Solid-State NMR III Organic Matter

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Publisher : Springer Science & Business Media
ISBN 13 : 3642612237
Total Pages : 218 pages
Book Rating : 4.6/5 (426 download)

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Book Synopsis Solid-State NMR III Organic Matter by : Bernhard Blümich

Download or read book Solid-State NMR III Organic Matter written by Bernhard Blümich and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 218 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.

Solid-State NMR III Organic Matter

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Author :
Publisher : Springer
ISBN 13 : 9783642647512
Total Pages : 0 pages
Book Rating : 4.6/5 (475 download)

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Book Synopsis Solid-State NMR III Organic Matter by : Bernhard Blümich

Download or read book Solid-State NMR III Organic Matter written by Bernhard Blümich and published by Springer. This book was released on 2011-09-28 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.

Solid-State NMR and Organic Geochemistry

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Author :
Publisher : Elsevier
ISBN 13 : 9780128195741
Total Pages : 710 pages
Book Rating : 4.1/5 (957 download)

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Book Synopsis Solid-State NMR and Organic Geochemistry by : Jingdong Mao

Download or read book Solid-State NMR and Organic Geochemistry written by Jingdong Mao and published by Elsevier. This book was released on 2021-11-15 with total page 710 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR and Organic Geochemistry explains solid-state NMR from the point of view of organic geochemists interested in applying solid-state NMR in their research. The book sets the scene in the first two chapters by describing the basic concepts of solid-state NMR adapted for non-NMR specialists as well as an overview of organic geochemistry for NMR specialists. The essentials for acquiring reliable spectra of complex organic matter are then described in Chapter 3. Chapter 4 introduces the systematic and advanced solid-state NMR techniques and approach to characterizing complex organic mixtures developed in Dr. Mao's laboratory. Practical aspects of performing solid-state NMR experiments of complex organic matter are discussed in Chapter 5. Chapters 6 through 15 are focused on applications of solid-state NMR in organic geochemistry, starting with geochemically important functional groups and biopolymers, followed by organic matter from soils, water, sediments, and aerosols, peat, coal, kerogen, and oil shale. The interactions of organic matter with organic contaminants probed by solid-state NMR are described in Chapter 16. Finally, the last chapter covers isotopic enrichment and labelling and solid-state NMR, and their applications in organic geochemistry. Bridges the gap between NMR specialists and organic geochemists, adapting solid-state NMR theory for non-NMR specialists Brings together NMR applications for a range of materials not often discussed in other NMR books, including applications to soil, aerosols, peat, coal, kerogen, and more Includes additional resources for further reading and problems to facilitate learning and application of key concepts in each chapter

Solid-State NMR IV Methods and Applications of Solid-State NMR

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Author :
Publisher : Springer Science & Business Media
ISBN 13 : 3642791271
Total Pages : 210 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Solid-State NMR IV Methods and Applications of Solid-State NMR by : B. Blümich

Download or read book Solid-State NMR IV Methods and Applications of Solid-State NMR written by B. Blümich and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 210 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance at NMR meetings, approaching that ofliquid state resonance. Important progress can be observed in the areas of methodological developments and applications to organic and inorganic matter. One volume devoted to more or less one of each of these areas has been published in the preceding three issues. This volume can be considered an addendum to this series. Selected methods and applications of Solid-State NMR are featured in three chapters. The first one treats the recoupling of dipolar interactions in solids, which are averaged by fast sample rotation. Following an introduction to effective Hamiltonians and Floquet theory, different types of experiment such as rotary resonance, dipolar chemical shift correlation spectroscopy, rotational resonance and multipulse recoupling are treated in the powerful Floquet formalism. In the second chapter, the different approaches to line narrowing of quadrupolar nuclei are reviewed in a. consistent formulation of double resonance (DaR) and dynamic angle spinning (DAS). Practical aspects of probe design are considered as well as advanced 2D experiments, sensitivity enhancement techniques, and spinning sideband manipulations. The use of such techniques dramatically increases the number of nuclei which can be probed in high resolution NMR spectroscopy. The final chapter describes new experimental approaches and results of structural studies of noncrystalline solids.

Nuclear Magnetic Resonance Spectroscopy in Environmental Chemistry

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Author :
Publisher : Oxford University Press
ISBN 13 : 0198025807
Total Pages : 341 pages
Book Rating : 4.1/5 (98 download)

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Book Synopsis Nuclear Magnetic Resonance Spectroscopy in Environmental Chemistry by : Mark A. Nanny

Download or read book Nuclear Magnetic Resonance Spectroscopy in Environmental Chemistry written by Mark A. Nanny and published by Oxford University Press. This book was released on 1997-04-03 with total page 341 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book demonstrates the usefulness of NMR spectroscopy for a wide variety of applications in environmental science and technology. It contains a wealth of information relating to instrumentation, sample preparation, and data interpretation. The book is divided into three sections discussing contaminant interaction, solution and condensed-phase characterization, and nutrients and natural organic matter characterization. In addition to these in-depth chapters, an introductory overview provides the basic principles of solution and solid-state NMR spectroscopy. Each section also contains a discussion of advances in each area directly attributable to NMR spectroscopy. A final chapter suggests future directions for the deployment of this powerful technology in environmental science.

NMR Spectroscopy

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Publisher : John Wiley & Sons
ISBN 13 : 111861643X
Total Pages : 916 pages
Book Rating : 4.1/5 (186 download)

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Book Synopsis NMR Spectroscopy by : Myrna J. Simpson

Download or read book NMR Spectroscopy written by Myrna J. Simpson and published by John Wiley & Sons. This book was released on 2014-06-12 with total page 916 pages. Available in PDF, EPUB and Kindle. Book excerpt: The challenges faced by environmental scientists today are vast, complex, and multi-faceted. For instance, predicting the fate of an environmental pollutant or understanding ecosystem responses to climate change, necessitate a firm understanding of molecular structure and dynamics of environmental media as well as the components that exist and interact within this media. Furthermore, linking information obtained at the molecular-scale to ecosystem-level processes is a major pursuit of modern environmental research. As such, NMR spectroscopy and its scalability from the molecular-scale to the macroscopic-scale, is facilitating rapid growth in environmental science. In addition, the versatility of NMR spectroscopy has resulted in the development and implementation of different types of NMR techniques to examine the structure of various types of environmental samples, living and non-living, as well as the study of critical environmental processes. This comprehensive handbook is a collection of chapters that span from methods to how NMR is used in environmental research to gain insight into various ecosystem properties. It is organized into three parts: Part A focuses on methods used in environmental NMR which span from solution-state to magnetic resonance imaging. Part B emphasizes how NMR spectroscopy plays an essential role in understanding various types of environmental components and related processes, including different forms of organic matter found in soil, water, and air as well as how NMR is used to probe the fate of water, organic pollutants, and metals in the environment. Part C focuses on the growing field of environmental metabolomics which uses NMR as its main discovery platform. This volume highlights the immense potential of NMR spectroscopy to expand our fundamental understanding of environmental processes and how it will continue to do so well into the future. About eMagRes Handbooks eMagRes (formerly the Encyclopedia of Magnetic Resonance) publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of eMagRes articles. In consultation with the eMagRes Editorial Board, the eMagRes handbooks are coherently planned in advance by specially-selected Editors, and new articles are written to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes

Nuclear Magnetic Resonance

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Publisher : Royal Society of Chemistry
ISBN 13 : 1847553818
Total Pages : 564 pages
Book Rating : 4.8/5 (475 download)

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Book Synopsis Nuclear Magnetic Resonance by : G A Webb

Download or read book Nuclear Magnetic Resonance written by G A Webb and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.

Solid-State NMR II

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Publisher : Springer Science & Business Media
ISBN 13 : 3642500498
Total Pages : 220 pages
Book Rating : 4.6/5 (425 download)

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Book Synopsis Solid-State NMR II by : B. Blümich

Download or read book Solid-State NMR II written by B. Blümich and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 220 pages. Available in PDF, EPUB and Kindle. Book excerpt: 1. G. Engelhardt, H. Koller, Stuttgart, FRG: 29Si NMR of Inorganic Solids 2. H. Pfeifer, Leizpig, FRG: NMR of Solid Surfaces 3. A. Sebald, Bayreuth, FRG: MAS and CP/MAS NMR of Less Common Spin-1/2 Nuclei 4. C. J{ger, Mainz, FRG: Satellite Transition Spectroscopy of Quadrupolar Nuclei 5. D. Brinkmann, M. Mali, Z}rich, CH: NMR-NQR Studies of High-Temperature Superconductors.

Nuclear Magnetic Resonance

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Publisher : Royal Society of Chemistry
ISBN 13 : 0854043373
Total Pages : 518 pages
Book Rating : 4.8/5 (54 download)

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Book Synopsis Nuclear Magnetic Resonance by : A. E. Aliev

Download or read book Nuclear Magnetic Resonance written by A. E. Aliev and published by Royal Society of Chemistry. This book was released on 2002 with total page 518 pages. Available in PDF, EPUB and Kindle. Book excerpt: For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage.

Chemistry & Physics of Carbon

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Publisher : CRC Press
ISBN 13 : 1439820945
Total Pages : 301 pages
Book Rating : 4.4/5 (398 download)

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Book Synopsis Chemistry & Physics of Carbon by : Ljubisa R. Radovic

Download or read book Chemistry & Physics of Carbon written by Ljubisa R. Radovic and published by CRC Press. This book was released on 2012-10-03 with total page 301 pages. Available in PDF, EPUB and Kindle. Book excerpt: Written by distinguished researchers, the long-running Chemistry and Physics of Carbon series provides a comprehensive and critical overview of carbon materials in terms of molecular structure, intermolecular relationships, bulk and surface properties, and their behavior in current and emerging applications. Volume 31 not only retains the high-quality content and reputation of previous volumes, but also complements them with reliable and timely coverage of the latest advances in the field. Maintaining the high level established by its predecessors, this book contains a prestigious and authoritative series of review chapters covering both chemistry and physics of carbon. The book examines properties and behavior of carbon materials ranging from coal to graphite, from activated carbons, chars, cokes, and carbon blacks to carbon fibers, fullerenes, nanotubes, and graphene. It complements previous volumes in the series by presenting updated information on ‘disordered’ carbons, a complex field that impacts nearly all aspects of carbon materials research. It includes a chapter on novel methods of characterization of carbon materials using ever more powerful techniques, as well as a chapter on the use of carbon materials in photocatalysis, a fast-moving and potentially exciting application. Emphasizing key experimental results and practical aspects, as well as important theoretical issues in every chapter, Volume 31 is a vital resource for those engaged in developing new technologies in a wide range of applicability of traditional and novel carbon materials from drug delivery to energy storage and conversion.

Current Developments in Solid State NMR Spectroscopy

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Publisher : Springer Science & Business Media
ISBN 13 : 3709137152
Total Pages : 143 pages
Book Rating : 4.7/5 (91 download)

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Book Synopsis Current Developments in Solid State NMR Spectroscopy by : Norbert Müller

Download or read book Current Developments in Solid State NMR Spectroscopy written by Norbert Müller and published by Springer Science & Business Media. This book was released on 2013-04-17 with total page 143 pages. Available in PDF, EPUB and Kindle. Book excerpt: Why to apply solid-state NMR? - By now, we should have learned that NMR is mainly used for the study of molecules in solution, while x-ray diffraction is the method of choice for solids. Based on this fact, the two recent 'NMR-Nobelprizes' went indeed into the liquid phase: my own one eleven years ago, and particularly the most recent one to Kurt Wuthrich. His prize is beyond any doubts very well justified. His contribution towards the study of biomolecules in solution, in their native (or almost native) environment is truly monumental. We all will profit from it indirectly when one of our future diseases will be cured with better drugs, based on the insightful knowledge gained through liquid-state NMR. Two fields of NMR are still left out of the Nobel Prize game: magnetic reso nance imaging (MRI) and solid-state NMR. The disrespect for MRI in Stockholm is particularly difficult to understand; but this is not a subject to be discussed at the present place. Solid-state NMR is the third of the three great fields of NMR, powerful already today and very promising for the near future.

Applications of NMR Spectroscopy

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Author :
Publisher : Bentham Science Publishers
ISBN 13 : 1681084392
Total Pages : 238 pages
Book Rating : 4.6/5 (81 download)

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Book Synopsis Applications of NMR Spectroscopy by : Atta-ur- Rahman

Download or read book Applications of NMR Spectroscopy written by Atta-ur- Rahman and published by Bentham Science Publishers. This book was released on 2017-12-04 with total page 238 pages. Available in PDF, EPUB and Kindle. Book excerpt: Applications of NMR Spectroscopy is a book series devoted to publishing the latest advances in the applications of nuclear magnetic resonance (NMR) spectroscopy in various fields of organic chemistry, biochemistry, health and agriculture. The sixth volume of the series features reviews focusing on NMR spectroscopic techniques for studying tautomerism, applications in medical diagnosis, in food chemistry and identifying secondary metabolites.

Soil Sampling and Methods of Analysis

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Publisher : CRC Press
ISBN 13 : 1420005278
Total Pages : 1264 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Soil Sampling and Methods of Analysis by : M.R. Carter

Download or read book Soil Sampling and Methods of Analysis written by M.R. Carter and published by CRC Press. This book was released on 2007-08-03 with total page 1264 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thoroughly updated and revised, this second edition of the bestselling Soil Sampling and Methods of Analysis presents several new chapters in the areas of biological and physical analysis and soil sampling. Reflecting the burgeoning interest in soil ecology, new contributions describe the growing number and assortment of new microbiological

Natural Organic Matter in Water

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Publisher : Butterworth-Heinemann
ISBN 13 : 0128017198
Total Pages : 382 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Natural Organic Matter in Water by : Mika Sillanpää

Download or read book Natural Organic Matter in Water written by Mika Sillanpää and published by Butterworth-Heinemann. This book was released on 2014-10-07 with total page 382 pages. Available in PDF, EPUB and Kindle. Book excerpt: Approximately 77 percent of the freshwater used in the United States comes from surface-water sources and is subject to natural organic matter contamination according to the United States Geological Survey. This presents a distinct challenge to water treatment engineers. An essential resource to the latest breakthroughs in the characterization, treatment and removal of natural organic matter (NOM) from drinking water, Natural Organic Matter in Waters: Characterization and Treatment Methods focuses on advance filtration and treatment options, and processes for reducing disinfection byproducts. Based on the author’s years of research and field experience, this book begins with the characterization of NOM including: general parameters, isolation and concentration, fractionation, composition and structural analysis and biological testing. This is followed by removal methods such as inorganic coagulants, polyelectrolytes and composite coagulants. Electrochemical and membranes removal methods such as: electrocoagulation, electrochemical oxidation, microfiltration and ultrafiltration, nanofiltration and membrane fouling. Covers conventional as well as advanced NOM removal methods Includes characterization methods of NOM Explains removal methods such as: removal by coagulation, electrochemical, advanced oxidation, and integrated methods

Nuclear Magnetic Resonance of Liquid Crystals

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Publisher : Springer Science & Business Media
ISBN 13 : 146121954X
Total Pages : 320 pages
Book Rating : 4.4/5 (612 download)

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Book Synopsis Nuclear Magnetic Resonance of Liquid Crystals by : Ronald Y. Dong

Download or read book Nuclear Magnetic Resonance of Liquid Crystals written by Ronald Y. Dong and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 320 pages. Available in PDF, EPUB and Kindle. Book excerpt: Intended for researchers and students in physics, chemistry and materials science, this book provides the necessary background information and sufficient mathematical and physical detail to study the current research literature. The book begins with a survey of liquid crystal phases and field effects, together with an introduction to the basic physics of nuclear magnetic resonance. It then discusses orientational ordering and molecular field theories for various liquid crystal molecules and nmr studies of uniaxial and biaxial phases. Subsequent chapters consider spin relaxation processes and rotational, translational, and internal molecular dynamics of liquid crystals. The final chapter discusses two-dimensional and multiple- quantum nmr spectroscopies and their application in elucidating liquid crystal properties. This second edition, updated throughout, incorporates many new references and includes new mathematical appendices.

Soil and Environmental Chemistry

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Publisher : Academic Press
ISBN 13 : 0128041951
Total Pages : 586 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Soil and Environmental Chemistry by : William F. Bleam

Download or read book Soil and Environmental Chemistry written by William F. Bleam and published by Academic Press. This book was released on 2016-11-30 with total page 586 pages. Available in PDF, EPUB and Kindle. Book excerpt: Soil and Environmental Chemistry, Second Edition, presents key aspects of soil chemistry in environmental science, including dose responses, risk characterization, and practical applications of calculations using spreadsheets. The book offers a holistic, practical approach to the application of environmental chemistry to soil science and is designed to equip the reader with the chemistry knowledge and problem-solving skills necessary to validate and interpret data. This updated edition features significantly revised chapters, averaging almost a 50% revision overall, including some reordering of chapters. All new problem sets and solutions are found at the end of each chapter, and linked to a companion site that reflects advances in the field, including expanded coverage of such topics as sample collection, soil moisture, soil carbon cycle models, water chemistry simulation, alkalinity, and redox reactions. There is also additional pedagogy, including key term and real-world scenarios. This book is a must-have reference for researchers and practitioners in environmental and soil sciences, as well as intermediate and advanced students in soil science and/or environmental chemistry. Includes additional pedagogy, such as key terms and real-world scenarios Supplemented by over 100 spreadsheets to migrate readers from calculator-based to spreadsheet-based problem-solving that are directly linked from the text Includes example problems and solutions to enhance understanding Significantly revised chapters link to a companion site that reflects advances in the field, including expanded coverage of such topics as sample collection, soil moisture, soil carbon cycle models, water chemistry simulation, alkalinity, and redox reactions

Solid State NMR

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Author :
Publisher :
ISBN 13 :
Total Pages : 232 pages
Book Rating : 4.E/5 ( download)

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Book Synopsis Solid State NMR by : Bernhard Blümich

Download or read book Solid State NMR written by Bernhard Blümich and published by . This book was released on 1994 with total page 232 pages. Available in PDF, EPUB and Kindle. Book excerpt: