Calibration Methods of Laser-Induced Breakdown Spectroscopy

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ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (115 download)

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Book Synopsis Calibration Methods of Laser-Induced Breakdown Spectroscopy by : Hongbo Fu

Download or read book Calibration Methods of Laser-Induced Breakdown Spectroscopy written by Hongbo Fu and published by . This book was released on 2018 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser-induced breakdown spectroscopy (LIBS) has gained great attention over the past two decades due to its many advantages, such as needless sample preparation, capability of remote measurement and fast multielement simultaneous analysis. However, because of its inherent uncertainty features of plasma, it is still a big challenge for LIBS community worldwide to realize high sensitivity and accurate quantitative analysis. Currently, many chemometric analytical methods have been applied to LIBS calibration analysis, including univariate regression, multivariate regression, principal component regression (PCR), partial least squares regression (PLSR) and so on. In addition, appropriate sample and spectral pretreatment can effectively improve the analytical performance (id est, limit of detection (LOD), accuracy and repeatability) of LIBS. In this chapter, we briefly summarize the progress of these calibration methods and their applications on LIBS and provide our recommendations.

Handbook of Laser-Induced Breakdown Spectroscopy

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Publisher : John Wiley & Sons
ISBN 13 : 1118567366
Total Pages : 452 pages
Book Rating : 4.1/5 (185 download)

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Book Synopsis Handbook of Laser-Induced Breakdown Spectroscopy by : David A. Cremers

Download or read book Handbook of Laser-Induced Breakdown Spectroscopy written by David A. Cremers and published by John Wiley & Sons. This book was released on 2013-03-15 with total page 452 pages. Available in PDF, EPUB and Kindle. Book excerpt: Starting from fundamentals and moving through a thorough discussion of equipment, methods, and techniques, the Handbook of Laser-Induced Breakdown Spectroscopy provides a unique reference source that will be of value for many years to come for this important new analysis method. The authors, with a total of over 60 years of experience in the LIBS method, use a combination of tutorial discussions ranging from basic principles up to more advanced descriptions along with extensive figures and photographs to clearly explain topics addressed in the text. In this second edition, chapters on the use of statistical analysis and advances in detection of weapons of mass destruction have been added. Tables of data related to analysis with LIBS have been updated. The Handbook of Laser-Induced Breakdown Spectroscopy, Second Edition: provides a thorough but understandable discussion of the basic principles of the method based on atomic emission spectroscopy, including recently available data leading to better characterization of the LIBS plasma; presents a discussion of the many advantages of the method along with limitations, to provide the reader a balanced overview of capabilities of the method; describes LIBS instrumentation ranging from basic set-ups to more advanced configurations; presents a comprehensive discussion of the different types of components (laser, spectrometers, detectors) that can be used for LIBS apparatuses along with suggestions for their use, as well as an up-to-date treatment of the newest advances and capabilities of LIBS instruments; presents the analytical capabilities of the method in terms of detection limits, accuracy, and precision of measurements for a variety of different sample types; discusses methods of sampling different media such as gases, liquids, and solids; presents an overview of some real-world applications of the method, with new emphasis on sampling of biologically and physically dangerous materials; provides an up-to-date list of references to LIBS literature along with the latest detection limits and a unique list of element detection limits using a uniform analysis method; provides annotated examples of LIBS spectra which can serve as references for the general reader and will be especially useful for those starting out in the field.

Laser-induced Breakdown Spectroscopy (LIBS)

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Publisher :
ISBN 13 : 9780511246692
Total Pages : 640 pages
Book Rating : 4.2/5 (466 download)

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Book Synopsis Laser-induced Breakdown Spectroscopy (LIBS) by : Andrzej W. Miziolek

Download or read book Laser-induced Breakdown Spectroscopy (LIBS) written by Andrzej W. Miziolek and published by . This book was released on 2014-05-14 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the first comprehensive reference explaining the fundamentals of the LIBS phenomenon, its history and its fascinating applications across eighteen chapters written by recognized leaders in the field. This book will be of significant interest to researchers in chemical and materials analysis within academia and industry.

Laser Induced Breakdown Spectroscopy (LIBS)

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Publisher : John Wiley & Sons
ISBN 13 : 1119758424
Total Pages : 2162 pages
Book Rating : 4.1/5 (197 download)

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Book Synopsis Laser Induced Breakdown Spectroscopy (LIBS) by : Vivek K. Singh

Download or read book Laser Induced Breakdown Spectroscopy (LIBS) written by Vivek K. Singh and published by John Wiley & Sons. This book was released on 2023-03-14 with total page 2162 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser Induced Breakdown Spectroscopy (LIBS) Essential resource covering the field of LIBS, with respect to its fundamentals, established and novel applications, and future prospects Laser Induced Breakdown Spectroscopy (LIBS), presents in two comprehensive volumes a thorough discussion of the basic principles of the method, including important recently available data which can lead to a better characterization of the LIBS plasma. This extensive work contains detailed discussions on the lasers, spectrometers, and detectors that can be used for LIBS apparatuses and describes various instrumentation, ranging from basic setups to more advanced configurations. As a modern resource, the work includes the newest advances and capabilities of LIBS instruments, featuring the recent developments of Dual-Pulse LIBS, Femtosecond LIBS, and Micro-LIBS as well as their applications. Throughout, the contributions discuss the analytical capabilities of the method in terms of detection limits, accuracy, and precision of measurements for a variety of samples. Lastly, an extensive range of applications is presented, including food technology, environmental science, nuclear reactors, nanoscience and nanotechnology, and biological and biomedical developments. Sample topics covered within the work include: iagnostics of laser induced plasma (LIP): LIBS plasma and its characteristics, factors affecting the LIBS plasma, methods of enhancing LIBS sensitivity, and LTE/non-LTE plasmas Instrumental developments in LIBS: light collection system and spectral detection systems, handheld LIBS, deep sea LIBS, and industrial sorters and analyzers Femtosecond laser ablation: laser-matter interaction, laser absorption, energy transport, ablation mechanisms and threshold, and plasma characterization Micro-analysis and LIBS imaging: microjoule laser sources, scaling libs to microjoule energies, micrometer scaling, advanced applications, and future prospects Spectroscopic and analytical scientists working with LIBS will find this wide-ranging reference immensely helpful in developing LIBS instrumentation and applications. Researchers and students in natural sciences and related programs of study will be able to use the work to acquire foundational knowledge on the method and learn about cutting-edge advancements being made in the field.

Calibration and Validation of Analytical Methods

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Publisher : BoD – Books on Demand
ISBN 13 : 1789230845
Total Pages : 176 pages
Book Rating : 4.7/5 (892 download)

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Book Synopsis Calibration and Validation of Analytical Methods by : Mark Stauffer

Download or read book Calibration and Validation of Analytical Methods written by Mark Stauffer and published by BoD – Books on Demand. This book was released on 2018-04-25 with total page 176 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book seeks to introduce the reader to current methodologies in analytical calibration and validation. This collection of contributed research articles and reviews addresses current developments in the calibration of analytical methods and techniques and their subsequent validation. Section 1, "Introduction," contains the Introductory Chapter, a broad overview of analytical calibration and validation, and a brief synopsis of the following chapters. Section 2 "Calibration Approaches" presents five chapters covering calibration schemes for some modern analytical methods and techniques. The last chapter in this section provides a segue into Section 3, "Validation Approaches," which contains two chapters on validation procedures and parameters. This book is a valuable source of scientific information for anyone interested in analytical calibration and validation.

Laser-Induced Breakdown Spectroscopy

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Publisher : Elsevier
ISBN 13 : 0128188308
Total Pages : 624 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Laser-Induced Breakdown Spectroscopy by : Jagdish P. Singh

Download or read book Laser-Induced Breakdown Spectroscopy written by Jagdish P. Singh and published by Elsevier. This book was released on 2020-06-02 with total page 624 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser-Induced Breakdown Spectroscopy, Second Edition, covers the basic principles and latest developments in instrumentation and applications of Laser Induced Breakdown Spectroscopy (LIBS). Written by active experts in the field, it serves as a useful resource for analytical chemists and spectroscopists, as well as graduate students and researchers engaged in the fields of combustion, environmental science, and planetary and space exploration. This fully revised second edition includes several new chapters on new LIBS techniques as well as several new applications, including flame and off-gas measurement, pharmaceutical samples, defense applications, carbon sequestration and site monitoring, handheld instruments, and more. LIBS has rapidly developed into a major analytical technology with the capability of detecting all chemical elements in a sample, of real- time response, and of close-contact or stand-off analysis of targets. It does not require any sample preparation, unlike conventional spectroscopic analytical techniques. Samples in the form of solids, liquids, gels, gases, plasmas, and biological materials (like teeth, leaves, or blood) can be studied with almost equal ease. This comprehensive reference introduces the topic to readers in a simple, direct, and accessible manner for easy comprehension and maximum utility. Covers even more applications of LIBS beyond the first edition, including combustion, soil physics, environment, and life sciences Includes new chapters on LIBS techniques that have emerged in the last several years, including Femtosecond LIBS and Molecular LIBS Provides inspiration for future developments in this rapidly growing field in the concluding chapter

Laser Induced Breakdown Spectroscopy

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Publisher : Cambridge University Press
ISBN 13 : 1139458310
Total Pages : 615 pages
Book Rating : 4.1/5 (394 download)

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Book Synopsis Laser Induced Breakdown Spectroscopy by : Andrzej W. Miziolek

Download or read book Laser Induced Breakdown Spectroscopy written by Andrzej W. Miziolek and published by Cambridge University Press. This book was released on 2006-09-07 with total page 615 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is a comprehensive reference explaining the fundamentals of the LIBS phenomenon, its history and its fascinating applications across eighteen chapters written by recognized leaders in the field. This book will be of significant interest to researchers in chemical and materials analysis within academia and industry.

Laser-Induced Breakdown Spectroscopy

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Publisher : Elsevier
ISBN 13 : 0080551017
Total Pages : 455 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Laser-Induced Breakdown Spectroscopy by : Jagdish P. Singh

Download or read book Laser-Induced Breakdown Spectroscopy written by Jagdish P. Singh and published by Elsevier. This book was released on 2007-10-03 with total page 455 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser induced breakdown spectroscopy (LIBS) is basically an emission spectroscopy technique where atoms and ions are primarily formed in their excited states as a result of interaction between a tightly focused laser beam and the material sample. The interaction between matter and high-density photons generates a plasma plume, which evolves with time and may eventually acquire thermodynamic equilibrium. One of the important features of this technique is that it does not require any sample preparation, unlike conventional spectroscopic analytical techniques. Samples in the form of solids, liquids, gels, gases, plasmas and biological materials (like teeth, leaf or blood) can be studied with almost equal ease. LIBS has rapidly developed into a major analytical technology with the capability of detecting all chemical elements in a sample, of real- time response, and of close-contact or stand-off analysis of targets. The present book has been written by active specialists in this field, it includes the basic principles, the latest developments in instrumentation and the applications of LIBS . It will be useful to analytical chemists and spectroscopists as an important source of information and also to graduate students and researchers engaged in the fields of combustion, environmental science, and planetary and space exploration. * Recent research work* Possible future applications* LIBS Principles

Remote Compositional Analysis

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Publisher : Cambridge University Press
ISBN 13 : 110718620X
Total Pages : 655 pages
Book Rating : 4.1/5 (71 download)

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Book Synopsis Remote Compositional Analysis by : Janice L. Bishop

Download or read book Remote Compositional Analysis written by Janice L. Bishop and published by Cambridge University Press. This book was released on 2019-11-28 with total page 655 pages. Available in PDF, EPUB and Kindle. Book excerpt: Comprehensive overview of the spectroscopic, mineralogical, and geochemical techniques used in planetary remote sensing.

Laser-Induced Breakdown Spectroscopy

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Publisher : Springer Science & Business Media
ISBN 13 : 3642206689
Total Pages : 547 pages
Book Rating : 4.6/5 (422 download)

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Book Synopsis Laser-Induced Breakdown Spectroscopy by : Reinhard Noll

Download or read book Laser-Induced Breakdown Spectroscopy written by Reinhard Noll and published by Springer Science & Business Media. This book was released on 2012-01-14 with total page 547 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is a comprehensive source of the fundamentals, process parameters, instrumental components and applications of laser-induced breakdown spectroscopy (LIBS). The effect of multiple pulses on material ablation, plasma dynamics and plasma emission is presented. A heuristic plasma modeling allows to simulate complex experimental plasma spectra. These methods and findings form the basis for a variety of applications to perform quantitative multi-element analysis with LIBS. These application potentials of LIBS have really boosted in the last years ranging from bulk analysis of metallic alloys and non-conducting materials, via spatially resolved analysis and depth profiling covering measuring objects in all physical states: gaseous, liquid and solid. Dedicated chapters present LIBS investigations for these tasks with special emphasis on the methodical and instrumental concepts as well as the optimization strategies for a quantitative analysis. Requirements, concepts, design and characteristic features of LIBS instruments are described covering laboratory systems, inspections systems for in-line process control, mobile systems and remote systems. State-of-the-art industrial applications of LIBS systems are presented demonstrating the benefits of inline process control for improved process guiding and quality assurance purposes.

Laser-induced Breakdown Spectrometry

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Publisher : Nova Publishers
ISBN 13 : 9781560728399
Total Pages : 194 pages
Book Rating : 4.7/5 (283 download)

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Book Synopsis Laser-induced Breakdown Spectrometry by : Yong-Ill Lee

Download or read book Laser-induced Breakdown Spectrometry written by Yong-Ill Lee and published by Nova Publishers. This book was released on 2000 with total page 194 pages. Available in PDF, EPUB and Kindle. Book excerpt: When the output from a pulsed laser is forced onto a small spot of a sample, optically induced plasma, called laser-induced plasma (LIP) is formed at the surface. The plasma is formed when the laser power density exceeds the breakdown threshold value of the surface. The plasma can be used in sampling but is proposed as a source for atomic emission spectrometry (AES). In this case the technique is referred to as laser induced breakdown (emission) spectrometry (LIBS). The spectrally and temporally resolved detection and subsequent determination of the specific atomic emission reveals analytical information about the elemental composition of the sample, including solids, liquids and gases. This book is devoted to the analytical technique of laser-induced breakdown spectrometry. An introduction covering some basic principles of atomic emission spectrometry, analytical performance characteristics, and a comparison to more conventional techniques provides background information for the reader. The book is then conveniently divided into three parts: the first part described the instrumentation required and options available, the second part on fundamental studies of the laser plasma, and the third part on applications. Finally the future development of LIBS is presented.

Laser Spectroscopy for Material Characterization

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ISBN 13 :
Total Pages : 115 pages
Book Rating : 4.:/5 (883 download)

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Book Synopsis Laser Spectroscopy for Material Characterization by : Krishna Kanth Ayyalasomayajula

Download or read book Laser Spectroscopy for Material Characterization written by Krishna Kanth Ayyalasomayajula and published by . This book was released on 2014 with total page 115 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser-Induced Breakdown Spectroscopy (LIBS) is a powerful tool for performing chemical analysis measurements of materials, such as slurries, soils, plastics and powder samples. The LIBS technique has proven to be sensitive, selective and robust for rapid, in situ analysis. The focus of this dissertation is the optimization of laser spectroscopic sensing methodologies for material characterization. The applications of the LIBS technique to slurry samples is very challenging due to the water content (~80%). A new sample preparation method called "spin-on-glass" was adopted to reduce the water content in slurry samples and improve the LIBS signal. The feasibility of using the new sampling method with a LIBS system was tested by applying multivariate analysis to the LIBS spectral data. The calibration results demonstrated that the LIBS technique with the new sampling method could successfully predict the elemental concentrations of slurry samples qualitatively and quantitatively. The possibility of developing a LIBS-based sensor system for total carbon quantification in soil samples was studied. The soil samples were studied in pellet form and the calibration models were developed by using simple linear regression (SLR) and multiple linear regression (MLR) analysis. It was found that both SLR- and MLR-based calibrations successfully predicted the carbon concentration in an unknown sample with relative accuracy (RA) within 8%. The LIBS experimental setup was designed, developed and tested for the determination of elemental impurities in plastic calibration standards that are used in dual-energy computed tomography (CT) scanning for petrophysical applications. Univariate calibration (UC) and multiple linear regression (MLR) analysis were used to develop calibration models. From this study, it was concluded that MLR improved the calibration results and data derived from the LIBS analysis enhanced the predictive capabilities of dual-energy CT scanning in general. A comparative study was performed for quantification of strontium (Sr) in an aluminum (Al) batch with both the atomic and molecular LIBS emissions. The calibration models were developed using SLR analysis and the limits of detection (LOD) were obtained. The study confirmed that molecular LIBS could be used for quantification of Sr in a binary mixture.

Laser-Induced Breakdown Spectroscopy

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Publisher : Springer
ISBN 13 : 3642450857
Total Pages : 577 pages
Book Rating : 4.6/5 (424 download)

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Book Synopsis Laser-Induced Breakdown Spectroscopy by : Sergio Musazzi

Download or read book Laser-Induced Breakdown Spectroscopy written by Sergio Musazzi and published by Springer. This book was released on 2014-07-08 with total page 577 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book deals with the Laser-Induced Breakdown Spectroscopy (LIBS) a widely used atomic emission spectroscopy technique for elemental analysis of materials. It is based on the use of a high-power, short pulse laser excitation. The book is divided into two main sections: the first one concerning theoretical aspects of the technique, the second one describing the state of the art in applications of the technique in different scientific/technological areas. Numerous examples of state of the art applications provide the readers an almost complete scenario of the LIBS technique. The LIBS theoretical aspects are reviewed. The book helps the readers who are less familiar with the technique to understand the basic principles. Numerous examples of state of the art applications give an almost complete scenario of the LIBS technique potentiality. These examples of applications may have a strong impact on future industrial utilization. The authors made important contributions to the development of this field.

Emerging Developments and Applications of Low Temperature Plasma

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Publisher : IGI Global
ISBN 13 : 1799884007
Total Pages : 239 pages
Book Rating : 4.7/5 (998 download)

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Book Synopsis Emerging Developments and Applications of Low Temperature Plasma by : Shahzad, Aamir

Download or read book Emerging Developments and Applications of Low Temperature Plasma written by Shahzad, Aamir and published by IGI Global. This book was released on 2021-12-17 with total page 239 pages. Available in PDF, EPUB and Kindle. Book excerpt: Low temperature plasma in medicine is a new field that rose from the research in the application of cold plasmas in bioengineering. Plasma medicine is an innovative and promising multidisciplinary novel field of research covering plasma physics, life sciences, and clinical medicine to apply physical plasma for therapeutic applications. Emerging Developments and Applications of Low Temperature Plasma explores all areas of experimental, computational, and theoretical study of low temperature and atmospheric plasmas and provides a collection of exciting new research on the fundamental aspects of low temperature and pressure plasmas and their applications. Covering topics such as carbon nanotubes, foodborne pathogens, and plasma formation, this book is an essential resource for research groups, plasma-based industries, plasma aerodynamics industries, metal and cutlery industries, medical institutions, researchers, and academicians.

Chemometrics in Spectroscopy

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Publisher : Academic Press
ISBN 13 : 0128053305
Total Pages : 1090 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Chemometrics in Spectroscopy by : Howard Mark

Download or read book Chemometrics in Spectroscopy written by Howard Mark and published by Academic Press. This book was released on 2018-07-13 with total page 1090 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemometrics in Spectroscopy, Second Edition, provides the reader with the methodology crucial to apply chemometrics to real world data. It allows scientists using spectroscopic instruments to find explanations and solutions to their problems when they are confronted with unexpected and unexplained results. Unlike other books on these topics, it explains the root causes of the phenomena that lead to these results. While books on NIR spectroscopy sometimes cover basic chemometrics, they do not mention many of the advanced topics this book discusses. In addition, traditional chemometrics books do not cover spectroscopy to the point of understanding the basis for the underlying phenomena. The second edition has been expanded with 50% more content covering advances in the field that have occurred in the last 10 years, including calibration transfer, units of measure in spectroscopy, principal components, clinical data reporting, classical least squares, regression models, spectral transfer, and more. Written in the column format of the authors’ online magazine Presents topical and important chapters for those involved in analysis work, both research and routine Focuses on practical issues in the implementation of chemometrics for NIR Spectroscopy Includes a companion website with 350 additional color figures that illustrate CLS concepts

Laser-Induced Breakdown Spectroscopy in Biological, Forensic and Materials Sciences

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Publisher : Springer Nature
ISBN 13 : 303114502X
Total Pages : 312 pages
Book Rating : 4.0/5 (311 download)

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Book Synopsis Laser-Induced Breakdown Spectroscopy in Biological, Forensic and Materials Sciences by : Gábor Galbács

Download or read book Laser-Induced Breakdown Spectroscopy in Biological, Forensic and Materials Sciences written by Gábor Galbács and published by Springer Nature. This book was released on 2022-12-13 with total page 312 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book offers a comprehensive overview of recent advances in the area of laser-induced breakdown spectroscopy (LIBS), focusing on its application to biological, forensic and materials sciences. LIBS, which was previously mainly used by physicists, chemists and in the industry, has now become a very useful tool with great potential in these other fields as well. LIBS has a unique set of characteristics including minimal destructiveness, remote sensing capabilities, potential portability, extremely high information content, trace analytical sensitivity and high throughput. With its content divided into two main parts, this book provides not only an introduction to the analytical capabilities and methodology, but also an overview of the results of recent applications in the above fields. The application-oriented, multidisciplinary approach of this work is also reflected in the diversity of the expert contributors. Given its breadth, this book will appeal to students, researchers and professionals interested in solving analytical/diagnostic/material characterization tasks with the application of LIBS.

Exploring and Testing the Assumptions of Calibration-free Laser Induced Breakdown Spectroscopy

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Publisher :
ISBN 13 :
Total Pages : 44 pages
Book Rating : 4.:/5 (11 download)

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Book Synopsis Exploring and Testing the Assumptions of Calibration-free Laser Induced Breakdown Spectroscopy by : Benjamin Skinner

Download or read book Exploring and Testing the Assumptions of Calibration-free Laser Induced Breakdown Spectroscopy written by Benjamin Skinner and published by . This book was released on 2019 with total page 44 pages. Available in PDF, EPUB and Kindle. Book excerpt: