Neutron Activation Analysis Detection Limits Using 252Cf Sources

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ISBN 13 :
Total Pages : 5 pages
Book Rating : 4.:/5 (684 download)

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Book Synopsis Neutron Activation Analysis Detection Limits Using 252Cf Sources by :

Download or read book Neutron Activation Analysis Detection Limits Using 252Cf Sources written by and published by . This book was released on 2000 with total page 5 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Savannah River Technology Center (SRTC) developed a neutron activation analysis facility several decades ago using low-flux 252Cf neutron sources. Throughout this time, the facility has addressed areas of applied interest in managing the Savannah River Site. Some applications are unique due to the site's operating history and its chemical processing facilities. Because sensitivity needs for many applications are not severe, they can be accomplished using an approximately 6 mg 252Cf neutron activation analysis facility. The SRTC 252Cf facility continues to support applied research programs at SRTC as well as other SRS programs for environmental and waste management customers. Samples analyzed by NAA include organic compounds, metal alloys, sediments, site process solutions, and many other materials. Numerous radiochemical analyses also rely on the facility for production of short-lived tracers and small-scale isotope production for separation methods testing. These applications are more fully reviewed in Reference 1. Although the flux (ca. 2 x 107 neutrons/(cm2.sec)) is low relative to reactor facilities, over 40 elements can be detected at low- and sub-part-per-million levels. Detection limits provided by the facility are adequate for many analytical projects. Other multielement analysis methods, particularly inductively coupled plasma atomic emission (ICP-AE) and inductively coupled plasma mass spectrometry (ICP-MS), can now provide sensitivities on dissolved samples that are often better than those available by NAA using low-flux isotopic sources.

Mercury Detection Limits for Prompt Gamma-ray Neutron Activation Analysis in Containers of Chlorine-rich Chemicals

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ISBN 13 :
Total Pages : 110 pages
Book Rating : 4.:/5 (166 download)

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Book Synopsis Mercury Detection Limits for Prompt Gamma-ray Neutron Activation Analysis in Containers of Chlorine-rich Chemicals by : Carl Jayson Wharton

Download or read book Mercury Detection Limits for Prompt Gamma-ray Neutron Activation Analysis in Containers of Chlorine-rich Chemicals written by Carl Jayson Wharton and published by . This book was released on 2006 with total page 110 pages. Available in PDF, EPUB and Kindle. Book excerpt: Prompt Gamma-ray Neutron Activation Analysis (PGNAA) measurements were performed on simulated mustard gas (HD) {Cl(CH2)2S(CH2)2Cl} using the Idaho National Laboratory's Portable Isotopic Neutron Spectroscopy (PINS) system in an attempt to determine the lower limit of detection for mercury contamination in ton containers filled with this chemical agent. For the experiment the simulant was homogeneously doped with five different concentrations of mercuric oxide (HgO), namely, 0, 100, 200, 400, and 800 ppm. The measurements were then repeated for three different container types, namely, a DOT type 500X ton container, a 55-gallon standard waste drum, and a cardboard box. To measure the 368-keV mercury capture gamma ray, a 5-microgram californium- 252 (252Cf) source, emitting 107 neutrons per second, was used to excite the contents of a container, and a high-resolution, high-purity germanium (HPGe) detector was used to measure the resulting gamma rays. The spectral data were background subtracted and a least-squares analysis was performed on the experimental data points to determine the minimum detection limit (MDL) using the analysis method of Currie. The mercury concentration detection limit was found at the 99% confidence level to be 10,000 ppm for a ton container, 961 ppm for a 55-gallon standard waste drum, and 661 ppm for the cardboard box. Additionally, the mercury concentration limit was found to be 1,930 ppm, 607 ppm, and 251 ppm at the 95% confidence level in the ton container, 55-gallon drum, and cardboard box, respectively. The sensitivity of the method is limited by the attenuation of exiting mercury gamma rays by the iron wall of the 500X ton container and by the number of thermal neutron capture gamma rays created by the container wall and by the chlorine present in agent HD. To improve the sensitivity to mercury, the chlorine and iron signals would need to be minimized.

Some Limitations on the Use of Neutron Activation Analysis

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ISBN 13 :
Total Pages : 8 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Some Limitations on the Use of Neutron Activation Analysis by : Richard Walter Fink

Download or read book Some Limitations on the Use of Neutron Activation Analysis written by Richard Walter Fink and published by . This book was released on 1962 with total page 8 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Californium-252 Progress

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ISBN 13 :
Total Pages : 652 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Californium-252 Progress by : U.S. Atomic Energy Commission

Download or read book Californium-252 Progress written by U.S. Atomic Energy Commission and published by . This book was released on 1972 with total page 652 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Nuclear Science Abstracts

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ISBN 13 :
Total Pages : 934 pages
Book Rating : 4.0/5 ( download)

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Book Synopsis Nuclear Science Abstracts by :

Download or read book Nuclear Science Abstracts written by and published by . This book was released on 1976 with total page 934 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Nuclear Cross Sections for Technology

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ISBN 13 :
Total Pages : 1064 pages
Book Rating : 4.:/5 (31 download)

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Book Synopsis Nuclear Cross Sections for Technology by : Joseph L. Fowler

Download or read book Nuclear Cross Sections for Technology written by Joseph L. Fowler and published by . This book was released on 1980 with total page 1064 pages. Available in PDF, EPUB and Kindle. Book excerpt:

NBS Special Publication

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ISBN 13 :
Total Pages : 1056 pages
Book Rating : 4.:/5 (2 download)

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Book Synopsis NBS Special Publication by :

Download or read book NBS Special Publication written by and published by . This book was released on 1980 with total page 1056 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Energy Research Abstracts

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ISBN 13 :
Total Pages : 1520 pages
Book Rating : 4.3/5 (129 download)

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Book Synopsis Energy Research Abstracts by :

Download or read book Energy Research Abstracts written by and published by . This book was released on 1979 with total page 1520 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Modern Instrumental Methods of Elemental Analysis of Petroleum Products and Lubricants

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Publisher : ASTM International
ISBN 13 : 0803114168
Total Pages : 160 pages
Book Rating : 4.8/5 (31 download)

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Book Synopsis Modern Instrumental Methods of Elemental Analysis of Petroleum Products and Lubricants by : R. A. Nadkarni

Download or read book Modern Instrumental Methods of Elemental Analysis of Petroleum Products and Lubricants written by R. A. Nadkarni and published by ASTM International. This book was released on 1991 with total page 160 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Californium-252 Review

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ISBN 13 :
Total Pages : 104 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Californium-252 Review by : U.S. Atomic Energy Commission

Download or read book Californium-252 Review written by U.S. Atomic Energy Commission and published by . This book was released on 1971 with total page 104 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Neutron Generators for Analytical Purposes

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Publisher : IAEA Radiation Technology Repo
ISBN 13 : 9789201251107
Total Pages : 145 pages
Book Rating : 4.2/5 (511 download)

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Book Synopsis Neutron Generators for Analytical Purposes by : International Atomic Energy Agency

Download or read book Neutron Generators for Analytical Purposes written by International Atomic Energy Agency and published by IAEA Radiation Technology Repo. This book was released on 2012 with total page 145 pages. Available in PDF, EPUB and Kindle. Book excerpt: This publication addresses recent developments in neutron generator (NG) technology. It presents information on compact instruments with high neutron yield to be used for neutron activation analysis (NAA) and prompt gamma neutron activation analysis in combination with high count rate spectrometers. Traditional NGs have been shown to be effective for applications including borehole logging, homeland security, nuclear medicine and the on-line analysis of aluminium, coal and cement. Pulsed fast thermal neutron analysis, as well as tagged and timed neutron analysis, are additional techniques which can be applied using NG. Furthermore, NG can effectively be used for elemental analysis and is also effective for analysis of hidden materials by neutron radiography. Useful guidelines for developing NG based research laboratories are also provided in this publication.

Transactions of the American Nuclear Society

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ISBN 13 :
Total Pages : 922 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Transactions of the American Nuclear Society by : American Nuclear Society

Download or read book Transactions of the American Nuclear Society written by American Nuclear Society and published by . This book was released on 2000 with total page 922 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Review

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ISBN 13 :
Total Pages : 564 pages
Book Rating : 4.3/5 (243 download)

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Book Synopsis Review by : Oak Ridge National Laboratory

Download or read book Review written by Oak Ridge National Laboratory and published by . This book was released on 1987 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt:

The Analysis of Nuclear Materials and Their Environments

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Publisher : Springer
ISBN 13 : 331958006X
Total Pages : 308 pages
Book Rating : 4.3/5 (195 download)

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Book Synopsis The Analysis of Nuclear Materials and Their Environments by : Claude André Degueldre

Download or read book The Analysis of Nuclear Materials and Their Environments written by Claude André Degueldre and published by Springer. This book was released on 2017-10-11 with total page 308 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides an overview of passive and interactive analytical techniques for nuclear materials. The book aims to update readers on new techniques available and provide an introduction for those who are new to the topic or are looking to move into actinides and nuclear materials science. The characterization of actinide species and radioactive materials is vital for understanding how these elements and radioactive isotopes are formed and behave and how these materials can be improved. The analysis of the actinides or radioactive materials goes beyond spent fuel science to the applicable complete fuel cycle and including analysis of reactor materials.

Neutron-activation Analysis

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Total Pages : pages
Book Rating : 4.:/5 (921 download)

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Book Synopsis Neutron-activation Analysis by :

Download or read book Neutron-activation Analysis written by and published by . This book was released on 1970 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: The general theory, methodology, and types of neutron activation analysis are discussed. Reactor-thermal neutrons are by far the most widely used in activation analysis, and observed limits of detection for the various elements are tabulated, and examples of applications of this technique to the purely analytical and geochemical fields are quoted. Generator-fast neutrons, which are suited to the determination of macro amounts of the major elements encountered in geology and the isotopic neutron source, are shown to be suitable for in situ irradiations - either in the field or in industrial plants where continuous monitoring is a requirement.

Activation Analysis

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Publisher : CRC Press
ISBN 13 : 9780849345845
Total Pages : 646 pages
Book Rating : 4.3/5 (458 download)

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Book Synopsis Activation Analysis by : Zeev Alfassi

Download or read book Activation Analysis written by Zeev Alfassi and published by CRC Press. This book was released on 1990-06-22 with total page 646 pages. Available in PDF, EPUB and Kindle. Book excerpt: This timely publication covers prompt measurements as well as delayed activation measurements used in chemical analysis of the elements. It describes the various possibilities of activation: neutrons, charged ions, and photons. Also discussed are the advantages and disadvantages of each activation method. These volumes are important for those in geology, archaeology, biology, analytical chemistry, radioanalytical and nuclear chemistry, the semiconductor industry, and others.

Biological Monitoring of Toxic Metals

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Publisher : Springer Science & Business Media
ISBN 13 : 1461309611
Total Pages : 672 pages
Book Rating : 4.4/5 (613 download)

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Book Synopsis Biological Monitoring of Toxic Metals by : Thomas W. Clarkson

Download or read book Biological Monitoring of Toxic Metals written by Thomas W. Clarkson and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 672 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the result of a conference on "Biological Monitoring of Metals" held in Rochester, June 2-6, 1986, organized jointly by the Environmental Health Sciences Center of the School of Medicine and Dentistry of the University of Rochester, NY, and the Scientific Committee on the Toxicology of Metals within the International Commission on Occupational Health (ICOH) at the Karolinska Institute and the National (Swedish) Institute of Environmental Medicine and the University of Umea, Sweden. The aim of the Conference was to define and evaluate the scientific basis for the biological monitoring of metals. The conference was co-sponsored by the World Health Organization through its International Program on Chemical Safety and received substantial encouragement and support from the Swedish Work Environmental Fund and the United States Environmental Protection Agency. This was the second conference organized jointly by the Scientific Committee on the Toxicology of Metals and The Toxicology Division of the University of Rochester. The previous joint conference was held in 1982 on the Reproductive and Developmental Toxicity of Metals. In addition, conferences have been organized by each group (see Appendices A and B). Several of these conferences are specially relevant to the topic of the current conference. These include the joint conference mentioned above and the conferences on dose-effect and dose-response relationship held in Tokyo in 1974 and on accumulation of metals held in Buenos Aires in 1972.