Sustainable Synthesis Of Ciclopentene Derivatives Through Multicomponent Reactions In Continuous Flow Regime

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Sustainable synthesis of ciclopentene derivatives through multicomponent reactions in continuous flow regime

Author : Yoisel Bueno Broterson
Publisher : Editora Dialética
ISBN 13 : 6527006950
Total Pages : 113 pages
Book Rating : 4.5/5 (27 download)

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Book Synopsis Sustainable synthesis of ciclopentene derivatives through multicomponent reactions in continuous flow regime by : Yoisel Bueno Broterson

Download or read book Sustainable synthesis of ciclopentene derivatives through multicomponent reactions in continuous flow regime written by Yoisel Bueno Broterson and published by Editora Dialética. This book was released on 2024-02-01 with total page 113 pages. Available in PDF, EPUB and Kindle. Book excerpt: At present, a highly efficient tool for organic synthesis is the combination of organocatalytic and multicomponent processes. In the organocatalysis reaction it is possible to generate a reactive intermediate with high enantioselectivity and later, in the multicomponent stage, the complexity and structural diversity of the process increases. This strategy allows the synthesis of various analogues of optically active natural compounds and biologically relevant molecules of pharmacological interest, which are essential for human life. The current study, which is divided into three chapters, describes a methodology for the synthesis of tetrasubstituted cliclopentene derivatives from an organocatalytic reaction, followed by a multicomponent Ugi-type reaction under continuous flow regime. The use of green solvents in each reaction step, as well as the adoption of flow chemistry, led to obtaining products with high yield and enantiomerically-enriched in a fast and efficient manner, allowing the development of more sustainable strategies in synthetic chemistry.

Multicomponent Synthesis

Author : Basudeb Basu
Publisher : Walter de Gruyter GmbH & Co KG
ISBN 13 : 3110985314
Total Pages : 452 pages
Book Rating : 4.1/5 (19 download)

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Book Synopsis Multicomponent Synthesis by : Basudeb Basu

Download or read book Multicomponent Synthesis written by Basudeb Basu and published by Walter de Gruyter GmbH & Co KG. This book was released on 2023-12-31 with total page 452 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Organic Synthesis in Water

Author : P.A. Grieco
Publisher : Springer Science & Business Media
ISBN 13 : 940114950X
Total Pages : 321 pages
Book Rating : 4.4/5 (11 download)

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Book Synopsis Organic Synthesis in Water by : P.A. Grieco

Download or read book Organic Synthesis in Water written by P.A. Grieco and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 321 pages. Available in PDF, EPUB and Kindle. Book excerpt: The use of water as a medium for promoting organic reactions has been rather neglected in the development of organic synthesis, despite the fact that it is the solvent in which almost all biochemical processes take place. Chemists have only recently started to appreciate the enormous potential water has to offer in the development of new synthetic reactions and strategies, where it can offer benefits in both unique chemistry and reduced environmental impact. In this new book, the editor, well known for his contribution to the development of water as a useful medium in synthetic organic chemistry, has assembled an international team of authors, themselves at the forefront of research into the use of the unique properties of water carrying out organic transformations, to provide a timely and concise overview of current research. By focusing on the practical use of water in synthetic organic chemistry, and with the concern for the use of solvents in organic chemistry, professional chemists, particularly those involved in industrial research and development, will find this book an essential guide to the current state of the art, and a useful starting point in their own research. Academic chemists, including postgraduate and advanced undergraduate students, will find this book an invaluable guide to this exciting and important area of chemistry.

Side Reactions in Organic Synthesis

Author : Florencio Zaragoza Dörwald
Publisher : John Wiley & Sons
ISBN 13 : 3527604987
Total Pages : 389 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Side Reactions in Organic Synthesis by : Florencio Zaragoza Dörwald

Download or read book Side Reactions in Organic Synthesis written by Florencio Zaragoza Dörwald and published by John Wiley & Sons. This book was released on 2006-03-06 with total page 389 pages. Available in PDF, EPUB and Kindle. Book excerpt: Most syntheses in the chemical research laboratory fail and usually require several attempts before proceeding satisfactorily. Failed syntheses are not only discouraging and frustrating, but also cost a lot of time and money. Many failures may, however, be avoided by understanding the structure-reactivity relationship of organic compounds. This textbook highlights the competing processes and limitations of the most important reactions used in organic synthesis. By allowing chemists to quickly recognize potential problems this book will help to improve their efficiency and success-rate. A must for every graduate student but also for every chemist in industry and academia. Contents: 1 Organic Synthesis: General Remarks 2 Stereoelectronic Effects and Reactivity 3 The Stability of Organic Compounds 4 Aliphatic Nucleophilic Substitutions: Problematic Electrophiles 5 The Alkylation of Carbanions 6 The Alkylation of Heteroatoms 7 The Acylation of Heteroatoms 8 Palladium-Catalyzed C-C Bond Formation 9 Cyclizations 10 Monofunctionalization of Symmetric Difunctional Substrates

Recent Developments Of Diazo Compounds In Organic Synthesis

Author : Di Qiu
Publisher : World Scientific
ISBN 13 : 1786348918
Total Pages : 533 pages
Book Rating : 4.7/5 (863 download)

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Book Synopsis Recent Developments Of Diazo Compounds In Organic Synthesis by : Di Qiu

Download or read book Recent Developments Of Diazo Compounds In Organic Synthesis written by Di Qiu and published by World Scientific. This book was released on 2020-12-29 with total page 533 pages. Available in PDF, EPUB and Kindle. Book excerpt: Diazo compounds are versatile substances with diverse transformations in organic synthesis and other fields. Studies of diazo compounds have been ongoing for a very long time but still attract significant attention within the organic chemistry community, with new papers related to diazo compounds appearing at a daily pace. Over the past twenty years, there have been over fifty reviews and accounts related to the reactions of diazo compounds, but most of them cover limited aspects of diazo compounds. In addition to organic synthesis, diazo compounds have found applications in interdisciplinary fields such as material sciences, chemical biology and also polymerization.In this comprehensive book, the authors cover the most recent advances in the fields related to diazo compounds, including the application of donor-acceptor carbenes, carbene-based cross-coupling reactions and polymerizations, as well as the breakthrough in catalytic asymmetric carbene O-H, S-H, and N-H bond insertions. They also cover the application of flow chemistry in diazo reactions. The authors aim to provide a contemporary and comprehensive review for investigators engaged in or with interest in diazo compounds to boost further developments in this fascinating field.

Catalytic Asymmetric Synthesis

Author : Takahiko Akiyama
Publisher : John Wiley & Sons
ISBN 13 : 1119736412
Total Pages : 798 pages
Book Rating : 4.1/5 (197 download)

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Book Synopsis Catalytic Asymmetric Synthesis by : Takahiko Akiyama

Download or read book Catalytic Asymmetric Synthesis written by Takahiko Akiyama and published by John Wiley & Sons. This book was released on 2022-05-27 with total page 798 pages. Available in PDF, EPUB and Kindle. Book excerpt: Catalytic Asymmetric Synthesis Seminal text presenting detailed accounts of the most important catalytic asymmetric reactions known today This book covers the preparation of enantiomerically pure or enriched chemical compounds by use of chiral catalyst molecules. While reviewing the most important catalytic methods for asymmetric organic synthesis, this book highlights the most important and recent developments in catalytic asymmetric synthesis. Edited by two well-qualified experts, sample topics covered in the work include: Metal catalysis, organocatalysis, photoredox catalysis, enzyme catalysis C–H bond functionalization reactions Carbon–carbon bond formation reactions, carbon–halogen bond formation reactions, hydrogenations, polymerizations, flow reactions Axially chiral compounds Retaining the best of its predecessors but now thoroughly up to date with the important and recent developments in catalytic asymmetric synthesis, the 4th edition of Catalytic Asymmetric Synthesis serves as an excellent desktop reference and text for researchers and students, from upper-level undergraduates all the way to experienced professionals in industry or academia.

Immobilized Catalysts

Author : Andreas Kirschning
Publisher : Springer Science & Business Media
ISBN 13 : 9783540209157
Total Pages : 354 pages
Book Rating : 4.2/5 (91 download)

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Book Synopsis Immobilized Catalysts by : Andreas Kirschning

Download or read book Immobilized Catalysts written by Andreas Kirschning and published by Springer Science & Business Media. This book was released on 2004-11-22 with total page 354 pages. Available in PDF, EPUB and Kindle. Book excerpt: R. Haag, S. Roller: Polymeric Supports for the Immobilisation of Catalysts .- J. Horn, F. Michalek, C.C. Tzschucke, W. Bannwarth: Non-Covalently Solid-Phase Bound Catalysts for Organic Synthesis .- Y. Uozumi: Recent Progress in Polymeric Palladium Catalysts for Organic Synthesis .- D.E. Bergbreiter, J. Li: Applications of Catalysts on Soluble Supports .- B. Desai, C.O. Kappe: Microwave-Assisted Synthesis Involving Immobilized Catalysts .- A. Kirschning, G. Jas: Applications of Immobilized Catalysts in Continuous Flow Processes .- N. End, K.-U. Schöning: Immobilized Catalysts in Industrial Research and Application .- N. End, K.-U. Schöning: Immobilized Biocatalysts in Industrial Research and Production

Modification of Polymers

Author : Charles E. Carraher
Publisher : Springer Science & Business Media
ISBN 13 : 1461337488
Total Pages : 414 pages
Book Rating : 4.4/5 (613 download)

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Book Synopsis Modification of Polymers by : Charles E. Carraher

Download or read book Modification of Polymers written by Charles E. Carraher and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 414 pages. Available in PDF, EPUB and Kindle. Book excerpt: The sheer volume of topics which could have been included under our general title prompted us to make some rather arbitrary decisions about content. Modification by irradiation is not included because the activity in this area is being treated elsewhere. We have chosen to emphasize chemical routes to modification and have striven to pre sent as balanced a representation of current activity as time and page count permit. Industrial applications, both real and potential, are included. Where appropriate, we have encouraged the contributors to include review material to help provide the reader with adequate context. The initial chapter is a review from a historical perspective of polymer modification and contains an extensive bibliography. The remainder of the book is divided into four general areas: Reactions and Preparation of Copolymers Reactions and Preparation of Block and Graft Copolymers Modification Through Condensation Reactions Applications The chemical modification of homopolymers such as polyvinylchlo ride, polyethylene, poly(chloroalkylene sulfides), polysulfones, poly chloromethylstyrene, polyisobutylene, polysodium acrylate, polyvinyl alcohol, polyvinyl chloroformate, sulfonated polystyrene; block and graft copolymers such as poly(styrene-block-ethylene-co-butylene block-styrene), poly(I,4-polybutadiene-block ethylene oxide), star chlorine-telechelic polyisobutylene, poly(isobutylene-co-2,3-dimethyl- 1,3-butadiene), poly(styrene-co-N-butylmethacrylate); cellulose, dex tran and inulin, is described.

Iron Catalysis

Author : Bernd Plietker
Publisher : Springer Science & Business Media
ISBN 13 : 3642146694
Total Pages : 227 pages
Book Rating : 4.6/5 (421 download)

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Book Synopsis Iron Catalysis by : Bernd Plietker

Download or read book Iron Catalysis written by Bernd Plietker and published by Springer Science & Business Media. This book was released on 2011-01-05 with total page 227 pages. Available in PDF, EPUB and Kindle. Book excerpt: Juan I. Padrón and Víctor S. Martín: Catalysis by means of Fe-based Lewis acids; Hiroshi Nakazawa*, Masumi Itazaki: Fe–H Complexes in Catalysis; Kristin Schröder, Kathrin Junge, Bianca Bitterlich, and Matthias Beller: Fe-catalyzed Oxidation Reactions of Olefins, Alkanes and Alcohols: Involvement of Oxo- and Peroxo Complexes; Chi-Ming Che, Cong-Ying Zhou, Ella Lai-Ming Wong: Catalysis by Fe=X Complexes (X=NR, CR2); René Peters, Daniel F. Fischer and Sascha Jautze: Ferrocene and Half Sandwich Complexes as Catalysts with Iron Participation; Markus Jegelka, Bernd Plietker: Catalysis by Means of Complex Ferrates.

Organic Electrochemistry

Author : Ole Hammerich
Publisher : CRC Press
ISBN 13 : 142008402X
Total Pages : 1706 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Organic Electrochemistry by : Ole Hammerich

Download or read book Organic Electrochemistry written by Ole Hammerich and published by CRC Press. This book was released on 2015-09-22 with total page 1706 pages. Available in PDF, EPUB and Kindle. Book excerpt: Praise for the Fourth Edition"Outstanding praise for previous editions.the single best general reference for the organic chemist."-Journal of the Electrochemical Society"The cast of editors and authors is excellent, the text is, in general, easily readable and understandable, well documented, and well indexed those who purchase the book will be sa

Quinoxalines

Author : Vakhid A. Mamedov
Publisher : Springer
ISBN 13 : 3319297732
Total Pages : 451 pages
Book Rating : 4.3/5 (192 download)

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Book Synopsis Quinoxalines by : Vakhid A. Mamedov

Download or read book Quinoxalines written by Vakhid A. Mamedov and published by Springer. This book was released on 2016-04-26 with total page 451 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book reviews the fundamental aspects of quinoxaline chemistry: synthesis, reactions, mechanisms, structure, properties, and uses. The first four chapters present a survey of the developments in quinoxaline chemistry since the publication of the monograph on “Condensed Pyrazines” by Cheeseman and Cookson in 1979. These chapters give comprehensive coverage of all the methods of the synthesis of quinoxalines and the important quinoxaline-containing ring systems such as thiazolo[3,4-a]-, pyrrolo[1,2-a]-, and imidazo[1,5-a]quinoxalines. Chapter five describes many new methods for the construction of quinoxaline macrocycles, which are important in applications such as optical devices and materials. The final chapter reviews all previously known rearrangements of heterocyclic systems that lead to benzimidazole derivatives. Mamedov critically analyses these transformations to reveal a novel acid-catalyzed rearrangement of quinoxalinones giving 2-heteroarylbenzimidazoles and 1-heteroarylbenzimidazolones in the presence of nucleophilic reactants (MAMEDOV Heterocycle Rearrangement). This book is of interest to researchers in the fields of heterocyclic and synthetic organic chemistry.

Chemical Engineering Design

Author : Gavin Towler
Publisher : Elsevier
ISBN 13 : 0080966608
Total Pages : 1321 pages
Book Rating : 4.0/5 (89 download)

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Book Synopsis Chemical Engineering Design by : Gavin Towler

Download or read book Chemical Engineering Design written by Gavin Towler and published by Elsevier. This book was released on 2012-01-25 with total page 1321 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemical Engineering Design, Second Edition, deals with the application of chemical engineering principles to the design of chemical processes and equipment. Revised throughout, this edition has been specifically developed for the U.S. market. It provides the latest US codes and standards, including API, ASME and ISA design codes and ANSI standards. It contains new discussions of conceptual plant design, flowsheet development, and revamp design; extended coverage of capital cost estimation, process costing, and economics; and new chapters on equipment selection, reactor design, and solids handling processes. A rigorous pedagogy assists learning, with detailed worked examples, end of chapter exercises, plus supporting data, and Excel spreadsheet calculations, plus over 150 Patent References for downloading from the companion website. Extensive instructor resources, including 1170 lecture slides and a fully worked solutions manual are available to adopting instructors. This text is designed for chemical and biochemical engineering students (senior undergraduate year, plus appropriate for capstone design courses where taken, plus graduates) and lecturers/tutors, and professionals in industry (chemical process, biochemical, pharmaceutical, petrochemical sectors). New to this edition: - Revised organization into Part I: Process Design, and Part II: Plant Design. The broad themes of Part I are flowsheet development, economic analysis, safety and environmental impact and optimization. Part II contains chapters on equipment design and selection that can be used as supplements to a lecture course or as essential references for students or practicing engineers working on design projects. - New discussion of conceptual plant design, flowsheet development and revamp design - Significantly increased coverage of capital cost estimation, process costing and economics - New chapters on equipment selection, reactor design and solids handling processes - New sections on fermentation, adsorption, membrane separations, ion exchange and chromatography - Increased coverage of batch processing, food, pharmaceutical and biological processes - All equipment chapters in Part II revised and updated with current information - Updated throughout for latest US codes and standards, including API, ASME and ISA design codes and ANSI standards - Additional worked examples and homework problems - The most complete and up to date coverage of equipment selection - 108 realistic commercial design projects from diverse industries - A rigorous pedagogy assists learning, with detailed worked examples, end of chapter exercises, plus supporting data and Excel spreadsheet calculations plus over 150 Patent References, for downloading from the companion website - Extensive instructor resources: 1170 lecture slides plus fully worked solutions manual available to adopting instructors

Hydroformylation for Organic Synthesis

Author : Maurizio Taddei
Publisher : Springer
ISBN 13 : 3642450598
Total Pages : 233 pages
Book Rating : 4.6/5 (424 download)

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Book Synopsis Hydroformylation for Organic Synthesis by : Maurizio Taddei

Download or read book Hydroformylation for Organic Synthesis written by Maurizio Taddei and published by Springer. This book was released on 2014-07-08 with total page 233 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Role of Metals and Ligands in Organic Hydroformylation, by Luca Gonsalvi, Antonella Guerriero, Eric Monflier, Frédéric Hapiot, Maurizio Peruzzini. Hydroformylation in Aqueous Biphasic Media Assisted by Molecular Receptors, by Frédéric Hapiot, Hervé Bricout, Sébastien Tilloy, Eric Monflier. Asymmetric Hydroformylation, by Bernabé F. Perandones, Cyril Godard, Carmen Claver. Domino Reactions Triggered by Hydroformylation, by Elena Petricci, Elena Cini. Rhodium-Catalyzed Hydroformylation in Fused Azapolycycles Synthesis, by Roberta Settambolo. Hydroformylation in Natural Product Synthesis, by Roderick W. Bates, Sivarajan Kasinathan.

Iron Catalysis in Organic Chemistry

Author : Bernd Plietker
Publisher : John Wiley & Sons
ISBN 13 : 3527623280
Total Pages : 295 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Iron Catalysis in Organic Chemistry by : Bernd Plietker

Download or read book Iron Catalysis in Organic Chemistry written by Bernd Plietker and published by John Wiley & Sons. This book was released on 2008-09-08 with total page 295 pages. Available in PDF, EPUB and Kindle. Book excerpt: This first comprehensive book to cover this exciting field also deals with the biological aspects, such as enzymes with iron. Following an introduction, this handy reference and handbook goes on to deal with reductions, oxidations of C, H- and C=C bonds, oxidative allylic oxygenation and amination, the oxidation of heteroatoms, cross coupling reactions, aromatic and nucleophilic substitutions, addition to carbonyl compounds, and cyclisations as well as ring opening reactions. The chapters are clearly classified according to the reaction type, allowing readers to quickly locate the desired information.

New Methodologies and Techniques for a Sustainable Organic Chemistry

Author : Alessandro Mordini
Publisher : Springer Science & Business Media
ISBN 13 : 1402067933
Total Pages : 339 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis New Methodologies and Techniques for a Sustainable Organic Chemistry by : Alessandro Mordini

Download or read book New Methodologies and Techniques for a Sustainable Organic Chemistry written by Alessandro Mordini and published by Springer Science & Business Media. This book was released on 2008-04-17 with total page 339 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemical industries have to face the challenge of finding adequate processes to produce large quantities of new products, while at the same time decreasing both the impact on the environment and the risk of disaster. This book addresses this challenge. It discusses the problems of environmentally benign organic processes on an interdisciplinary approach. The book features experts in selective catalysis, development of new reagents and methods who present their recent results.

Dienamine Catalysis for Organic Synthesis

Author : Kengadarane Anebouselvy
Publisher : Royal Society of Chemistry
ISBN 13 : 1782620907
Total Pages : 220 pages
Book Rating : 4.7/5 (826 download)

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Book Synopsis Dienamine Catalysis for Organic Synthesis by : Kengadarane Anebouselvy

Download or read book Dienamine Catalysis for Organic Synthesis written by Kengadarane Anebouselvy and published by Royal Society of Chemistry. This book was released on 2018-03-02 with total page 220 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the last decade a new era in asymmetric catalysis has been realised by the discovery of L-proline induced chiral enamines from carbonyls. Inspired by this, researchers have developed many other primary catalytic species in situ, more recently secondary catalytic species such as aminals have been identified for use in asymmetric synthesis. High-yielding asymmetric synthesis of bioactive and natural products through mild catalysis is an efficient approach in reaction engineering. In the early days, synthetic chemists mainly focused on the synthesis of complex molecules, with less attention on the reaction efficiency and eco-friendly conditions. Recent investigations have been directed towards the development of atom economy, eco-friendly and enantioselective synthesis for more targeted and efficient synthesis. Building on the momentum of this rapidly expanding research area, Dienamine catalysis for organic synthesis will provide a comprehensive introduction, from the preformed species, in situ generation and onto their applications in the synthesis of bioactive molecules and natural products.

Organic Reactions in Water

Author : U. Marcus Lindstrom
Publisher : John Wiley & Sons
ISBN 13 : 047099424X
Total Pages : 424 pages
Book Rating : 4.4/5 (79 download)

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Book Synopsis Organic Reactions in Water by : U. Marcus Lindstrom

Download or read book Organic Reactions in Water written by U. Marcus Lindstrom and published by John Wiley & Sons. This book was released on 2008-04-15 with total page 424 pages. Available in PDF, EPUB and Kindle. Book excerpt: Volatile organic solvents are the normal media used in both research scale and industrial scale synthesis of organic chemicals. Their environmental impact is significant, however, and so the development of alternative reaction media has become of great interest. Developments in the use of water as a solvent for organic synthesis have reached the point where it could now be considered a viable solvent for many organic reactions. Organic Reactions in Water demonstrates the underlying principles of using water as a reaction solvent and, by reference to a range of reaction types and systems, it’s effective use in synthetic organic chemistry. Written by an internationally respected team of contributors, and with a strong focus on the practical use of water as a reaction medium, this book illustrates the enormous potential of water for the development of new and unique chemistries and synthetic strategies, while at the same time offering a much reduced environmental impact.