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Milestones In The Evolution Of Chromatography
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Book Synopsis Chapters In The Evolution Of Chromatography by : Leslie S Ettre
Download or read book Chapters In The Evolution Of Chromatography written by Leslie S Ettre and published by World Scientific. This book was released on 2008-06-11 with total page 492 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chromatography, invented more than 100 years ago, is the most widely used separation technique in the world today. It has helped the birth of modern analytical instrumentation and continues to strongly influence the profiles of our chemical, biochemical and clinical laboratories.This book deals with the history of the invention and evolution of chromatography and of the various chromatographic techniques. After discussing the precursors, it elaborates on the activities of M.S. Tswett, the inventor of the technique, and of a few selected key pioneers. It then summarizes the evolution of the various branches of chromatography (planar, ion-exchange, gas and liquid), and also reviews the key role of international symposia in setting the trends in this evolution. Except for individual publications of the author, the history of the evolution of chromatography has not been the subject of any book. Thus, this book fills a major gap in the scientific literature./a
Book Synopsis The Essence of Chromatography by : C. F. Poole
Download or read book The Essence of Chromatography written by C. F. Poole and published by Elsevier. This book was released on 2003 with total page 940 pages. Available in PDF, EPUB and Kindle. Book excerpt: General concepts in column chromatography -- The column in gas chromatography -- Instrumental aspects of gas chromatography -- The column in liquid chromatography -- Instrumental aspects of liquid chromatography -- Thin-layer chromatography -- Supercritical fluid chromatography -- Capillary-electromigration separation techniques -- Spectroscopic detectors for identification and quantification -- Separation of stereoisomers -- Laboratory-scale preparative chromatography.
Book Synopsis Chromatography-A Century of Discovery 1900-2000.The Bridge to The Sciences/Technology by :
Download or read book Chromatography-A Century of Discovery 1900-2000.The Bridge to The Sciences/Technology written by and published by Elsevier. This book was released on 2001-12-18 with total page 734 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chromatography - A Century of Discovery 1900-2000 represents the combined thinking and contributions of many chromatographers. It includes several in-depth feature chapters covering the Beginnings of Chromatography, which highlights M.S. Tswett, the inventor of chromatography, and several other early pioneers. Included are the contributions of several Nobel Laureates,and 125 Chromatography Award Winners and contributors, an extensive bibliography of publications on the History of the Evolution of Chromatography; a presentation of Major International Symposia supporting chromatography and as a bridge to selected sciences. Special chapters are written by well-known Chromatographers on Support and Stationary Phases, and Separations followed by a chapter on Milestones and Paradigm Shifts in Science. New discoveries in the life sciences and medicine, agriculture, the environment and separations technology in the 21st century will rely immeasurably on the 20th century research tools in chromatography and those yet to be developed.
Book Synopsis Liquid Chromatography by : Salvatore Fanali
Download or read book Liquid Chromatography written by Salvatore Fanali and published by Elsevier. This book was released on 2017-06-22 with total page 810 pages. Available in PDF, EPUB and Kindle. Book excerpt: Liquid Chromatography: Fundamentals and Instrumentation, Second Edition, is a single source of authoritative information on all aspects of the practice of modern liquid chromatography. It gives those working in both academia and industry the opportunity to learn, refresh, and deepen their understanding of new fundamentals and instrumentation techniques in the field. In the years since the first edition was published, thousands of papers have been released on new achievements in liquid chromatography, including the development of new stationary phases, improvement of instrumentation, development of theory, and new applications in biomedicine, metabolomics, proteomics, foodomics, pharmaceuticals, and more. This second edition addresses these new developments with updated chapters from the most expert researchers in the field. - Emphasizes the integration of chromatographic methods and sample preparation - Explains how liquid chromatography is used in different industrial sectors - Covers the most interesting and valuable applications in different fields, e.g., proteomic, metabolomics, foodomics, pollutants and contaminants, and drug analysis (forensic, toxicological, pharmaceutical, biomedical) - Includes references and tables with commonly used data to facilitate research, practical work, comparison of results, and decision-making
Book Synopsis Practical Gas Chromatography by : Katja Dettmer-Wilde
Download or read book Practical Gas Chromatography written by Katja Dettmer-Wilde and published by Springer. This book was released on 2014-11-05 with total page 904 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.
Book Synopsis Preparative Enantioselective Chromatography by : Geoffrey B. Cox
Download or read book Preparative Enantioselective Chromatography written by Geoffrey B. Cox and published by John Wiley & Sons. This book was released on 2008-04-15 with total page 344 pages. Available in PDF, EPUB and Kindle. Book excerpt: The development of chiral liquid chromatography, facilitating thestraightforward separation of enantiomers, was a significantadvance in chromatography, leading to widespread application inanalytical chemistry. Application in preparative chromatography hasbeen less rapid, but with the development of single enantiomerpharmaceuticals its use is increasingly common in chemicalsynthesis at laboratory, pilot plant and even full productionscale. Brings non-experts up to speed quickly and comprehensively,facilitating the rapid development of effective separations ofenantiomeric mixtures on a range of process scales Presents case studies drawn from within the pharmaceuticalindustry to clearly illustrate the utility and value of preparativescale enantioselective chromatography in chemical research,development and production Key reference source and entry to the literature so the readerdoes not have to engage in expensive and time consuming literaturesearching
Book Synopsis Columns for Gas Chromatography by : Eugene F. Barry
Download or read book Columns for Gas Chromatography written by Eugene F. Barry and published by John Wiley & Sons. This book was released on 2007-04-27 with total page 315 pages. Available in PDF, EPUB and Kindle. Book excerpt: Choosing the right column is key in Gas Chromatography Gas Chromatography (GC) is the most widely used method for separating and analyzing a wide variety of organic compounds and gases. There have been many recent advancements in both packed column and capillary column GC. With numerous options and considerations, selecting the right column can be complicated. This resource provides essential guidance for scientists and technicians, including: Methods of choosing both capillary and packed columns Selection of dimensions (column length, I.D., film thickness, etc.) and type of column Guidelines for proper connections of the column to the injector and detector United States Pharmacopeia and National Formulary chromatographic methods ASTM, EPA, NIOSH, and OSHA column selection specifications Information on the advantages of computer assistance in GC and multidimensional GC Comprehensive information on column oven temperature control Columns for Gas Chromatography: Performance and Selection is a hands-on reference for scientists and technicians using GC.
Book Synopsis From Classical to Modern Chemistry by : Peter J. T. Morris
Download or read book From Classical to Modern Chemistry written by Peter J. T. Morris and published by Royal Society of Chemistry. This book was released on 2002 with total page 386 pages. Available in PDF, EPUB and Kindle. Book excerpt: Most chemists today have either taken part in, or been affected by, the chemical revolution that has taken place over the course of the last century. Developments in instrumentation have changed not just what chemists do, but also how they think about chemistry. New and exciting areas of previously inaccessible research have been opened up as a direct result of this revolution. This is the first book to examine this instrumental revolution and goes on to assess the impact on chemical practice in areas ranging from organic chemistry and biochemistry to environmental analysis and process control, thus demonstrating how fundamental and extensive are the changes that have occurred. With contributions from internationally recognised specialists, this lavishly illustrated book provides a focal point for any historian of chemistry or chemist with an interest in this fascinating topic. This book is published in association with the Science Museum, London, UK and the Chemical Heritage Foundation, Philadelphia.
Book Synopsis Liquid-Phase Extraction by : Colin F. Poole
Download or read book Liquid-Phase Extraction written by Colin F. Poole and published by Elsevier. This book was released on 2019-08-29 with total page 818 pages. Available in PDF, EPUB and Kindle. Book excerpt: Liquid Phase Extraction thoroughly presents both existing and new techniques in liquid phase extraction. It not only provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample, but also showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including countercurrent chromatography, pressurized-liquid extraction, single-drop Microextraction, and more. Written by recognized experts in their respective fields, it serves as a one-stop reference for those who need to know which technique to choose for liquid phase extraction. Used in conjunction with a similar release, Solid Phase Extraction, it allows users to master this crucial aspect of sample preparation. - Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice - Includes extensive referencing that facilitates the identification of key information - Aimed at both entry-level scientists and those who want to explore new techniques and methods
Book Synopsis Liquid Chromatography by : L.R. Snyder
Download or read book Liquid Chromatography written by L.R. Snyder and published by Elsevier Inc. Chapters. This book was released on 2013-01-08 with total page 27 pages. Available in PDF, EPUB and Kindle. Book excerpt: The evolution of high performance liquid chromatography is reviewed with an emphasis on the innovations that occurred in the technique in response to sample needs. The general themes are the development and/or applications of basic theory as catalyst for change, invention of new chromatographic modes, evolution of column technology, and the development and improvement of instrumentation. Steady progress in these areas rather than sudden change is responsible for the column chemistries, particle technology, instrumentation, and data handling tools available today.
Download or read book LC-NMR written by Nina C. Gonnella and published by CRC Press. This book was released on 2020-01-15 with total page 344 pages. Available in PDF, EPUB and Kindle. Book excerpt: The isolation and structural characterization of substances present at very low concentrations, as is necessary to satisfy regulatory requirements for pharmaceutical drug degradants and impurities, can present scientific challenges. The coupling of HPLC with NMR spectroscopy has been at the forefront of cutting-edge technologies to address these issues. LC-NMR: Expanding the Limits of Structure Elucidation presents a comprehensive overview of key concepts in HPLC and NMR that are required to achieve definitive structure elucidation with very low levels of analytes. Because skill sets from both of these highly established disciplines are involved in LC-NMR, the author provides introductory background to facilitate readers’ proficiency in both areas, including an entire chapter on NMR theory. The much-anticipated second edition provides guidance in setting up LC-NMR systems, discussion of LC methods that are compatible with NMR, and an update on recent hardware and software advances for system performance, such as improvements in magnet design, probe technology, and solvent suppression techniques that enable unprecedented mass sensitivity in NMR. This edition features methods to quantify concentration and assess purity of isolated metabolites on the micro scale and incorporates computational approaches to accelerate the structure elucidation process. The author also includes implementation and application of qNMR and automated and practical use of computational chemistry combined with QM and DFT to predict highly accurate NMR chemical shifts. The text focuses on current developments in chromatographic-NMR integration, with particular emphasis on utility in the pharmaceutical industry. Applications include trace analysis, analysis of mixtures, and structural characterization of degradation products, impurities, metabolites, peptides, and more. The text discusses novel uses and emerging technologies that challenge detection limits as well future directions for this important technique. This book is a practical primary resource for NMR structure determination—including theory and application—that guides the reader through the steps required for isolation and NMR structure elucidation on the micro scale.
Book Synopsis New Generation Green Solvents for Separation and Preconcentration of Organic and Inorganic Species by : Mustafa Soylak
Download or read book New Generation Green Solvents for Separation and Preconcentration of Organic and Inorganic Species written by Mustafa Soylak and published by Elsevier. This book was released on 2020-04-07 with total page 482 pages. Available in PDF, EPUB and Kindle. Book excerpt: New Generation Green Solvents for Separation and Preconcentration of Organic and Inorganic Species is designed to help researchers and students understand the production and application of new generation green solvents in separation- and preconcentration-based analytical methods. Beginning with the historical background and milestones in the development of analytical instrumentation, the book goes on to give a detailed overview of the most up-to-date uses of green solvents in sample preparation. Using a wealth of examples, it compares old and new extraction procedures and explores the many applications of new generation green solvents. Practical, easy-to-follow experiments are used to illustrate the key concepts. This practical guide helps to promote the use of safer, more sustainable solvents in analytical chemistry and beyond for environmental scientists, researchers in pharmaceutical and biotech industries, and students in analytical chemistry. - Covers the basic analytical theory essential for understanding extraction- and microextraction-based separation and preconcentration methods - Explains combination use of new generation solvents with various detection systems, including UV-VIS, ICP-MS, HPLC, LC-MS, GC-MS, and LC-MS/MS - Emphasizes trace chemical component separation, preconcentration and analysis
Book Synopsis Bioprocess Engineering by : Pau Loke Show
Download or read book Bioprocess Engineering written by Pau Loke Show and published by CRC Press. This book was released on 2019-05-24 with total page 233 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bioprocess Engineering: Downstream Processing is the first book to present the principles of bioprocess engineering, focusing on downstream bioprocessing. It aims to provide the latest bioprocess technology and explain process analysis from an engineering point of view, using worked examples related to biological systems. This book introduces the commonly used technologies for downstream processing of biobased products. The covered topics include centrifugation, filtration, membrane separation, reverse osmosis, chromatography, biosorption, liquid-liquid separation, and drying. The basic principles and mechanism of separation are covered in each of the topics, wherein the engineering concept and design are emphasized. This book is aimed at bioprocess engineers and professionals who wish to perform downstream processing for their feedstock, as well as students.
Book Synopsis Encyclopedia of Analytical Science by :
Download or read book Encyclopedia of Analytical Science written by and published by Elsevier. This book was released on 2019-04-02 with total page 5142 pages. Available in PDF, EPUB and Kindle. Book excerpt: The third edition of the Encyclopedia of Analytical Science, Ten Volume Set is a definitive collection of articles covering the latest technologies in application areas such as medicine, environmental science, food science and geology. Meticulously organized, clearly written and fully interdisciplinary, the Encyclopedia of Analytical Science, Ten Volume Set provides foundational knowledge across the scope of modern analytical chemistry, linking fundamental topics with the latest methodologies. Articles will cover three broad areas: analytical techniques (e.g., mass spectrometry, liquid chromatography, atomic spectrometry); areas of application (e.g., forensic, environmental and clinical); and analytes (e.g., arsenic, nucleic acids and polycyclic aromatic hydrocarbons), providing a one-stop resource for analytical scientists. Offers readers a one-stop resource with access to information across the entire scope of modern analytical science Presents articles split into three broad areas: analytical techniques, areas of application and and analytes, creating an ideal resource for students, researchers and professionals Provides concise and accessible information that is ideal for non-specialists and readers from undergraduate levels and higher
Book Synopsis Temperature-Programmed Gas Chromatography by : Leonid M. Blumberg
Download or read book Temperature-Programmed Gas Chromatography written by Leonid M. Blumberg and published by John Wiley & Sons. This book was released on 2010-12-13 with total page 363 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a comprehensive up-to-date overview of temperature-programmed gas chromatography (GC). The first part of the book introduces the reader to the basics concepts of GC, as well as the key properties of GC columns. The second part describes the mathematical and physical background of GC. In the third part, different aspects in the formation of a chromatogram are discussed, including retention times, peak spacing and peak widths. An invaluable reference for any chromatographer and analytical chemist, it provides all the answers to questions like: At what temperature does a solute elute in a temperature-programmed analysis? What is the value of the retention factor of eluting solute? How wide are the peaks? How large is the time distance between two peaks? How do all these parameters depend on the heating rate?
Book Synopsis Fundamentals of Analytical Toxicology by : Robert J. Flanagan
Download or read book Fundamentals of Analytical Toxicology written by Robert J. Flanagan and published by John Wiley & Sons. This book was released on 2008-02-28 with total page 546 pages. Available in PDF, EPUB and Kindle. Book excerpt: The analytical toxicologist may be required to detect, identify,and in many cases measure a wide variety of compounds in samplesfrom almost any part of the body or in related materials such asresidues in syringes or in soil. This book gives principles andpractical information on the analysis of drugs and poisons inbiological specimens, particularly clinical and forensic specimens. After providing some background information the book coversaspects of sample collection, transport, storage and disposal, andsample preparation. Analytical techniques - colour tests andspectrophotometry, chromatography and electrophoresis, massspectrometry, and immunoassay – are covered in depth, and achapter is devoted to the analysis of trace elements and toxicmetals. General aspects of method implementation/validation andlaboratory operation are detailed, as is the role of the toxicologylaboratory in validating and monitoring the performance of point ofcare testing (POCT) devices. The book concludes with reviews ofxenobiotic absorption, distribution and metabolism,pharmacokinetics, and general aspects of the interpretation ofanalytical toxicology results. A clearly written, practical, integrated approach to the basicsof analytical toxicology. Focuses on analytical, statistical and pharmacokineticprinciples rather than detailed applications. Assumes only a basic knowledge of analytical chemistry. An accompanying website provides additional material and linksto related sites. Written by an experienced team of authors,Fundamentals ofAnalytical Toxicology is an invaluable resource for thosestarting out in a career in analytical toxicology across a widerange of disciplines including clinical and forensic science, foodsafety, and pharmaceutical development. Praise from the reviews: “This is an ambitious effort to describe in detail themany and varied aspects of the science of toxicological analysis.The 17 chapters cover every foreseeable aspect, from specimencollection through analytical techniques and quality control topharmacological principles and interpretation of results. Theauthors bring together a great deal of experience in the field andhave succeeded admirably in achieving their goal: "to giveprinciples and practical information on the analysis of drugs,poisons and other relevant analytes in biological specimens...".The book is very readable and quite up-to-date, and contains manyillustrative figures, charts and tables. Both the student and thepracticing professional would do well to study this materialcarefully, as there is something here for every conceivable levelof interest.” Review from RandallBaselt "This text comes highly recommended for any analyticaltoxicology trainee." The Bulletin of the Royal College ofPathologists “Overall, this book provides a comprehensive, thorough,clear, up to date and practical treatment of analytical toxicologyat a high standard. Understanding of the text is enhanced bythe use of many illustrations. Specifications, guidelines,and methods are highlighted in grey background“Boxes”. The many and up to date literaturereferences in each chapter demonstrate the authors’ thoroughwork and permit easy access to deeper information. Thereforethis book can be highly recommended as a valuable source ofknowledge in analytical toxicology both as an introduction and forthe advanced reader.” GTFCh Bulletin“Toxichem + Krimtech”, May 2008 (translated,original review in German) “Many toxicologists will add this important referenceto their libraries because it competently fills a need...” International Journal of Toxicology “The book is very well illustrated, easy to understandand pleasant to read, and contains a wealth of dedicatedinformation.” International Journal of EnvironmentalAnalytical Chemistry
Book Synopsis Chromatographic Methods Development by : Gregory K. Webster
Download or read book Chromatographic Methods Development written by Gregory K. Webster and published by CRC Press. This book was released on 2019-10-28 with total page 567 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is a comprehensive compilation of modern and cutting-edge chromatographic techniques written by pharmaceutical industry experts, academics, and vendors in the field. This book is an inclusive guide to developing all chromatographic methods (such as liquid chromatography and gas chromatography). It covers modern techniques for developing methods using chromatographic development software, requirements for validations, discussion on orthogonality, and how to transfer methods from HPLC to UHPLC. The text introduces some newer techniques that are heavily employed by chemists analyzing proteins and RNAi, as well as novel techniques such as counter current chromatography. This book is valuable for both the novice starting out in undergraduate labs and those who are new to the pharmaceutical industry and is a useful reference for seasoned analysts.
