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NMR Case Studies

Author : Jeffrey H Simpson
Publisher : Elsevier
ISBN 13 : 0128033533
Total Pages : 234 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis NMR Case Studies by : Jeffrey H Simpson

Download or read book NMR Case Studies written by Jeffrey H Simpson and published by Elsevier. This book was released on 2017-09-19 with total page 234 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR Case Studies: Data Analysis of Complicated Molecules provides a detailed discussion of the full logical flow associated with assigning the NMR spectra of complex molecules, also helping readers further develop their NMR spectral assignment skills. The robust case studies present the logic of each assignment, from beginning to end, fully exploring the available range of potential solutions. Readers will gain a better appreciation of various approaches and develop an intuitive sense for when this particular concept should be implemented, thus enhancing their skillsets and providing a host of methodologies potentially amenable to yielding correct assignments. Authored by a scientist with more than 20 years of experience in research and instruction, this book is the ideal reference for anyone in search of application-based content. The book addresses complicated molecules, including corticosteroids, biomolecules, polypeptides, and secondary metabolites. Features the nuclear magnetic resonance (NMR) spectra of a number of large and interesting molecules, ranging from corticosteroids, to secondary metabolites and large synthetically prepared molecules Uses case studies to pair the spectral signals from the various sites of each molecule to their molecular counterparts in a process called assignment Includes complex NMR problems, aiding readers in the development of NMR spectral assignment skills Features input from a leading scientist with over 20 years of research and instruction experience in the field

Case Studies in Superconducting Magnets

Author : Yukikazu Iwasa
Publisher : Springer Science & Business Media
ISBN 13 : 0306470624
Total Pages : 421 pages
Book Rating : 4.3/5 (64 download)

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Book Synopsis Case Studies in Superconducting Magnets by : Yukikazu Iwasa

Download or read book Case Studies in Superconducting Magnets written by Yukikazu Iwasa and published by Springer Science & Business Media. This book was released on 2006-04-11 with total page 421 pages. Available in PDF, EPUB and Kindle. Book excerpt: Designed for graduate students in mechanical engineering, this textbook discusses the basic concepts of superconducting magnet technology. Important topics covered include field distribution, magnets, force, thermal stability, dissipation, and protection. To help the students excel in the field, each chapter contains tutorial problems, accompanied by solutions, utilizing solenoidal magnets as examples.

Modern NMR Approaches to the Structure Elucidation of Natural Products

Author : Antony Williams
Publisher : Royal Society of Chemistry
ISBN 13 : 1849733937
Total Pages : 532 pages
Book Rating : 4.8/5 (497 download)

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Book Synopsis Modern NMR Approaches to the Structure Elucidation of Natural Products by : Antony Williams

Download or read book Modern NMR Approaches to the Structure Elucidation of Natural Products written by Antony Williams and published by Royal Society of Chemistry. This book was released on 2016-12-14 with total page 532 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Ghanian plant Cryptolepis sanguinolenta is the source of a series of fascinating indoloquinoline alkaloids. The most unusual member of this alkaloid series was initially proposed to be a spiro nonacyclic structure, named cryptospirolepine, and was elucidated in 1993 based on the technologies available at that time. There were, however, several annoying attributes to the structure that bothered analysts for the ensuing 22 years. During the two decades that followed the initial work there have been enormous developments in NMR technology. Using new experimental approaches, specifically homodecoupled 1,1- and 1,n-HD-ADEQUATE NMR experiments developed in 2014, the structure of only a 700 µg sample of cryptospirolepine has been revised and is shown on the cover of this volume. The confluence of the NMR technological and methodological advances that allowed the revision of the structure of cryptospirolepine using a submilligram sample seems a fitting example for this book, which is dedicated to the NMR characterization of various classes of natural products. Volume 2 considers data processing and algorithmic based analyses tailored to natural product structure elucidation and reviews the application of NMR to the analysis of a series of different natural product families including marine natural products, terpenes, steroids, alkaloids and carbohydrates. Volume 1 discusses contemporary NMR approaches including optimized and future hardware and experimental approaches to obtain both the highest quality and most appropriate spectral data for analysis. These books, bringing together acknowledged experts, uniquely focus on the combination of experimental approaches and modern hardware and software applied to the structure elucidation of natural products. The volumes will be an essential resource for NMR spectroscopists, natural product chemists and industrial researchers working on natural product analysis or the characterization of impurities and degradation products of pharmaceuticals that can be as scarce as natural product samples.

NMR and MRI of Electrochemical Energy Storage Materials and Devices

Author : Yong Yang
Publisher : Royal Society of Chemistry
ISBN 13 : 1839160101
Total Pages : 573 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis NMR and MRI of Electrochemical Energy Storage Materials and Devices by : Yong Yang

Download or read book NMR and MRI of Electrochemical Energy Storage Materials and Devices written by Yong Yang and published by Royal Society of Chemistry. This book was released on 2021-06-17 with total page 573 pages. Available in PDF, EPUB and Kindle. Book excerpt: Energy storage material is a hot topic in material science and chemistry. During the past decade, nuclear magnetic resonance (NMR) has emerged as a powerful tool to aid understanding of the working and failing mechanisms of energy storage materials and devices. The aim of this book is to introduce the use of NMR methods for investigating electrochemical storage materials and devices. Presenting a comprehensive overview of NMR spectroscopy and magnetic resonance imaging (MRI) on energy storage materials, the book will include the theory of paramagnetic interactions and relevant calculation methods, a number of specific NMR approaches developed in the past decade for battery materials (e.g. in situ, ex situ NMR, MRI, DNP, 2D NMR, NMR dynamics) and case studies on a variety of related materials. Helping both NMR spectroscopists entering the field of batteries and battery specialists seeking diagnostic methods for material and device degradation, it is written by leading authorities from international research groups in this field.

Case Studies in Superconducting Magnets

Author : Yukikazu Iwasa
Publisher : Springer Science & Business Media
ISBN 13 : 0387098003
Total Pages : 717 pages
Book Rating : 4.3/5 (87 download)

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Book Synopsis Case Studies in Superconducting Magnets by : Yukikazu Iwasa

Download or read book Case Studies in Superconducting Magnets written by Yukikazu Iwasa and published by Springer Science & Business Media. This book was released on 2009-04-05 with total page 717 pages. Available in PDF, EPUB and Kindle. Book excerpt: The 2nd edition emphasizes two areas not emphasized in the 1st edition: 1) high-temperature superconductor (HTS) magnets; 2) NMR (nuclear magnetic resonance) and MRI (magnetic resonance imaging) magnets. Despite nearly 40 years of R and D on superconducting magnet technology, most areas, notably fusion and electric power applications, are still in the R and D stage. One exception is in the area of NMR and MRI. NMR magnets are very popular among chemists, biologists, genome scientists, and most of all, by drug manufacturers for drug discovery and development. MRI and NMR magnets have become the most successful application of superconducting magnet technology and this trend should continue. The 2nd edition will have new materials never treated formally in any other book of this kind. As with the 1st, most subjects will be presented through problem format to educate and train the designer.

NMR in Physiology and Biomedicine

Author : Robert J. Gillies
Publisher :
ISBN 13 :
Total Pages : 506 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis NMR in Physiology and Biomedicine by : Robert J. Gillies

Download or read book NMR in Physiology and Biomedicine written by Robert J. Gillies and published by . This book was released on 1994 with total page 506 pages. Available in PDF, EPUB and Kindle. Book excerpt: Collected works of a noted Pakistani poet, particularly songs without musical notation.

Experimental Approaches of NMR Spectroscopy

Author : The Nuclear Magnetic Resonance Society of Japan
Publisher : Springer
ISBN 13 : 9811059667
Total Pages : 636 pages
Book Rating : 4.8/5 (11 download)

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Book Synopsis Experimental Approaches of NMR Spectroscopy by : The Nuclear Magnetic Resonance Society of Japan

Download or read book Experimental Approaches of NMR Spectroscopy written by The Nuclear Magnetic Resonance Society of Japan and published by Springer. This book was released on 2017-11-23 with total page 636 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book describes the advanced developments in methodology and applications of NMR spectroscopy to life science and materials science. Experts who are leaders in the development of new methods and applications of life and material sciences have contributed an exciting range of topics that cover recent advances in structural determination of biological and material molecules, dynamic aspects of biological and material molecules, and development of novel NMR techniques, including resolution and sensitivity enhancement. First, this book particularly emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potentials of NMR spectroscopy. Second, the book is designed for those who are involved in either developing the technique or expanding the NMR application fields by applying them to specific samples. Third, the Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.

Structure-activity Relationship Studies in Drug Development by NMR Spectroscopy

Author : Atta-ur- Rahman
Publisher : Bentham Science Publishers
ISBN 13 : 1608051641
Total Pages : 221 pages
Book Rating : 4.6/5 (8 download)

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Book Synopsis Structure-activity Relationship Studies in Drug Development by NMR Spectroscopy by : Atta-ur- Rahman

Download or read book Structure-activity Relationship Studies in Drug Development by NMR Spectroscopy written by Atta-ur- Rahman and published by Bentham Science Publishers. This book was released on 2011 with total page 221 pages. Available in PDF, EPUB and Kindle. Book excerpt: "NMR (Nuclear Magnetic Resonance) Spectroscopy has found significant applications in drug discovery based on its capacity to map molecular interactions at the atomic level. Chemical shifts, cross relaxation, and exchange of protons are among the NMR parame"

Annual Reports on NMR Spectroscopy

Author :
Publisher : Academic Press
ISBN 13 : 0128209739
Total Pages : 378 pages
Book Rating : 4.1/5 (282 download)

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Book Synopsis Annual Reports on NMR Spectroscopy by :

Download or read book Annual Reports on NMR Spectroscopy written by and published by Academic Press. This book was released on 2020-04-29 with total page 378 pages. Available in PDF, EPUB and Kindle. Book excerpt: Annual Reports on NMR Spectroscopy, Volume 100, is a premier resource for both specialists and non-specialists who are looking to become familiar with new techniques and applications in NMR spectroscopy. Chapters in this new release cover In Operando NMR Studies, Recent Developments in Automotive Differential Analysis of NMR Results, Applications of SIMPSON to NMR Studies of Peptides and Proteins, Recent Developments in NMR Line Shape Analysis, and more. Serves as the premier resource for learning the new techniques and applications of NMR spectroscopy Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)

NMR and MRI of Electrochemical Energy Storage Materials and Devices

Author : Yong Yang
Publisher : Royal Society of Chemistry
ISBN 13 : 1788018486
Total Pages : 573 pages
Book Rating : 4.7/5 (88 download)

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Book Synopsis NMR and MRI of Electrochemical Energy Storage Materials and Devices by : Yong Yang

Diffusion and Electrophoretic NMR

Author : Peter Stilbs
Publisher : Walter de Gruyter GmbH & Co KG
ISBN 13 : 3110551535
Total Pages : 350 pages
Book Rating : 4.1/5 (15 download)

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Book Synopsis Diffusion and Electrophoretic NMR by : Peter Stilbs

Download or read book Diffusion and Electrophoretic NMR written by Peter Stilbs and published by Walter de Gruyter GmbH & Co KG. This book was released on 2019-08-19 with total page 350 pages. Available in PDF, EPUB and Kindle. Book excerpt: Diffusion and Eletrophoretic NMR experiments resolve chemical compounds based on their molecular motion. This publication introduces the basics of these methods and explains how they can be used to measure the size of molecules and aggregates, to determine degree of polymerization and to solve other chemical problems. Supplied with many case studies, the book is a must-have for students and researchers who work with practical NMR measurements.

200 and More NMR Experiments

Author : Stefan Berger
Publisher : John Wiley & Sons
ISBN 13 : 3527310673
Total Pages : 868 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis 200 and More NMR Experiments by : Stefan Berger

Download or read book 200 and More NMR Experiments written by Stefan Berger and published by John Wiley & Sons. This book was released on 2004-07-02 with total page 868 pages. Available in PDF, EPUB and Kindle. Book excerpt: This work-book will guide you safely, in step-by-step descriptions, through every detail of the NMR experiments within, beginning with 1D routine experiments and ending with a series of advanced 3D experiments on a protein: ? Which experiment can best yield the desired information? ? How must the chosen experiment be performed? ? How does one read the required information from the spectrum? ? How does this particular pulse sequence work? ? Which other experiments give similar information? This third edition of the book, following its two highly successful predecessors, has been revised and expanded to 206 experiments. They are organized in 15 chapters, covering test procedures and routine spectra, variable temperature measurements, the use of auxiliary reagents, 1D multipulse experiments, spectra of heteronuclides, and the application of selective pulses. The second and third dimensions are introduced using pulsed field gradients, and experiments on solid state materials are described. A key part describes 3D experiments on the protein ubiquitin with 76 amino acids. What is new in this third edition? 1. 24 new experiments have been inserted into the 14 chapters that were in the 2nd edition, e.g., alpha/beta-SELINCOR-TOCSY, WET, DOSY, ct-COSY, HMSC, HSQC with adiabatic pulses, HETLOC. J-resolved HMBC, (1,1)- and (1,n)-ADEQUATE, STD, REDOR, and HR-MAS. 2. 20 new protein NMR experiments have been specially devised and are collected in the newly added Chapter 15, ProteinNMR, for which one needs a special model sample: fully 13C- and 15N-labeled human ubiquitin. Techniques used include the constant time principle, the PEP method, filters, gradient selection, and the echo/anti-echo procedure. The guide has been written by experts in this field, following the principle of learning by doing: all the experiments have been specially performed for this book, exactly as described and shown in the spectra that are reproduced. Being a reference source and work-book for the NMR laboratory as well as a textbook, it is a must for every scientist working with NMR, as well as for students preparing for their laboratory courses

Modern NMR Techniques for Chemistry Research

Author : A.E. Derome
Publisher : Elsevier
ISBN 13 : 1483286428
Total Pages : 299 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis Modern NMR Techniques for Chemistry Research by : A.E. Derome

Download or read book Modern NMR Techniques for Chemistry Research written by A.E. Derome and published by Elsevier. This book was released on 2013-10-22 with total page 299 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.

Carbohydrate Chemistry: Chemical and Biological Approaches Volume 44

Author : Amelia Pilar Rauter
Publisher : Royal Society of Chemistry
ISBN 13 : 1788013689
Total Pages : 307 pages
Book Rating : 4.7/5 (88 download)

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Book Synopsis Carbohydrate Chemistry: Chemical and Biological Approaches Volume 44 by : Amelia Pilar Rauter

Download or read book Carbohydrate Chemistry: Chemical and Biological Approaches Volume 44 written by Amelia Pilar Rauter and published by Royal Society of Chemistry. This book was released on 2020-10-06 with total page 307 pages. Available in PDF, EPUB and Kindle. Book excerpt: Carbohydrate Chemistry is an invaluable volume demonstrating the interdisciplinary nature of modern carbohydrate research and containing analysed, evaluated and distilled information on the latest research in the area.

50 and More Essential NMR Experiments

Author : Matthias Findeisen
Publisher : John Wiley & Sons
ISBN 13 : 352733694X
Total Pages : 322 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis 50 and More Essential NMR Experiments by : Matthias Findeisen

Download or read book 50 and More Essential NMR Experiments written by Matthias Findeisen and published by John Wiley & Sons. This book was released on 2013-07-30 with total page 322 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.

Two-Dimensional (2D) NMR Methods

Author : Konstantin Ivanov
Publisher : John Wiley & Sons
ISBN 13 : 1119806690
Total Pages : 597 pages
Book Rating : 4.1/5 (198 download)

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Book Synopsis Two-Dimensional (2D) NMR Methods by : Konstantin Ivanov

Download or read book Two-Dimensional (2D) NMR Methods written by Konstantin Ivanov and published by John Wiley & Sons. This book was released on 2023-07-03 with total page 597 pages. Available in PDF, EPUB and Kindle. Book excerpt: TWO-DIMENSIONAL (2D) NMR METHODS Practical guide explaining the fundamentals of 2D-NMR for experienced scientists as well as relevant for advanced students Two-Dimensional (2D) NMR Methods is a focused work presenting an overview of 2D-NMR concepts and techniques, including basic principles, practical applications, and how NMR pulse sequences work. Contributed to by global experts with extensive experience in the field, Two-Dimensional (2D) NMR Methods provides in-depth coverage of sample topics such as: Basics of 2D-NMR, data processing methods (Fourier and beyond), product operator formalism, basics of spin relaxation, and coherence transfer pathways Multidimensional methods (single- and multiple-quantum spectroscopy), NOESY (principles and applications), and DOSY methods Multiple acquisition strategies, anisotropic NMR in molecular analysis, ultrafast 2D methods, and multidimensional methods in bio-NMR TROSY (principles and applications), field-cycling and 2D NMR, multidimensional methods and paramagnetic NMR, and relaxation dispersion experiments This text is a highly useful resource for NMR specialists and advanced students studying NMR, along with users in research, academic and commercial laboratories that study or conduct experiments in NMR.

Modern NMR Techniques for Synthetic Chemistry

Author : Julie Fisher
Publisher : CRC Press
ISBN 13 : 1466592249
Total Pages : 364 pages
Book Rating : 4.4/5 (665 download)

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Book Synopsis Modern NMR Techniques for Synthetic Chemistry by : Julie Fisher

Download or read book Modern NMR Techniques for Synthetic Chemistry written by Julie Fisher and published by CRC Press. This book was released on 2014-10-13 with total page 364 pages. Available in PDF, EPUB and Kindle. Book excerpt: A blend of theory and practical advice, Modern NMR Techniques for Synthetic Chemistry illustrates how NMR spectroscopy can be used to determine the abundance, size, shape, and function of organic molecules. It provides you with a description the NMR technique used (more pictorial than mathematical), indicating the most common pulse sequences, some practical information as appropriate, followed by illustrative examples. This format is followed for each chapter so you can skip the more theoretical details if the practical aspects are what interest you. Following a discussion of basic parameters, the book describes the utility of NMR in detecting and quantifying dynamic processes, with particular emphasis on the usefulness of saturation-transfer (STD) techniques. It details pulsed–field gradient approaches to diffusion measurement, diffusion models, and approaches to ‘inorganic’ nuclei detection, important as many synthetic pathways to new organics involve heavier elements. The text concludes with coverage of applications of NMR to the analysis of complex mixtures, natural products, carbohydrates, and nucleic acids—all areas of activity for researchers working at the chemistry-life sciences interface. The book’s unique format provides some theoretical insight into the NMR technique used, indicating the most common pulse sequences. The book draws upon several NMR methods that are resurging or currently hot in the field and indicates the specific pulse sequence used by various spectrometer manufacturers for each technique. It examines the analysis of complex mixtures, a feature not found in most books on this topic.