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Recent Developments In Crystallization
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Book Synopsis Recent Developments in Crystallization by : Garry Hollis
Download or read book Recent Developments in Crystallization written by Garry Hollis and published by . This book was released on 2015-03-28 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystals can be formed from solids, melts, liquids and even vapors. Crystals are of various kinds, both organic and inorganic, and the process of crystallization is an age-old multidimensional subject of research study. Though complex in its characteristics, the process of crystallization forms a part of our regular lives from making ice cubes in our refrigerators to latest and advanced chemical and electronic industry processes. This book is aimed at bringing forth novel perspectives while presenting important data for experts in the related fields of crystallography. It elaborates the fundamentals and theoretical aspects in crystallization. The reader is introduced to various different perspectives of the crystallization process which will prove to be a valuable reference source to those with diverse backgrounds.
Book Synopsis Handbook of Industrial Crystallization by : Allan Myerson
Download or read book Handbook of Industrial Crystallization written by Allan Myerson and published by Butterworth-Heinemann. This book was released on 2002-01-08 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes. The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design. Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the field Covers all aspects of industrial crystallization in a single, complete volume
Book Synopsis Advanced Topics in Crystallization by : Yitzhak Mastai
Download or read book Advanced Topics in Crystallization written by Yitzhak Mastai and published by BoD – Books on Demand. This book was released on 2015-05-06 with total page 374 pages. Available in PDF, EPUB and Kindle. Book excerpt: In nearly all process industries, crystallization is used at some stage as a method of production, purification or recovery of solid materials. In recent years, a number of new applications have also come to rely on crystallization processes such as the crystallization of nano and amorphous materials. The articles in this book have been contributed by some of the most respected researchers in this area and cover the frontier areas of research and developments in crystallization processes. Divided into three sections, this book provides the latest research developments in many aspects of crystallization including the crystallization of biological macromolecules and pharmaceutical compounds, the crystallization of nanomaterials and the crystallization of amorphous and glassy materials. This book is of interest to both fundamental research and practicing scientists and will prove invaluable to all chemical engineers and industrial chemists in process industries, as well as crystallization workers and students in industry and academia.
Book Synopsis Advances in Crystallization Processes by : Yitzhak Mastai
Download or read book Advances in Crystallization Processes written by Yitzhak Mastai and published by BoD – Books on Demand. This book was released on 2012-04-27 with total page 672 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. In recent years, a number of new applications have also come to rely on crystallization processes such as the crystallization of nano and amorphous materials. The articles for this book have been contributed by the most respected researchers in this area and cover the frontier areas of research and developments in crystallization processes. Divided into five parts this book provides the latest research developments in many aspects of crystallization including: chiral crystallization, crystallization of nanomaterials and the crystallization of amorphous and glassy materials. This book is of interest to both fundamental research and also to practicing scientists and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia.
Book Synopsis Crystallization by : Marcello Andreeta
Download or read book Crystallization written by Marcello Andreeta and published by BoD – Books on Demand. This book was released on 2012-09-19 with total page 582 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is one of the most ancient and interdisciplinary topics of research known to mankind. Crystals can be organic or inorganic and may be produced from melts, liquid solutions, vapors or even in solid state. Notwithstanding its inherently high complexity, the crystallization process is part of our everyday lives, from ice making in our homes to the most state-of-the-art chemical and electronic industry. In this book, our purpose was to present new insights to the reader, as well as crucial and very useful information for researchers working in this field, while simultaneously creating a comprehensive text about crystallization processes which may serve as a starting point for people with different backgrounds.
Download or read book Crystallization written by J W Mullin and published by Elsevier. This book was released on 2001-05-09 with total page 600 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the first publication of this definitive work nearly 40 years ago, this fourth edition has been completely rewritten. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Incorporating all the recent developments and applications of crystallization technology, Crystallization gives clear accounts of the underlying principles, a review of the past and current research themes and guidelines for equipment and process design. This new edition introduces and enlarges upon such subjects as: Control and Separation of polymorphs and chiral crystals Micro- and macro-mixing and the use of computer fluid dynamics Seeding and secondary nucleation in batch crystallization processes Incorporation of upstream and downstream requirements into design procedures for crystallization plant Computer-aided molecular design and its use in crystal habit modifier selection Crystallization provides a comprehensive overview of the subject and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia. Crystallization is written with the precision and clarity of style that is John Mullin's hallmark - a special feature being the large number of appendices that provide relevant physical property data. Covers all new developments and trends in crystallization Comprehensive coverage of subject area
Book Synopsis Industrial Crystallization by : Narayan S. Tavare
Download or read book Industrial Crystallization written by Narayan S. Tavare and published by Springer Science & Business Media. This book was released on 2013-11-11 with total page 550 pages. Available in PDF, EPUB and Kindle. Book excerpt: Incorporating all recent developments and applications of crystallization technology, this volume offers a clear account of the field's underlying principles, reviews of past and current research, and provides guidelines for equipment and process design. The book takes a balanced functional approach in its critical survey of research literature, and includes several problems based on real practical situations that illustrate theoretical development. Several new concepts and techniques used in process simulation and identification analysis are featured.
Book Synopsis Crystallization by : Wolfgang Beckmann
Download or read book Crystallization written by Wolfgang Beckmann and published by John Wiley & Sons. This book was released on 2013-01-14 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.
Book Synopsis Crystallization of Organic Compounds by : Hsien-Hsin Tung
Download or read book Crystallization of Organic Compounds written by Hsien-Hsin Tung and published by John Wiley & Sons. This book was released on 2009-06-17 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: Filled with industrial examples emphasizing the practical applications of crystallization methodologies Based on the authors' hands-on experiences as process engineers at Merck, Crystallization of Organic Compounds guides readers through the practical aspects of crystallization. It uses plenty of case studies and examples of crystallization processes, ranging from development through manufacturing scale-up. The book not only emphasizes strategies that have been proven successful, it also helps readers avoid common pitfalls that can render standard procedures unsuccessful. The goal of this text is twofold: Build a deeper understanding of the fundamental properties of crystallization as well as the impact of these properties on crystallization process development. Improve readers' problem-solving abilities by using actual industrial examples with real process constraints. Crystallization of Organic Compounds begins with detailed discussions of fundamental thermodynamic properties, nucleation and crystal growth kinetics, process dynamics, and scale-up considerations. Next, it investigates modes of operation, including cooling, evaporation, anti-solvent, and reactive crystallization. The authors conclude with special applications such as ultrasound in crystallization and computational fluid dynamics in crystallization. Most chapters feature multiple examples that guide readers step by step through the crystallization of active pharmaceutical ingredients (APIs). With its focus on industrial applications, this book is recommended for chemical engineers and chemists who are involved with the development, scale-up, or operation of crystallization processes in the pharmaceutical and fine chemical industries.
Book Synopsis Crystallization of Organic Compounds by : Hsien-Hsin Tung
Download or read book Crystallization of Organic Compounds written by Hsien-Hsin Tung and published by John Wiley & Sons. This book was released on 2023-07-05 with total page 388 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization of Organic Compounds Practical resource covering applications of crystallization principles with methodologies, case studies, and numerous industrial examples for emphasis Based on the authors’ hands-on experiences as process engineers, through the use of case studies and examples of crystallization processes, ranging from laboratory development through manufacturing scale-up, Crystallization of Organic Compounds guides readers through the practical applications of crystallization and emphasizes strategies that have proven to be successful, enabling readers to avoid common pitfalls that can render standard procedures unsuccessful. Most chapters feature multiple examples that guide readers, step by step, through the crystallization of active pharmaceutical ingredients (APIs), including an analysis of the major methods of carrying out crystallization operations, their strengths and potential issues, as well as numerous examples of crystallization processes from development through manufacturing scale. Advancements in the field of crystallization have been integrated throughout the book in the newly revised Second Edition to ensure the content adequately reflects current state-of-the-art industrial know-hows and practice. The new edition also adds chapters addressing downstream operations after the crystallization, including filtration/washing and drying, together with industrial use cases. Crystallization of Organic Compounds includes detailed information on: Solubility and solid behavior, covering phase rule, polymorph, salt/co-crystal, chiral resolution and in-silico solubility prediction; and kinetics, covering seed, supersaturation, nucleation, crystal growth and model-based experimental design Critical issues in the crystallization practice, covering oiling out, seeding/wet-milling, agglomeration/aggregation, mixing scale-up and quality-by-design principles Cooling, anti-solvent, evaporation and reactive crystallization process design, covering batch and continuous operations with industrial examples Special applications, covering crystallization with ultrasound, reaction selectivity enhancement, and computation fluid dynamics, and solid dispersion With highly practical coverage of the subject, Crystallization of Organic Compounds is an essential resource for engineers and chemists involved with the development, scaling, or operation of crystallization process in the pharmaceutical and fine chemical industries, particularly those with degrees in chemical engineering and chemistry.
Book Synopsis Advances in Industrial Crystallization by : John Garside
Download or read book Advances in Industrial Crystallization written by John Garside and published by Butterworth-Heinemann. This book was released on 1991 with total page 264 pages. Available in PDF, EPUB and Kindle. Book excerpt: A treatment of crystallization as a separation and purification technique in the chemical industry, reflecting its application to new metallic, ceramic, and polymer materials; fine and specialty chemicals; and medical, biochemical, and biotechnological products. The 15 papers, from a meeting of unspecified date and location, discuss precipitation and nucleation, crystallization kinetics, habit modification, and crystallizer design and operation. No index. Annotation copyrighted by Book News, Inc., Portland, OR
Book Synopsis Theory of Particulate Processes by : Alan Ranodolph
Download or read book Theory of Particulate Processes written by Alan Ranodolph and published by Elsevier. This book was released on 2012-12-02 with total page 386 pages. Available in PDF, EPUB and Kindle. Book excerpt: Theory of Particulate Processes: Analysis and Techniques of Continuous Crystallization, Second Edition covers the numerous population balance-based particulate studies. This edition emerged from the notes for an industrial short course on crystallization. This book is divided into 10 chapters and begins with an outline of the methods for representation of particle distributions and a systematic approach to the predictive modeling of processes where there is a need to characterize distributions in time and space and by some identifying property. The succeeding chapters provide a specific and more elementary approach to modeling crystal size distributions, as well as the modeling the kinetics of crystal nucleation and growth rates. Other chapters discuss a wide range of system analysis and design considerations specific to crystallization for both the steady state and unsteady state. The final chapters illustrate the use of a population balance analysis to interpret data from both laboratory and process equipment. These chapters also explore a wide variety of particulate processes and systems for which the population balance analysis is useful. This book is of great value to graduate students with particulate systems course.
Book Synopsis Crystallization in Multiphase Polymer Systems by : Sabu Thomas
Download or read book Crystallization in Multiphase Polymer Systems written by Sabu Thomas and published by Elsevier. This book was released on 2017-09-15 with total page 610 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization in Multiphase Polymer Systems is the first book that explains in depth the crystallization behavior of multiphase polymer systems. Polymeric structures are more complex in nature than other material structures due to their significant structural disorder. Most of the polymers used today are semicrystalline, and the subject of crystallization is still one of the major issues relating to the performance of semicrystalline polymers in the modern polymer industry. The study of the crystallization processes, crystalline morphologies and other phase transitions is of great significance for the understanding the structure-property relationships of these systems. Crystallization in block copolymers, miscible blends, immiscible blends, and polymer composites and nanocomposites is thoroughly discussed and represents the core coverage of this book. The book critically analyzes the kinetics of nucleation and growth process of the crystalline phases in multi-component polymer systems in different length scales, from macro to nanoscale. Various experimental techniques used for the characterization of polymer crystallization process are discussed. Written by experts in the field of polymer crystallization, this book is a unique source and enables professionals and students to understand crystallization behavior in multiphase polymer systems such as block copolymers, polymer blends, composites and nanocomposites. Covers crystallization of multiphase polymer systems, including copolymers, blends and nanocomposites Features comprehensive, detailed information about the basic research, practical applications and new developments for these polymeric materials Analyzes the kinetics of nucleation and growth process of the crystalline phases in multi-component polymer systems in different length scales, from macro to nanoscale
Book Synopsis Crystallization Processes by : H. Ohtaki
Download or read book Crystallization Processes written by H. Ohtaki and published by John Wiley & Sons. This book was released on 1998 with total page 232 pages. Available in PDF, EPUB and Kindle. Book excerpt: An overview of crystallization processes of organic and inorganic substances from various homogeneous liquids. Crystal structures, phase transitions and crystallization rates are described in the book in connection with the structure of ions, complexes and molecules of the solution phase.
Book Synopsis Continuous Manufacturing of Pharmaceuticals by : Peter Kleinebudde
Download or read book Continuous Manufacturing of Pharmaceuticals written by Peter Kleinebudde and published by John Wiley & Sons. This book was released on 2017-09-05 with total page 645 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive look at existing technologies and processes for continuous manufacturing of pharmaceuticals As rising costs outpace new drug development, the pharmaceutical industry has come under intense pressure to improve the efficiency of its manufacturing processes. Continuous process manufacturing provides a proven solution. Among its many benefits are: minimized waste, energy consumption, and raw material use; the accelerated introduction of new drugs; the use of smaller production facilities with lower building and capital costs; the ability to monitor drug quality on a continuous basis; and enhanced process reliability and flexibility. Continuous Manufacturing of Pharmaceuticals prepares professionals to take advantage of that exciting new approach to improving drug manufacturing efficiency. This book covers key aspects of the continuous manufacturing of pharmaceuticals. The first part provides an overview of key chemical engineering principles and the current regulatory environment. The second covers existing technologies for manufacturing both small-molecule-based products and protein/peptide products. The following section is devoted to process analytical tools for continuously operating manufacturing environments. The final two sections treat the integration of several individual parts of processing into fully operating continuous process systems and summarize state-of-art approaches for innovative new manufacturing principles. Brings together the essential know-how for anyone working in drug manufacturing, as well as chemical, food, and pharmaceutical scientists working on continuous processing Covers chemical engineering principles, regulatory aspects, primary and secondary manufacturing, process analytical technology and quality-by-design Contains contributions from researchers in leading pharmaceutical companies, the FDA, and academic institutions Offers an extremely well-informed look at the most promising future approaches to continuous manufacturing of innovative pharmaceutical products Timely, comprehensive, and authoritative, Continuous Manufacturing of Pharmaceuticals is an important professional resource for researchers in industry and academe working in the fields of pharmaceuticals development and manufacturing.
Book Synopsis Chemical Engineering in the Pharmaceutical Industry by : Mary T. am Ende
Download or read book Chemical Engineering in the Pharmaceutical Industry written by Mary T. am Ende and published by John Wiley & Sons. This book was released on 2019-04-08 with total page 1435 pages. Available in PDF, EPUB and Kindle. Book excerpt: A guide to the important chemical engineering concepts for the development of new drugs, revised second edition The revised and updated second edition of Chemical Engineering in the Pharmaceutical Industry offers a guide to the experimental and computational methods related to drug product design and development. The second edition has been greatly expanded and covers a range of topics related to formulation design and process development of drug products. The authors review basic analytics for quantitation of drug product quality attributes, such as potency, purity, content uniformity, and dissolution, that are addressed with consideration of the applied statistics, process analytical technology, and process control. The 2nd Edition is divided into two separate books: 1) Active Pharmaceutical Ingredients (API’s) and 2) Drug Product Design, Development and Modeling. The contributors explore technology transfer and scale-up of batch processes that are exemplified experimentally and computationally. Written for engineers working in the field, the book examines in-silico process modeling tools that streamline experimental screening approaches. In addition, the authors discuss the emerging field of continuous drug product manufacturing. This revised second edition: Contains 21 new or revised chapters, including chapters on quality by design, computational approaches for drug product modeling, process design with PAT and process control, engineering challenges and solutions Covers chemistry and engineering activities related to dosage form design, and process development, and scale-up Offers analytical methods and applied statistics that highlight drug product quality attributes as design features Presents updated and new example calculations and associated solutions Includes contributions from leading experts in the field Written for pharmaceutical engineers, chemical engineers, undergraduate and graduation students, and professionals in the field of pharmaceutical sciences and manufacturing, Chemical Engineering in the Pharmaceutical Industry, Second Edition contains information designed to be of use from the engineer's perspective and spans information from solid to semi-solid to lyophilized drug products.
Book Synopsis Industrial Crystallization Process Monitoring and Control by : Angelo Chianese
Download or read book Industrial Crystallization Process Monitoring and Control written by Angelo Chianese and published by John Wiley & Sons. This book was released on 2012-04-06 with total page 253 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is an important technique for separation and purification of substances as well as for product design in chemical, pharmaceutical and biotechnological process industries. This ready reference and handbook draws on research work and industrial practice of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges. First the instrumentation and techniques used to measure the crystal size distribution, the nucleation and solubility points, and the chemical composition of the solid and liquid phase are outlined. Then the main techniques adopted to control industrial crystallizers, starting from fundamental approaches to the most advanced ones, including the multivariable predictive control are described. An overview of the main crystallizer types is given with details of the main control schemes adopted in industry as well as the more suitable sensors and actuators.
