimentally the planar lipid bilayer systems and spherical liposomes This volume is dedicated to mark the Bilayer Lipid Membranes 45th anniversary

Selective Averaging in High Resolution Liquid-state NMR

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Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (127 download)

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Book Synopsis Selective Averaging in High Resolution Liquid-state NMR by : Jens Daniel Haller

Download or read book Selective Averaging in High Resolution Liquid-state NMR written by Jens Daniel Haller and published by . This book was released on 2021 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Annual Reports on NMR Spectroscopy

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Publisher : Academic Press
ISBN 13 : 0128209755
Total Pages : 422 pages
Book Rating : 4.1/5 (282 download)

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Book Synopsis Annual Reports on NMR Spectroscopy by :

Download or read book Annual Reports on NMR Spectroscopy written by and published by Academic Press. This book was released on 2020-09-25 with total page 422 pages. Available in PDF, EPUB and Kindle. Book excerpt: Annual Reports on NMR Spectroscopy, has established itself as a premier resource for both specialists and non-specialists who are looking to become familiar with new techniques and applications pertaining to NMR spectroscopy. Serves as the premier resource for learning the new techniques and applications of NMR spectroscopy Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)

Principles of Magnetic Resonance

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Publisher : Springer Science & Business Media
ISBN 13 : 366209441X
Total Pages : 662 pages
Book Rating : 4.6/5 (62 download)

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Book Synopsis Principles of Magnetic Resonance by : Charles P. Slichter

Download or read book Principles of Magnetic Resonance written by Charles P. Slichter and published by Springer Science & Business Media. This book was released on 2013-04-17 with total page 662 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first edition of this book was written in 1961 when I was Morris Loeb Lecturer in Physics at Harvard. In the preface I wrote: "The problem faced by a beginner today is enormous. If he attempts to read a current article, he often finds that the first paragraph refers to an earlier paper on which the whole article is based, and with which the author naturally assumes familiarity. That reference in turn is based on another, so the hapless student finds himself in a seemingly endless retreat. I have felt that graduate students or others beginning research in magnetic resonance needed a book which really went into the details of calculations, yet was aimed at the beginner rather than the expert. " The original goal was to treat only those topics that are essential to an understanding of the literature. Thus the goal was to be selective rather than comprehensive. With the passage of time, important new concepts were becoming so all-pervasive that I felt the need to add them. That led to the second edition, which Dr. Lotsch, Physics Editor of Springer-Verlag, encouraged me to write and which helped launch the Springer Series in Solid-State Sciences. Now, ten years later, that book (and its 1980 revised printing) is no longer available. Meanwhile, workers in magnetic resonance have continued to develop startling new insights.

Perspectives on Solid State NMR in Biology

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Publisher : Springer Science & Business Media
ISBN 13 : 9401725799
Total Pages : 227 pages
Book Rating : 4.4/5 (17 download)

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Book Synopsis Perspectives on Solid State NMR in Biology by : S.R. Kiihne

Download or read book Perspectives on Solid State NMR in Biology written by S.R. Kiihne and published by Springer Science & Business Media. This book was released on 2013-03-14 with total page 227 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid state NMR is rapidly emerging as a universally applicable method for the characterization of ordered structures that cannot be studied with solution methods or diffraction techniques. This proceedings -; from a recent international workshop - captures an image of the latest developments and future directions for solid state NMR in biological research, particularly on membrane proteins. Detailed information on how hormones or drugs bind to their membrane receptor targets is needed, e.g. for rational drug design. Higher fields are bringing clear improvements, and the power of solid state NMR techniques for studying amorphous and membrane associated peptides, proteins and complexes is shown by examples of applications at ultra-high fields. Progress in protein expression, experimental design and data analysis are also presented by leaders in these research areas.

New Techniques in Solid-State NMR

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Publisher : Springer Science & Business Media
ISBN 13 : 9783540221685
Total Pages : 372 pages
Book Rating : 4.2/5 (216 download)

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Book Synopsis New Techniques in Solid-State NMR by : Jacek Klinowski

Download or read book New Techniques in Solid-State NMR written by Jacek Klinowski and published by Springer Science & Business Media. This book was released on 2004-12-10 with total page 372 pages. Available in PDF, EPUB and Kindle. Book excerpt: With contributions by numerous experts

Nuclear Magnetic Resonance of Liquid Crystals

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Publisher : Springer Science & Business Media
ISBN 13 : 1468402080
Total Pages : 268 pages
Book Rating : 4.4/5 (684 download)

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Book Synopsis Nuclear Magnetic Resonance of Liquid Crystals by : Ronald Y. Dong

Download or read book Nuclear Magnetic Resonance of Liquid Crystals written by Ronald Y. Dong and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt: Liquid crystals have become ubiquitous in the displays for electronic devices, ranging from wrist watches to laptop computers. Nuclear magnetic resonance is one of the important mechanisms for determining their structures tures and properties. This book covers NMR techniques used in studying liquid crystals and present up to date results from such studies. Ronald Dong has worked on NMR in liquid crystals for much of his professional career. Topics covered include: Nuclear spin dynamics, orientational order, molecular field theories of liquid-crystal molecules, nuclear spin relaxation, spin relaxation, rotational and translational dynamics, internal dynamics of liquid-crystal molecules, NMR in liquid crystals; an appendix covers rotations, Euler angles and Wigner rotation matrices.

12th Annual Conference on Composites and Advanced Ceramic Materials, Part 2 of 2, Volume 9, Issue 9/10

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Publisher : John Wiley & Sons
ISBN 13 : 0470315210
Total Pages : 477 pages
Book Rating : 4.4/5 (73 download)

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Book Synopsis 12th Annual Conference on Composites and Advanced Ceramic Materials, Part 2 of 2, Volume 9, Issue 9/10 by : John B. Wachtman

Download or read book 12th Annual Conference on Composites and Advanced Ceramic Materials, Part 2 of 2, Volume 9, Issue 9/10 written by John B. Wachtman and published by John Wiley & Sons. This book was released on 2009-09-28 with total page 477 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume is part of the Ceramic Engineering and Science Proceeding (CESP) series. This series contains a collection of papers dealing with issues in both traditional ceramics (i.e., glass, whitewares, refractories, and porcelain enamel) and advanced ceramics. Topics covered in the area of advanced ceramic include bioceramics, nanomaterials, composites, solid oxide fuel cells, mechanical properties and structural design, advanced ceramic coatings, ceramic armor, porous ceramics, and more.