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Author : Stefan Mogck
Publisher :
ISBN 13 : 9789036720076
Total Pages : 132 pages
Book Rating : 4.7/5 (2 download)
Download or read book Transmission Electron Microscopy Studies of Interfaces in Multi-component Systems written by Stefan Mogck and published by . This book was released on 2004 with total page 132 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : L.M Clarebrough
Publisher : Routledge
ISBN 13 : 1351453203
Total Pages : 435 pages
Book Rating : 4.3/5 (514 download)
Download or read book Electron Microscopy of Interfaces in Metals and Alloys written by L.M Clarebrough and published by Routledge. This book was released on 2021-09-01 with total page 435 pages. Available in PDF, EPUB and Kindle. Book excerpt: Electron Microscopy of Interfaces in Metals and Alloys examines the structure of interfaces in metals and alloys using transmission electron microscopy. The book presents quantitative methods of analysis and reviews the most significant work on interface structure over the last 20 years. It provides the first book description of the methods used for quantitative identification of Burgers vectors of interfacial dislocations, including the geometric analysis of periodicities in interface structure and the comparison of experimental and theoretical electron micrographs. The book explores low- and high-angle grain boundaries and interphase interfaces between neighboring grains, emphasizing interfacial dislocations and rigid-body displacements to the structure and properties of interfaces. It also analyzes the use of two-beam images and diffraction patterns for analysis and studies n-beam lattice imaging. The book includes numerous worked examples of the analysis of the structure of grain boundaries and interphase interfaces, which are particularly useful to those who need to consider the nature of intercrystalline interfaces.
Author : C.T Forwood
Publisher : CRC Press
ISBN 13 : 9780750301169
Total Pages : 446 pages
Book Rating : 4.3/5 (11 download)
Download or read book Electron Microscopy of Interfaces in Metals and Alloys written by C.T Forwood and published by CRC Press. This book was released on 1991-01-01 with total page 446 pages. Available in PDF, EPUB and Kindle. Book excerpt: Electron Microscopy of Interfaces in Metals and Alloys examines the structure of interfaces in metals and alloys using transmission electron microscopy. The book presents quantitative methods of analysis and reviews the most significant work on interface structure over the last 20 years. It provides the first book description of the methods used for quantitative identification of Burgers vectors of interfacial dislocations, including the geometric analysis of periodicities in interface structure and the comparison of experimental and theoretical electron micrographs. The book explores low- and high-angle grain boundaries and interphase interfaces between neighboring grains, emphasizing interfacial dislocations and rigid-body displacements to the structure and properties of interfaces. It also analyzes the use of two-beam images and diffraction patterns for analysis and studies n-beam lattice imaging. The book includes numerous worked examples of the analysis of the structure of grain boundaries and interphase interfaces, which are particularly useful to those who need to consider the nature of intercrystalline interfaces.
Author : Ugo Valdre
Publisher : Springer Science & Business Media
ISBN 13 : 1461595371
Total Pages : 321 pages
Book Rating : 4.4/5 (615 download)
Download or read book Surface and Interface Characterization by Electron Optical Methods written by Ugo Valdre and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 321 pages. Available in PDF, EPUB and Kindle. Book excerpt: The importance of real space imaging and spatially-resolved spectroscopy in many of the most significant problems of surface and interface behaviour is almost self evident. To join the expertise of the tradi tional surface scientist with that of the electron microscopist has however been a slow and difficult process. In the past few years remarkable progress has been achieved, including the development of new techniques of scanning transmission and reflection imaging as well as low energy microscopy, all carried out in greatly improved vacuum conditions. Most astonishing of all has been the advent of the scanning tunneling electron microscope providing atomic resolution in a manner readily compatible with most surface science diagnostic procedures. The problem of beam damage, though often serious, is increasingly well understood so that we can assess the reliability and usefulness of the results which can now be obtained in catalysis studies and a wide range of surface science applications. These new developments and many others in more established surface techniques are all described in this book, based on lectures given at a NATO Advanced Study Institute held in Erice, Sicily, at Easter 1987. It is regretted that a few lectures on low energy electron diffraction and channeling effects could not be included. Fifteen lecturers from seven different Countries and 67 students from 23 Countries and a wide variety of backgrounds attended the school.
Author : Jean Ling Lee
Publisher :
ISBN 13 :
Total Pages : 392 pages
Book Rating : 4.E/5 ( download)
Download or read book Scanning Transmission Electron Microscopy Studies of Interfaces Involving Yttrium Barium Copper Oxide written by Jean Ling Lee and published by . This book was released on 1996 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Christian Rockenhäuser
Publisher : Springer
ISBN 13 : 3658087935
Total Pages : 117 pages
Book Rating : 4.6/5 (58 download)
Download or read book Electron Microscopical Investigation of Interdiffusion and Phase Formation at Gd2O3/CeO2- and Sm2O3/CeO2-Interfaces written by Christian Rockenhäuser and published by Springer. This book was released on 2015-03-17 with total page 117 pages. Available in PDF, EPUB and Kindle. Book excerpt: Christian Rockenhäuser adresses phase formation and cation interdiffusion of the GdxCe1-xO2-x/2-and SmxCe1-xO2-x/2-material systems at temperatures ranging from 970 to 1270°C. Diffusion couples with CeO2/Sm2O3 and CeO2/Gd2O3 interfaces were fabricated for the investigations. The resulting reaction phases were investigated utilizing transmission electron microscopy (TEM) and allow conclusions regarding the phase diagrams in the examined temperature range. A miscibility gap can be ruled out for GdxCe1-xO2-x/2 across the whole composition range. Cation interdiffusion coefficients were determined for both material systems by measuring and evaluating concentration profiles at the material interfaces. The activation enthalpies for interdiffusion were calculated using the temperature dependence of the interdiffusion coefficients. The study for the first time compiles comprehensively the previous results regarding the phase diagrams of the two material systems since 1923.
Author : Renu Sharma
Publisher : John Wiley & Sons
ISBN 13 : 3527347984
Total Pages : 389 pages
Book Rating : 4.5/5 (273 download)
Download or read book In-Situ Transmission Electron Microscopy Experiments written by Renu Sharma and published by John Wiley & Sons. This book was released on 2023-05-15 with total page 389 pages. Available in PDF, EPUB and Kindle. Book excerpt: In-Situ Transmission Electron Microscopy Experiments Design and execute cutting-edge experiments with transmission electron microscopy using this essential guide In-situ microscopy is a recently-discovered and rapidly-developing approach to transmission electron microscopy (TEM) that allows for the study of atomic and/or molecular changes and processes while they are in progress. Experimental specimens are subjected to stimuli that replicate near real-world conditions and their effects are observed at a previously unprecedented scale. Though in-situ microscopy is becoming an increasingly important approach to TEM, there are no current texts combining an up-to-date overview of this cutting-edge set of techniques with the experience of in-situ TEM professionals. In-Situ Transmission Electron Microscopy Experiments meets this need with a work that synthesizes the collective experience of myriad collaborators. It constitutes a comprehensive guide for planning and performing in-situ TEM measurements, incorporating both fundamental principles and novel techniques. Its combination of technical detail and practical how-to advice makes it an indispensable introduction to this area of research. In-Situ Transmission Electron Microscopy Experiments readers will also find: Coverage of the entire experimental process, from method selection to experiment design to measurement and data analysis Detailed treatment of multimodal and correlative microscopy, data processing and machine learning, and more Discussion of future challenges and opportunities facing this field of research In-Situ Transmission Electron Microscopy Experiments is essential for graduate students, post-doctoral fellows, and early career researchers entering the field of in-situ TEM.
Author : Rik Brydson
Publisher : John Wiley & Sons
ISBN 13 : 1119979900
Total Pages : 235 pages
Book Rating : 4.1/5 (199 download)
Download or read book Aberration-Corrected Analytical Transmission Electron Microscopy written by Rik Brydson and published by John Wiley & Sons. This book was released on 2011-08-02 with total page 235 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book is concerned with the theory, background, and practical use of transmission electron microscopes with lens correctors that can correct the effects of spherical aberration. The book also covers a comparison with aberration correction in the TEM and applications of analytical aberration corrected STEM in materials science and biology. This book is essential for microscopists involved in nanoscale and materials microanalysis especially those using scanning transmission electron microscopy, and related analytical techniques such as electron diffraction x-ray spectrometry (EDXS) and electron energy loss spectroscopy (EELS).
Author : C. Barry Carter
Publisher : Springer
ISBN 13 : 3319266519
Total Pages : 543 pages
Book Rating : 4.3/5 (192 download)
Download or read book Transmission Electron Microscopy written by C. Barry Carter and published by Springer. This book was released on 2016-08-24 with total page 543 pages. Available in PDF, EPUB and Kindle. Book excerpt: This text is a companion volume to Transmission Electron Microscopy: A Textbook for Materials Science by Williams and Carter. The aim is to extend the discussion of certain topics that are either rapidly changing at this time or that would benefit from more detailed discussion than space allowed in the primary text. World-renowned researchers have contributed chapters in their area of expertise, and the editors have carefully prepared these chapters to provide a uniform tone and treatment for this exciting material. The book features an unparalleled collection of color figures showcasing the quality and variety of chemical data that can be obtained from today’s instruments, as well as key pitfalls to avoid. As with the previous TEM text, each chapter contains two sets of questions, one for self assessment and a second more suitable for homework assignments. Throughout the book, the style follows that of Williams & Carter even when the subject matter becomes challenging—the aim is always to make the topic understandable by first-year graduate students and others who are working in the field of Materials Science Topics covered include sources, in-situ experiments, electron diffraction, Digital Micrograph, waves and holography, focal-series reconstruction and direct methods, STEM and tomography, energy-filtered TEM (EFTEM) imaging, and spectrum imaging. The range and depth of material makes this companion volume essential reading for the budding microscopist and a key reference for practicing researchers using these and related techniques.
Author : Lisa Anne Tietz
Publisher :
ISBN 13 :
Total Pages : 580 pages
Book Rating : 4.E/5 ( download)
Download or read book Transmission Electron Microscopy Studies of Nucleation, Growth and Interfaces in Ceramic Oxide Heterojunctions written by Lisa Anne Tietz and published by . This book was released on 1991 with total page 580 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Brent Fultz
Publisher : Springer Science & Business Media
ISBN 13 : 3662045168
Total Pages : 759 pages
Book Rating : 4.6/5 (62 download)
Download or read book Transmission Electron Microscopy and Diffractometry of Materials written by Brent Fultz and published by Springer Science & Business Media. This book was released on 2013-11-21 with total page 759 pages. Available in PDF, EPUB and Kindle. Book excerpt: Aims and Scope of the Book This textbook was written for advanced un dergraduate students and beginning graduate students with backgrounds in physical science. Its goal is to acquaint them, as quickly as possible, with the central concepts and some details of transmission electron microscopy (TEM) and x-ray diffractometry (XRD) that are important for the characterization of materials. The topics in this book are developed to a level appropriate for most modern materials characterization research using TEM and XRD. There are, of course, many specialties that have attained a higher level of sophistication than presented here. The content of this book has been chosen in part to provide the background needed for a transition to these research specialties, or to other techniques such as neutron diffractometry. Although the book includes many practical details and examples, it does not cover some topics important for laboratory work. Perhaps the most obvious is the omission of specimen preparation methods for TEM. Beneath the details of principle and practice lies a larger goal of unifying the concepts common to both TEM and XRD. Coherence and wave interfer ence are conceptually similar for both x-ray waves and electron wavefunctions.
Author : Alina Bruma
Publisher : CRC Press
ISBN 13 : 0429512732
Total Pages : 164 pages
Book Rating : 4.4/5 (295 download)
Download or read book Scanning Transmission Electron Microscopy written by Alina Bruma and published by CRC Press. This book was released on 2020-12-20 with total page 164 pages. Available in PDF, EPUB and Kindle. Book excerpt: Scanning Transmission Electron Microscopy is focused on discussing the latest approaches in the recording of high-fidelity quantitative annular dark-field (ADF) data. It showcases the application of machine learning in electron microscopy and the latest advancements in image processing and data interpretation for materials notoriously difficult to analyze using scanning transmission electron microscopy (STEM). It also highlights strategies to record and interpret large electron diffraction datasets for the analysis of nanostructures. This book: Discusses existing approaches for experimental design in the recording of high-fidelity quantitative ADF data Presents the most common types of scintillator-photomultiplier ADF detectors, along with their strengths and weaknesses. Proposes strategies to minimize the introduction of errors from these detectors and avenues for dealing with residual errors Discusses the practice of reliable multiframe imaging, along with the benefits and new experimental opportunities it presents in electron dose or dose-rate management Focuses on supervised and unsupervised machine learning for electron microscopy Discusses open data formats, community-driven software, and data repositories Proposes methods to process information at both global and local scales, and discusses avenues to improve the storage, transfer, analysis, and interpretation of multidimensional datasets Provides the spectrum of possibilities to study materials at the resolution limit by means of new developments in instrumentation Recommends methods for quantitative structural characterization of sensitive nanomaterials using electron diffraction techniques and describes strategies to collect electron diffraction patterns for such materials This book helps academics, researchers, and industry professionals in materials science, chemistry, physics, and related fields to understand and apply computer-science–derived analysis methods to solve problems regarding data analysis and interpretation of materials properties.
Author : Alain Claverie
Publisher : John Wiley & Sons
ISBN 13 : 1118579054
Total Pages : 280 pages
Book Rating : 4.1/5 (185 download)
Download or read book Transmission Electron Microscopy in Micro-nanoelectronics written by Alain Claverie and published by John Wiley & Sons. This book was released on 2013-01-29 with total page 280 pages. Available in PDF, EPUB and Kindle. Book excerpt: Today, the availability of bright and highly coherent electron sources and sensitive detectors has radically changed the type and quality of the information which can be obtained by transmission electron microscopy (TEM). TEMs are now present in large numbers not only in academia, but also in industrial research centers and fabs. This book presents in a simple and practical way the new quantitative techniques based on TEM which have recently been invented or developed to address most of the main challenging issues scientists and process engineers have to face to develop or optimize semiconductor layers and devices. Several of these techniques are based on electron holography; others take advantage of the possibility of focusing intense beams within nanoprobes. Strain measurements and mappings, dopant activation and segregation, interfacial reactions at the nanoscale, defect identification and specimen preparation by FIB are among the topics presented in this book. After a brief presentation of the underlying theory, each technique is illustrated through examples from the lab or fab.
Author :
Publisher :
ISBN 13 :
Total Pages : 700 pages
Book Rating : 4.3/5 (91 download)
Download or read book Scientific and Technical Aerospace Reports written by and published by . This book was released on 1995 with total page 700 pages. Available in PDF, EPUB and Kindle. Book excerpt: Lists citations with abstracts for aerospace related reports obtained from world wide sources and announces documents that have recently been entered into the NASA Scientific and Technical Information Database.
Author : David J. Lohse
Publisher : Springer Science & Business Media
ISBN 13 : 1475755597
Total Pages : 304 pages
Book Rating : 4.4/5 (757 download)
Download or read book Interfacial Aspects of Multicomponent Polymer Materials written by David J. Lohse and published by Springer Science & Business Media. This book was released on 2013-04-17 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: In August, 1996, the ACS Division of Polymeric Materials: Science and Engineering hosted a symposium on Interfacial Aspects of Multicomponent Polymer Materials at the Orlando, Florida, American Chemical Society meeting. Over 50 papers and posters were presented. The symposium proper was preceded by a one-day workshop, where the. basics of this relatively new field were developed. This edited book is a direct outcome of the symposium and workshop. Every object in the universe has surfaces and interfaces. A surface is defined as that part of a material in contact with either a gas or a vacuum. An interface is defined as that part of a material in contact with a condensed phase, be it liquid or solid. Surfaces of any substance are different from their interior. The appearance of surface or interfacial tension is one simple manifestation. Polymer blends and composites usually contain very finely divided phases, which are literally full of interfaces. Because interfaces are frequently weak mechanically, they pose special problems in the manufacture of strong, tough plastics, adhesives, elastomers, coatings, and fibers. This book provides a series of papers addressing this issue. Some papers delineate the nature of the interface both chemically and physically. The use of newer instrumental methods and new theories are described. Concepts of interdiffusion and entanglement are developed. Other papers describe state-of-the-art approaches to improving the interface, via graft and block copolymers, direct covalent bonding, hydrogen bonding, and more.
Author : Richard Y. Hashimoto
Publisher :
ISBN 13 : 9781423545101
Total Pages : 100 pages
Book Rating : 4.5/5 (451 download)
Download or read book Analytical Transmission Electron Microscopy Studies on Copper-Alumina Interfaces written by Richard Y. Hashimoto and published by . This book was released on 1999-06-01 with total page 100 pages. Available in PDF, EPUB and Kindle. Book excerpt: A diffusion bonded copper-alumina interface had been studied using energy dispersive x-ray spectroscopy (EDX) and electron energy loss spectroscopy (EELS). Investigations of polycrystalline alumina showed that silica, a common commercial impurity, was present at the triple junctions in the form of fine mullite crystals in a glassy, silicon rich phase. Silicon was also detected along the alumina grain boundaries near triple junctions. There was no observed diffusion of Cu into alumina or alumina into copper. TEM results indicated no interface phase in the these vacuum formed samples. EDX studies of the interfaces revealed that silicon was present in varying concentrations from 1.O at.% to 10.0 at.%. Using spatial difference, PEELS at the interface showed two distinct residuals: a coordination similar to an aluminosilicate for silicon rich areas and a coordination similar to a metal to metal coordination for low silicon regions. Comparison of the Si rich interface residual PEELS spectra to that of the alumina triple junction PEELS spectra showed that the interface had atomic environments similar to that of as aluminosilicate, such as mullite. The interface results suggest that Si segregation may contribute to the observed higher strength of the metal-ceramic composite by void filling and modified bond character.
Author : Litao Sun
Publisher : Springer Nature
ISBN 13 : 9811968454
Total Pages : 378 pages
Book Rating : 4.8/5 (119 download)
Download or read book In-Situ Transmission Electron Microscopy written by Litao Sun and published by Springer Nature. This book was released on 2023-03-11 with total page 378 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book focuses on in-situ transmission electron microscopy (TEM), an investigatory technique used to observe a sample’s response to a given stimulus (including electron irradiation, thermal excitation, mechanical force, optical excitation, electric and magnetic fields) at the nanoscale in real time. The book introduces readers to the technical strategy behind the in-situ technique and its developments. It reviews the research frontiers of using in-situ TEM in energy conversion and storage, catalysis, nanomaterials synthesis, nanoelectronics, etc. Furthermore, it discusses the future prospects for in-situ TEM. The book offers a valuable guide for all undergraduate and graduate students who are interested in TEM characterization technology. It also serves as a reference source on cutting-edge in-situ techniques for researchers and engineers.
