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Synthesis And Characterization Of Hyperbranched Polyurea Urethanes
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Book Synopsis Synthesis and Characterization of Hyperbranched Poly(urea-urethane)s by :
Download or read book Synthesis and Characterization of Hyperbranched Poly(urea-urethane)s written by and published by . This book was released on 2004 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: The thesis aims to synthesize hyperbranched poly(urea-urethane) polymers (HPU) in one-pot method using commercially available monomers which are 2,4-toluylene diisocyanate (TDI) as aromatic diisocyanate and isophorone diisocyanate (IPDI) and 2(3-isocyanatopropyl) cyclohexylisocyanate (IPCI) as aliphatic diisocyanates. Those proposed diisocyanates were reacted with diethanolamine (DEA) or diisopropanolamine (DIPA). Conditions of polymerisation reactions were optimised. Complete structural analysis using 1H and 13C NMR for the obtained aromatic polymers was carried out. Degree of branching up to 70% was calculated. Aliphatic polymers have spectra with overlapped signals therefore, no full structural analysis was possible. Molar masses were determined using SEC/RI detector which shows that the prepared polymers have Mw values between 1600 g/mol and 106000 g/mol. Thermal analysis for different polymer systems showed that aliphatic HPU are more thermally stable and have values of glass transition temperature higher than aromatic ones. Modification of the end groups in the prepared hyperbranched polymers was carried out using three different modifiers and degree of modification up to 100%. Linear polymers based on the same diisocyanate monomers were prepared to compare the properties of hyperbranched systems with their linear analogs. Measurements of solution viscosity showed that HPU have lower solution viscosity values than their linear analogs of comparable molar masses. Rheological measurement of some polymer samples of different systems were carried out and showed that our hyperbranched systems exhibit a more elastic behavior than the linear polymers. Surface studies for thin films prepared from different polymer systems (hyperbranched, linear and modified) were carried out and the obtained thin films were characterized using light microscope, microglider, GC-MS, and AFM. Contact angle measurements showed that HPU have a relatively hydrophilic character. The modified.
Book Synopsis Synthesis and Characterization of Hyperbranched Poly(urea-urethane)s by : Mona Abdel Rehim
Download or read book Synthesis and Characterization of Hyperbranched Poly(urea-urethane)s written by Mona Abdel Rehim and published by . This book was released on 2004 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Porous Carbons – Hyperbranched Polymers – Polymer Solvation by : Timothy E. Long
Download or read book Porous Carbons – Hyperbranched Polymers – Polymer Solvation written by Timothy E. Long and published by Springer. This book was released on 2014-12-26 with total page 239 pages. Available in PDF, EPUB and Kindle. Book excerpt: The series Advances in Polymer Science presents critical reviews of the present and future trends in polymer and biopolymer science. It covers all areas of research in polymer and biopolymer science including chemistry, physical chemistry, physics, material science. The thematic volumes are addressed to scientists, whether at universities or in industry, who wish to keep abreast of the important advances in the covered topics. Advances in Polymer Science enjoy a longstanding tradition and good reputation in its community. Each volume is dedicated to a current topic, and each review critically surveys one aspect of that topic, to place it within the context of the volume. The volumes typically summarize the significant developments of the last 5 to 10 years and discuss them critically, presenting selected examples, explaining and illustrating the important principles, and bringing together many important references of primary literature. On that basis, future research directions in the area can be discussed. Advances in Polymer Science volumes thus are important references for every polymer scientist, as well as for other scientists interested in polymer science - as an introduction to a neighboring field, or as a compilation of detailed information for the specialist. Review articles for the individual volumes are invited by the volume editors. Single contributions can be specially commissioned. Readership: Polymer scientists, or scientists in related fields interested in polymer and biopolymer science, at universities or in industry, graduate students.
Book Synopsis Hyperbranched Polyesters for Polyurethane Coatings: Their Preparation, Structure and Crosslinking with Polyisocyanates by :
Download or read book Hyperbranched Polyesters for Polyurethane Coatings: Their Preparation, Structure and Crosslinking with Polyisocyanates written by and published by . This book was released on 2007 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: In this work, hyperbranched aromatic polyesters-polyphenols based on 4,4-bis(4' hydroxyƠphenyl)pentanoic acid (BHPPA) were prepared and, according to the authors knowledge, for the first time tested as precursors for polyurethane bulk resins and coatings. Comparison of poly-BHPPA with competing products The materials prepared in this work show better properties than their aliphatic polyester-polyol analoga based on 2,2-bis-(hydroxymethyl)propanoic acid (BHMPA). Especially, the solubility of poly-BHPPA in organic solvents is better and poly-BHPPAs also do not tend to microphase separation during their reaction with isocyanates, in contrast to poly-BHMPAs. The poly-BHPPA and the polyurethane networks made from them display higher Tg values than analogous poly- BHMPA compounds. Because of the high Tg of the reacting and final systems, curing must occur at elevated temperatures (90°C) in order to avoid undercure. The lower reactivity of phenolic OH groups prevents the reaction from being too fast at that temperature. A drawback of the polyurethanes based on the aromatic polyesters-polyols prepared is the lower thermal stability of their urethane bonds, if compared to aliphatic urethanes. An interesting possibility for future investigations would be the modification of the BHPPA monomer in order to change the OH functionality from phenolic to aliphatic OH, e.g. by replacement of the phenolic OH by hydroxymethyl or hydroxyethyl groups (requires a strong modification of the monomer synthesis) or simpler by reacting the phenolic OH of BHPPA with a suitable reagent like oxirane, which would lead to groups like O-CH2-CH2-OH in the place of the phenolic OH. Such a BHPPA modification should in turn yield modified "poly-BHPPA" polycondensates, which would combine the advantages of poly-BHPPA with those of aliphatic OH precursors of polyurethanes. Poly-BHPPA synthesis Hyperbranched polymers of the 4,4-bis-(4'-hydroxyphenyl)pentanoic acid (BHPPA) were synthesized successfully by t.
Book Synopsis Roadmap to Sustainable Textiles by : Ayşegül Körlü
Download or read book Roadmap to Sustainable Textiles written by Ayşegül Körlü and published by BoD – Books on Demand. This book was released on 2024-03-13 with total page 120 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book examines the relationships between sustainability and textiles in terms of environmental, social, and economic development. It includes six chapters that address a variety of subjects, ranging from green chemistry to digitalization in the textile industry.
Download or read book Advanced Tribology written by Jianbin Luo and published by Springer Science & Business Media. This book was released on 2010-07-16 with total page 1040 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Advanced Tribology" is the proceedings of the 5th China International Symposium on Tribology (held every four years) and the 1st International Tribology Symposium of IFToMM, held in Beijing 24th-27th September 2008. It contains seven parts: lubrication; friction and wear; micro/nano-tribology; tribology of coatings, surface and interface; biotribology; tribo-chemistry; industry tribology. The book reflects the recent progress in the fields such as lubrication, friction and wear, coatings, and precision manufacture etc. in the world. The book is intended for researchers, engineers and graduate students in the field of tribology, lubrication, mechanical production and industrial design. The editors Jianbin Luo, Yonggang Meng, Tianmin Shao and Qian Zhao are all the professors at the State Key Lab of Tribology, Tsinghua University, Beijing.
Book Synopsis Synthesis, Characterization, and Applications of Graphitic Carbon Nitride by : Sabu Thomas
Download or read book Synthesis, Characterization, and Applications of Graphitic Carbon Nitride written by Sabu Thomas and published by Elsevier. This book was released on 2022-09-21 with total page 428 pages. Available in PDF, EPUB and Kindle. Book excerpt: Synthesis, Characterization and Applications of Graphitic Carbon Nitride: An Uprising Carbonaceous Material offers an up-to-date record on the major findings and observations relating to graphitic carbon nitride-based systems, elaborately covering all the aspects of carbon nitride as chemical stable and pollution-free materials that are easy to prepare in a cost-effective way, along with their applications in photocatalytic degradation of pollutants, photocatalytic hydrogen generation, carbon dioxide reduction, disinfection, sensors and supercapacitors. Graphitic carbon nitride (g-C3N4) is a fascinating visible light photocatalyst, which possesses many properties that can be used for many applications.This makes the book an indispensable reference for (post)-graduate students, researchers in academia and industry, and engineers working in the field of graphitic carbon-nitride-based systems. - Includes the applications of graphitic carbon nitride as a photocatalyst for the reduction of CO2 - Describes the synthesis structure and properties of graphitic carbon nitride-based systems - Deals with the development of graphitic carbon nitride-based nanocomposites - Includes hydrogen production via water splitting by using graphitic carbon nitride - Describes the applications of graphitic carbon nitride in the field of sensors, solar cells, fuel cells and in analytical chemistry
Book Synopsis Advances in Polyurethane Biomaterials by : Stuart L. Cooper
Download or read book Advances in Polyurethane Biomaterials written by Stuart L. Cooper and published by Woodhead Publishing. This book was released on 2016-01-23 with total page 720 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advances in Polyurethane Biomaterials brings together a thorough review of advances in the properties and applications of polyurethanes for biomedical applications. The first set of chapters in the book provides an important overview of the fundamentals of this material with chapters on properties and processing methods for polyurethane. Further sections cover significant uses such as their tissue engineering and vascular and drug delivery applications Written by an international team of leading authors, the book is a comprehensive and essential reference on this important biomaterial. - Brings together in-depth coverage of an important material, essential for many advanced biomedical applications - Connects the fundamentals of polyurethanes with state-of-the-art analysis of significant new applications, including tissue engineering and drug delivery - Written by a team of highly knowledgeable authors with a range of professional and academic experience, overseen by an editor who is a leading expert in the field
Book Synopsis Springer Handbook of Nanomaterials by : Robert Vajtai
Download or read book Springer Handbook of Nanomaterials written by Robert Vajtai and published by Springer Science & Business Media. This book was released on 2013-08-20 with total page 1234 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Springer Handbook of Nanomaterials covers the description of materials which have dimension on the "nanoscale". The description of the nanomaterials in this Handbook follows the thorough but concise explanation of the synergy of structure, properties, processing and applications of the given material. The Handbook mainly describes materials in their solid phase; exceptions might be e.g. small sized liquid aerosols or gas bubbles in liquids. The materials are organized by their dimensionality. Zero dimensional structures collect clusters, nanoparticles and quantum dots, one dimensional are nanowires and nanotubes, while two dimensional are represented by thin films and surfaces. The chapters in these larger topics are written on a specific materials and dimensionality combination, e.g. ceramic nanowires. Chapters are authored by well-established and well-known scientists of the particular field. They have measurable part of publications and an important role in establishing new knowledge of the particular field.
Book Synopsis Functional Biomaterials by : Sougata Jana
Download or read book Functional Biomaterials written by Sougata Jana and published by Springer Nature. This book was released on 2022-03-29 with total page 524 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book explores in depth a wide range of functional biomaterials-based systems for drug, gene delivery, and biomedical aspects. The chapters cover newer technologies such as polymeric micelle, pH-responsive biomaterials, stimuli-responsive hydrogels, silk fibroin, inorganic biomaterials, synthetic biomaterials, 3D printed biomaterials, metallic biomaterials, ceramic and hybrid biomaterials. It also describes the theranostic approaches for cancer therapy, the biomaterials-based nanofibers scaffolds in tissue engineering, as well as the strategies applications of metallic biomaterials for the medical and dental prosthetic field. This newer and updated approach will be attractive for biomedical engineering students working on materials science in the development of novel drug delivery strategies. The book will be an important reference for researchers and professionals working on biomaterial research in the pharmaceutical and medical fields.
Book Synopsis Synthesis and Characterization of Polyurethane Prepolymers by : E. Lalioti
Download or read book Synthesis and Characterization of Polyurethane Prepolymers written by E. Lalioti and published by . This book was released on 1990 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Polyurethane Polymers: Composites and Nanocomposites by : Sabu Thomas
Download or read book Polyurethane Polymers: Composites and Nanocomposites written by Sabu Thomas and published by Elsevier. This book was released on 2017-08-17 with total page 635 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polyurethane Polymers: Composites and Nanocomposites concentrates on the composites and nanocomposites of polyurethane based materials. Polyurethane composites are a very important class of materials widely used in the biomedical and industrial field that offer numerous potential applications in many areas. This book discusses current research and identifies future research needs in the area. - Provides an elaborate coverage of the chemistry of polyurethane, its synthesis, and properties - Includes available characterization techniques - Relates types of polyurethanes to their potential properties - Discusses composites, nanocomposites options, and PU recycling
Book Synopsis Synthesis and Characterization of Polyurethane Ionomers by : Shih-Wa Wang
Download or read book Synthesis and Characterization of Polyurethane Ionomers written by Shih-Wa Wang and published by . This book was released on 2011 with total page 175 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Hyperbranched Polymers by : Deyue Yan
Download or read book Hyperbranched Polymers written by Deyue Yan and published by John Wiley & Sons. This book was released on 2011-05-04 with total page 414 pages. Available in PDF, EPUB and Kindle. Book excerpt: A much-needed overview of the state of the art of hyperbranched polymers The last two decades have seen a surge of interest in hyperbranched polymers due to their ease of synthesis on a large scale and their promising applications in diverse fields, from medicine to nanotechnology. Written by leading scientists in academia and industry, this book provides for the first time a comprehensive overview of the topic, bringing together in one complete volume a wealth of information previously available only in articles scattered across the literature. Drawing on their work at the cutting edge of this dynamic area of research, the authors cover everything readers need to know about hyperbranched polymers when designing highly functional materials. Clear, thorough discussions include: How irregular branching affects polymer properties and their potential applications Important theoretical basics, plus a useful summary of characterization techniques How hyperbranched polymers compare with dendrimers as well as linear polymers Future trends in the synthesis and application of hyperbranched polymers Geared to novices and experts alike, Hyperbranched Polymers is a must-have resource for anyone working in polymer architectures, polymer engineering, and functional materials. It is also useful for scientists in related fields who need a primer on the synthesis, theory, and applications of hyperbranched polymers.
Book Synopsis Synthesis and Characterization of Shape Memory Poly (epsilon-caprolactone) Polyurethane-ureas by : Hongfeng Ren
Download or read book Synthesis and Characterization of Shape Memory Poly (epsilon-caprolactone) Polyurethane-ureas written by Hongfeng Ren and published by . This book was released on 2012 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: A series of segmented poly (epsilon-caprolactone) polyurethane-ureas (PCLUUs) were prepared from poly (epsilon-caprolactone) (PCL) diol, different dissociates and chain extenders to improve the recovery stress of shape memory polymers. NMR and FT-IR were used to identify the structure of the synthesized shape memory polyurethane-ureas. Parameters such as soft segment content (molecular weight and content), chain extender and the rigidity of the main chain were investigated to understand the structure-property relationships of the shape memory polymer systems through DSC, DMA, physical property test, etc. Cyclic thermal mechanic tests were applied to measure the shape memory properties which showed that the recovery stress can be improved above 200% simply by modifying the chain extender. Meanwhile, the synthesis process was optimized to be similar to that of Spandex /LYCRA®. Continuous fibers were made from a wet spinning process, which indicated excellent spinnability of the polymer solution. Small angle neutron scattering (SANS) was used to study the morphology of the hard segment at different temperatures and stretch rates and found that the monodisperse rigid cylinder model fit the SANS data quite well. From the cylinder model, the radius of the cylinder increases with the increasing hard segment content. The SANS results revealed phase separation of hard and soft segments into nano scale domains.
Book Synopsis Novel Aliphatic Hyperbranched Polyurethanes by : Carolina Galmes Meerholff
Download or read book Novel Aliphatic Hyperbranched Polyurethanes written by Carolina Galmes Meerholff and published by . This book was released on 2005 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis of Polymers by : Dieter A. Schlüter
Download or read book Synthesis of Polymers written by Dieter A. Schlüter and published by John Wiley & Sons. This book was released on 2012-05-14 with total page 1229 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymers are huge macromolecules composed of repeating structural units. While polymer in popular usage suggests plastic, the term actually refers to a large class of natural and synthetic materials. Due to the extraordinary range of properties accessible, polymers have come to play an essential and ubiquitous role in everyday life - from plastics and elastomers on the one hand to natural biopolymers such as DNA and proteins on the other hand. The study of polymer science begins with understanding the methods in which these materials are synthesized. Polymer synthesis is a complex procedure and can take place in a variety of ways. This book brings together the "Who is who" of polymer science to give the readers an overview of the large field of polymer synthesis. It is a one-stop reference and a must-have for all Chemists, Polymer Chemists, Chemists in Industry, and Materials Scientists.
