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The Critical Process Conditions For Controlled Growth Of Iron Oxide Nanoparticles Synthesized Using Continuous Hydrothermal Synthesis
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Book Synopsis The Critical Process Conditions for Controlled Growth of Iron Oxide Nanoparticles Synthesized Using Continuous Hydrothermal Synthesis by : Brett Craig Kriedemann
Download or read book The Critical Process Conditions for Controlled Growth of Iron Oxide Nanoparticles Synthesized Using Continuous Hydrothermal Synthesis written by Brett Craig Kriedemann and published by . This book was released on 2014 with total page 386 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Continuous and Batch Hydrothermal Synthesis of Metal Oxide Nanoparticles and Metal Oxide-activated Carbon Nanocomposites by : Chunbao Xu
Download or read book Continuous and Batch Hydrothermal Synthesis of Metal Oxide Nanoparticles and Metal Oxide-activated Carbon Nanocomposites written by Chunbao Xu and published by . This book was released on 2006 with total page 258 pages. Available in PDF, EPUB and Kindle. Book excerpt: The continuous hydrothermal technique was also extended to materials other than metal oxides by synthesizing lithium iron phosphate. Differences in the particle sizes obtained using the batch and continuous methods were shown to be due to the different mechanisms of particle formation in the two techniques. Better particle characteristics (size, size distribution and morphology) were obtained using the continuous hydrothermal technique than using the batch hydrothermal method.
Book Synopsis Near-critical and supercritical hydrothermal flow synthesis of metal oxide nanoparticles and hybrid metal oxide nanoparticles presenting clickable anchors by : Daschner de Tercero, Maren
Download or read book Near-critical and supercritical hydrothermal flow synthesis of metal oxide nanoparticles and hybrid metal oxide nanoparticles presenting clickable anchors written by Daschner de Tercero, Maren and published by KIT Scientific Publishing. This book was released on 2014-11-26 with total page 298 pages. Available in PDF, EPUB and Kindle. Book excerpt: "The continuous hydrothermal flow synthesis of functionalized and non-functionalized nanoparticle dispersions was pursued. Besides improving the understanding of the relationship between process variables and the resulting nanoparticle dispersions, the usability of this process was extended by introducing clickable organic modifiers, a step toward the development of a convenient and versatile process for the synthesis of metal oxide nanoparticles with universal anchors on their surface."--Publisher's website.
Book Synopsis Handbook of Solid State Chemistry, 6 Volume Set by : Richard Dronskowski
Download or read book Handbook of Solid State Chemistry, 6 Volume Set written by Richard Dronskowski and published by John Wiley & Sons. This book was released on 2017-10-23 with total page 3912 pages. Available in PDF, EPUB and Kindle. Book excerpt: This most comprehensive and unrivaled compendium in the field provides an up-to-date account of the chemistry of solids, nanoparticles and hybrid materials. Following a valuable introductory chapter reviewing important synthesis techniques, the handbook presents a series of contributions by about 150 international leading experts -- the "Who's Who" of solid state science. Clearly structured, in six volumes it collates the knowledge available on solid state chemistry, starting from the synthesis, and modern methods of structure determination. Understanding and measuring the physical properties of bulk solids and the theoretical basis of modern computational treatments of solids are given ample space, as are such modern trends as nanoparticles, surface properties and heterogeneous catalysis. Emphasis is placed throughout not only on the design and structure of solids but also on practical applications of these novel materials in real chemical situations.
Book Synopsis Green Nanoparticles by : Jayanta Kumar Patra
Download or read book Green Nanoparticles written by Jayanta Kumar Patra and published by Springer Nature. This book was released on 2020-04-06 with total page 395 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanotechnology is the application of science to control matter at the molecular level. It has become one of the most promising applied technologies in all areas of science. Nanoparticles have multi-functional properties and have created very interesting applications in various fields such as medicine, nutrition, bioenergy, agriculture and the environment. But the biogenic syntheses of monodispersed nanoparticles with specific sizes and shapes have been a challenge in biomaterial science. Nanoparticles are of great interest due to their extremely small size and large surface-to-volume ratio, which lead to both chemical and physical differences in their properties (e.g., mechanical properties, biological and sterical properties, catalytic activity, thermal and electrical conductivity, optical absorption and melting point) compared to bulk of the same chemical composition. Recently, however, synthesizing metal nanoparticles using green technology via microorganisms, plants, viruses, and so on, has been extensively studied and has become recognized as a green and efficient way for further exploiting biological systems as convenient nanofactories. Thus the biological synthesis of nanoparticles is increasingly regarded as a rapid, ecofriendly, and easily scaled-up technology. Today researchers are developing new techniques and materials using nanotechnology that may be suitable for plants to boost their native functions. Recently, biological nanoparticles were found to be more pharmacologically active than physico-chemically synthesized nanoparticles. Various applications of biosynthesized nanoparticles have been discovered, especially in the field of biomedical research, such as applications to specific delivery of drugs, use for tumor detection, angiogenesis, genetic disease and genetic disorder diagnosis, photoimaging, and photothermal therapy. Further, iron oxide nanoparticles have been applied to cancer therapy, hyperthermia, drug delivery, tissue repair, cell labeling, targeting and immunoassays, detoxification of biological fluids, magnetic resonance imaging, and magnetically responsive drug delivery therapy. Nanoparticle synthesis for plant byproducts for biomedical applications has vast potential. This book offers researchers in plant science and biomedicine the latest research and opportunity to develop new tools for the synthesis of environmentally friendly and cost-effective nanoparticles for applications in biomedicine as well as other various fields.
Book Synopsis Iron Oxide Nanoparticles for Biomedical Applications by : Sophie Laurent
Download or read book Iron Oxide Nanoparticles for Biomedical Applications written by Sophie Laurent and published by Elsevier. This book was released on 2017-10-20 with total page 336 pages. Available in PDF, EPUB and Kindle. Book excerpt: Iron Oxide Nanoparticles for Biomedical Applications: Synthesis, Functionalization and Application begins with several chapters covering the synthesis, stabilization, physico-chemical characterization and functionalization of iron oxide nanoparticles. The second part of the book outlines the various biomedical imaging applications that currently take advantage of the magnetic properties of iron oxide nanoparticles. Brief attention is given to potential iron oxide based therapies, while the final chapter covers nanocytotoxicity, which is a key concern wherever exposure to nanomaterials might occur. This comprehensive book is an essential reference for all those academics and professionals who require thorough knowledge of recent and future developments in the role of iron oxide nanoparticles in biomedicine. Unlocks the potential of iron oxide nanoparticles to transform diagnostic imaging techniques Contains full coverage of new developments and recent research, making this essential reading for researchers and engineers alike Explains the synthesis, processing and characterization of iron oxide nanoparticles with a view to their use in biomedicine
Book Synopsis Synthesis, Surface Functionalization, and Biological Testing of Iron Oxide Nanoparticles for Development as a Cancer Therapeutic by : Stanley Eugene Gilliland (III)
Download or read book Synthesis, Surface Functionalization, and Biological Testing of Iron Oxide Nanoparticles for Development as a Cancer Therapeutic written by Stanley Eugene Gilliland (III) and published by . This book was released on 2015 with total page 214 pages. Available in PDF, EPUB and Kindle. Book excerpt: Iron oxide nanoparticles are highly researched for their use in biomedical applications such as drug delivery, diagnosis, and therapy. The inherent biodegradable and biocompatible nanoparticle properties make them highly advantageous in nanomedicine. The magnetic properties of iron oxide nanoparticles make them promising candidates for magnetic fluid hyperthermia applications. Designing an efficient iron oxide nanoparticle for hyperthermia requires synthetic, surface functionalization, stability, and biological investigations. This research focused on the following three areas: optimizing synthesis conditions for maximum radiofrequency induced magnetic hyperthermia, designing a simple and modifiable surface functionalization method for specific or broad biological stability, and in vitro and in vivo testing of surface functionalized iron oxide nanoparticles in delivering effective hyperthermia or radiotherapy. The benzyl alcohol modified seed growth method of synthesizing iron oxide nanoparticles using iron acetylacetonate as an iron precursor was investigated to identify significant nanoparticle properties that effect radiofrequency induced magnetic hyperthermia. Investigation of this synthesis under atmospheric conditions revealed a combination of thermal decomposition and oxidation-reduction mechanisms that can produce nanoparticles with larger crystallite sizes and decreased size distributions. Nanoparticles were easily surface functionalized with (3-Glycidyloxypropyl)trimethoxysilane (GLYMO) without the need for organic-aqueous phase transfer methods. The epoxy ring on GLYMO facilitated post-modifications via a base catalyzed epoxy ring opening to obtain nanoparticles with different terminal groups. Glycine, serine, [gamma]-aminobutryic acid (ABA), (S)-( - )-4-amino-2-hydroxybutyric acid (SAHBA), ethylenediamine, and tetraethylenepentamine were successful in modifying GLYMO coated-iron oxide nanoparticles to provide colloidal and varying biological stability while also allowing for further conjugation of chemotherapeutics or radiotherapeutics. The colloidal stability of cationic and anionic nanoparticles in several biologically relevant media was studied to address claims of increased cellular uptake for cationic nanoparticles. The surface functionalized iron oxide nanoparticles were investigated to determine effects on cellular uptake and viability. In vitro tests were used to confirm the ability of iron oxide nanoparticles to provide effective hyperthermia treatment. S-2-(4-Aminobenzyl)-1,4,7,10-tetraazacyclododecane tetraacetic acid (DOTA) was coupled to SAHBA and carboxymethylated polyvinyl alcohol surface functionalized iron oxide nanoparticles and radiolabeled with 177Lu. The capability of radiolabeled iron oxide nanoparticles for delivering radiation therapy to a U87MG murine orthotopic xenograft model of glioblastoma was initially investigated.
Book Synopsis The Iron Oxides by : Rochelle M. Cornell
Download or read book The Iron Oxides written by Rochelle M. Cornell and published by John Wiley & Sons. This book was released on 2006-12-13 with total page 703 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book brings together in one, compact volume all aspects of the available information about the iron oxides. It presents a coherent, up to date account of the properties, reactions and mechanisms of formation of these compounds. In addition, there are chapters dealing with iron oxides in rocks and soils, as biominerals and as corrosion products together with methods of synthesis and the numerous application of these compounds. Their role in the environment is also discussed. The authors are experts in the field of iron oxides and have worked on all the topics covered. Much recent data from the authors' own laboratories is included and opportunities for further research are indicated. Special features are the electron micrographs and colour plates together with the many different spectra used to illustrate properties and aspects of behaviour. Numerous tables and graphs enable trends and relationships to be seen at a glance. The book concludes with an extensive bibliography. This book should prove invaluable to industry and to all researchers who, whatever their background and level of experience, are interested in this rapidly expanding field. It is an essential volume for any scientific library and is now in its second, completely revised and extended edition!
Book Synopsis Handbook of Hydrothermal Technology by : K. Byrappa
Download or read book Handbook of Hydrothermal Technology written by K. Byrappa and published by William Andrew. This book was released on 2012-12-31 with total page 796 pages. Available in PDF, EPUB and Kindle. Book excerpt: Quartz, zeolites, gemstones, perovskite type oxides, ferrite, carbon allotropes, complex coordinated compounds and many more -- all products now being produced using hydrothermal technology. Handbook of Hydrothermal Technology brings together the latest techniques in this rapidly advancing field in one exceptionally useful, long-needed volume.The handbook provides a single source for understanding how aqueous solvents or mineralizers work under temperature and pressure to dissolve and recrystallize normally insoluble materials, and decompose or recycle any waste material. The result, as the authors show in the book, is technologically the most efficient method in crystal growth, materials processing, and waste treatment. The book gives scientists and technologists an overview of the entire subject including: À Evolution of the technology from geology to widespread industrial use. À Descriptions of equipment used in the process and how it works.À Problems involved with the growth of crystals, processing of technological materials, environmental and safety issues.À Analysis of the direction of today's technology. In addition, readers get a close look at the hydrothermal synthesis of zeolites, fluorides, sulfides, tungstates, and molybdates, as well as native elements and simple oxides. Delving into the commercial production of various types, the authors clarify the effects of temperature, pressure, solvents, and various other chemical components on the hydrothermal processes. Gives an overview of the evolution of Hydrothermal Technology from geology to widespread industrial use Describes the equipment used in the process and how it works Discusses problems involved with the growth of crystals, processing of technological materials, and environmental and safety issues
Download or read book Nanotechnology written by Sunipa Roy and published by CRC Press. This book was released on 2017-09-18 with total page 299 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nano particles have created a high interest in recent years by virtue of their unusual mechanical, electrical, optical and magnetic properties and find wide applications in all fields of engineering. This edited volume aims to present the latest trends and updates in nanogenerators, thin film solar cells and green synthesis of metallic nanoparticles with a focus on nanostructured semiconductor devices. Exclusive chapter on electrical transport of nanostructure explains device physics for material properties for reduced dimensions. Additionally, the text describes the functionality of metallic nanoparticles and their application in molecular imaging and optical metamaterials. Piezoelectric nanogenerators has been touched upon from the energy perspective as well. Key Features: • Organized contents on Nanogenerators, VOC sensing, nanoelectronics, and NEMS. • Discusses eco-friendly green synthesis methods for metallic nanoparticles. • Touches upon low power nano devices (e.g. nanogenerators) for energy harvesting with quantum mechanical study. • Thin film/heterojunction based high efficiency solar cell addressed aimed at reducing global energy consumption.
Book Synopsis Spinel Nanoferrites by : Surender K. Sharma
Download or read book Spinel Nanoferrites written by Surender K. Sharma and published by Springer Nature. This book was released on 2021-10-29 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book highlights the complexity of spinel nanoferrites, their synthesis, physio-chemical properties and prospective applications in the area of advanced electronics, microwave devices, biotechnology as well as biomedical sciences. It presents an overview of spinel nanoferrites: synthesis, properties and applications for a wide audience: from beginners and graduate-level students up to advanced specialists in both academic and industrial sectors. There are 15 chapters organized into four main sections. The first section of the book introduces the readers to spinel ferrites and their applications in advanced electronics industry including microwave devices, whereas the second section mainly focus on the synthesis strategy and their physio-chemical properties. The last sections of the book highlight the importance of this class of nanomaterials in the field of biotechnology and biomedical sector with a special chapter on water purification.
Book Synopsis Iron Oxide Nanoparticles for Biomedical Applications by : Sophie Laurent
Download or read book Iron Oxide Nanoparticles for Biomedical Applications written by Sophie Laurent and published by Elsevier. This book was released on 2017-10-10 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Iron Oxide Nanoparticles for Biomedical Applications: Synthesis, Functionalization and Application begins with several chapters covering the synthesis, stabilization, physico-chemical characterization and functionalization of iron oxide nanoparticles. The second part of the book outlines the various biomedical imaging applications that currently take advantage of the magnetic properties of iron oxide nanoparticles. Brief attention is given to potential iron oxide based therapies, while the final chapter covers nanocytotoxicity, which is a key concern wherever exposure to nanomaterials might occur. This comprehensive book is an essential reference for all those academics and professionals who require thorough knowledge of recent and future developments in the role of iron oxide nanoparticles in biomedicine.
Book Synopsis Nanoparticle Technology Handbook by : Masuo Hosokawa
Download or read book Nanoparticle Technology Handbook written by Masuo Hosokawa and published by Elsevier. This book was released on 2007-10-19 with total page 645 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanoparticle technology, which handles the preparation, processing, application and characterisation of nanoparticles, is a new and revolutionary technology. It becomes the core of nanotechnology as an extension of the conventional Fine Particle / Powder Technology. Nanoparticle technology plays an important role in the implementation of nanotechnology in many engineering and industrial fields including electronic devices, advanced ceramics, new batteries, engineered catalysts, functional paint and ink, Drug Delivery System, biotechnology, etc.; and makes use of the unique properties of the nanoparticles which are completely different from those of the bulk materials. This new handbook is the first to explain complete aspects of nanoparticles with many application examples showing their advantages and advanced development. There are handbooks which briefly mention the nanosized particles or their related applications, but no handbook describing the complete aspects of nanoparticles has been published so far. The handbook elucidates of the basic properties of nanoparticles and various nanostructural materials with their characterisation methods in the first part. It also introduces more than 40 examples of practical and potential uses of nanoparticles in the later part dealing with applications. It is intended to give readers a clear picture of nanoparticles as well as new ideas or hints on their applications to create new materials or to improve the performance of the advanced functional materials developed with the nanoparticles. * Introduces all aspects of nanoparticle technology, from the fundamentals to applications. * Includes basic information on the preparation through to the characterization of nanoparticles from various viewpoints * Includes information on nanostructures, which play an important role in practical applications.
Book Synopsis CRC Concise Encyclopedia of Nanotechnology by : Boris Ildusovich Kharisov
Download or read book CRC Concise Encyclopedia of Nanotechnology written by Boris Ildusovich Kharisov and published by CRC Press. This book was released on 2016-01-06 with total page 1203 pages. Available in PDF, EPUB and Kindle. Book excerpt: The CRC Concise Encyclopedia of Nanotechnology sets the standard against which all other references of this nature are measured. As such, it is a major resource for both skilled professionals and novices to nanotechnology.The book examines the design, application, and utilization of devices, techniques, and technologies critical to research at the
Book Synopsis The Synthesis of Novel Metal and Metal Oxide Nanoparticles with Applications Towards Catalysis by : Meredith Joanne McMurdo
Download or read book The Synthesis of Novel Metal and Metal Oxide Nanoparticles with Applications Towards Catalysis written by Meredith Joanne McMurdo and published by . This book was released on 2010 with total page 152 pages. Available in PDF, EPUB and Kindle. Book excerpt: This dissertation describes the synthesis of novel nanoparticles that are interesting for catalytic applications. The decomposition of RhCp(C2H4)2 and Rh(hfacac)(CO)2 were investigated, and the complex RhCp(C2H4)2 was successfully shown to decompose to rhodium nanoparticles. Analysis of the decomposition chemistry was used to control nanoparticle seed formation and growth. New stabilizer ligands, both polymeric and molecular, were attempted for the synthesis of rhodium nanoparticles. Polymeric stabilizers were screened as replacements for the widely used polyvinylpyrollidone (PVP) surfactant, however none afforded the high degree of control exhibited by PVP. However, molecular stabilizers were screened and small, monodisperse rhodium nanoparticles were synthesized with the stabilizer octadecylphosphonic acid, with a size and size dispersity of 1.92 +/-0.16 nm. A concurrent hydrogenation catalytic process was also utilized for the synthesis of small rhodium seed particles. In this nanoparticle synthesis, a rhodium precursor and a stabilizer were combined in the presence of an olefin and hydrogen, which aids in decomposition of the rhodium precursor to nanoparticles, and also catalytically converts the olefin to a saturated compound. The rate of hydrogen uptake was monitored and fit to a two-step autocatalytic mechanism correlated to nanoparticle formation and growth. Two new rhodium complexes were synthesized that contained a stabilizer ligand, however the most successful attempt to produce small, monodisperse rhodium nanoparticles by this process was with the rhodium source [(COD)Rh(NCCH3)2]BF4, and the stabilizer (Bu4N)2HPO4 in the presence of an equivalent of Proton Sponge0. Rhodium nanoparticles synthesized by this process have a size and size distribution of 1.88 +/-0.27 nm. The presence of olefin and hydrogen pressure of 42 psi was found to be ideal for the stabilization of nanoparticles during their formation. Also, reactant concentrations and the rate of the cyclohexene consumption are crucial to yield nanoparticles with this excellent size dispersity. Growth reactions with these small rhodium nanoparticles have been successful the synthesis of larger nanoparticles under conditions involving alternate stabilizers. The small nanoparticles were then tested and found to be useful as seed particles in the synthesis of larger rhodium nanoparticles. For each procedure, a mixture of 1-hexadecylamine, adamantane carboxylic acid, and 1,2-hexadecanediol was used to stabilize the nanoparticles. The use of synthesized seed particles allowed for the formation of tetrahedral (average edge length: 4.77 +/- 0.72 nm) or icosahedral shaped particles, depending on reaction temperature. Subsequent characterization revealed that approximately half of the tetrahedrally shaped nanoparticles are in fact triangular flat rafts, where one corner of the tetrahedron appears to be "cut off." However, the use of in situ seeds resulted in the formation of multipod structures. The multipods are single crystals with 2-8 arms per multipod, that propagate both the (110) and (111) directions. The synthesis and characterization of mixed-metal oxide spinel nanoparticles was then attempted for water oxidation catalysis. Nanoparticles of the compositions MnFe2O4 and CoFe2O4 (5.7 nm and 6.1 nm respectively) were synthesized according to a literature procedure with the stabilizers oleic acid and oleylamine, however they were characterized by ICP-OES to have low M:Fe (M = Mn, Co) ratios of 1:5 and 1:4 respectively. Nanoparticles of NiFe2O4 (8.0 nm) were also synthesized by a similar approach, and had the expected Ni:Fe ratio of 1:2 by ICP-OES. Cubic nanoparticles of Co3O4 were also synthesized, and through a subsequent cation exchange reaction with this material, CuxCo3-xO4 and NixCo3-xO4 nanoparticles could be synthesized with varying degrees of copper or nickel incorporation. Linear scan voltammograms were conducted on anodes modified with these nanoparticle materials. For the mixed-metal ferrites, CoFe2O4 showed the lowest overpotentials in the water oxidation reaction in the range of 0-100 mA cm-2. Copper modified Co3O4 nanoparticles had a lower onset potential than Co3O4 and performed with lower overpotentials at low current densities (20 mA cm-2). The nickel modified Co3O4 nanoparticles were superior to the other MxCo3-xO4 materials at all current densities measured (0-100 mA cm-2).
Book Synopsis Metal Oxide Chemistry and Synthesis by : Jean-Pierre Jolivet
Download or read book Metal Oxide Chemistry and Synthesis written by Jean-Pierre Jolivet and published by John Wiley & Sons. This book was released on 2000-10-19 with total page 352 pages. Available in PDF, EPUB and Kindle. Book excerpt: The precipitation of metal oxides from aqueous solutions creates nanoparticles with interesting solid state properties, thus building a bridge between solution chemistry and solid state chemistry. This book is the first monograph to deal with the formation of metal oxides from aqueous solutions with emphasis on the formation and physical chemistry of nanoparticles. Metal Oxide Chemistry and Synthesis: From Solution to Solid State * Provides a comprehensive introduction to the synthesis of finely divided materials * Presents the chemistry, physics and applications of these materials * Builds a bridge between classical solution chemistry and new developments in solid state chemistry * Introduces an important new area in inorganic chemistry Part I examines the mechanism of condensation of aqueous cations leading to polynuclear species or lattices, and rationalizes the behaviour of cations in precipitation phenomena by identifying pathways from soluble species to solids. The cation complex is also analysed in relation to the synthesis of some technologically interesting polymetallic oxides, e.g. ferroelectric, ferrimagnetic and supraconductor materials. Part II is devoted to the surface chemistry of oxide particles. The basic concepts relating to the reactivity of the oxide-solution interface are introduced and applied to various adsorption phenomena, such as aggregation, stability of particle size against ripening, etc. These properties are exploited for the synthesis of nanomaterials for a broad range of applictions such as ceramic powders, catalysts and nanocomposites. This will also be of interest to those wishing to understand geochemical and some biological processes. As well as being invaluable to researchers and postgraduate students of inorganic chemistry, this book will also be appreciated by solid-state chemists, materials scientists and colloid chemists with an interest in metal oxides.
Download or read book Perovskite Materials written by Likun Pan and published by BoD – Books on Demand. This book was released on 2016-02-03 with total page 652 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book summarizes the current state of the know-how in the field of perovskite materials: synthesis, characterization, properties, and applications. Most chapters include a review on the actual knowledge and cutting-edge research results. Thus, this book is an essential source of reference for scientists with research fields in energy, physics, chemistry and materials. It is also a suitable reading material for graduate students.
