Microscopic X Ray Fluorescence Analysis

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Microscopic X-Ray Fluorescence Analysis

Author : Koen H. A. Janssens
Publisher :
ISBN 13 :
Total Pages : 454 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Microscopic X-Ray Fluorescence Analysis by : Koen H. A. Janssens

Download or read book Microscopic X-Ray Fluorescence Analysis written by Koen H. A. Janssens and published by . This book was released on 2000-06-15 with total page 454 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microscopic X-ray Fluorescence Analysis Edited by Koen H. A. Janssens, Freddy C. V. Adams Department of Chemistry, University of Antwerp, Belgium and Anders Rindby Department of Physics, Chalmers University of Technology, Göteborg, Sweden In the last 10-15 years many analytical advances in X-ray fluorescence analysis (XRF) have taken place, giving rise to non-destructive ultrasensitive surface analyses of materials. One of the variants of XRF developed is micro-XRF (μ-XRF), which is able to analyse the distribution of major, minor and trace elements in microscopic sample surface areas. Due to the availability of commercial instrumentation and the development of simple devices for focusing X-rays, μ-XRF has increased in popularity and is able to fill the gap between bulk X-ray fluorescence and electron probe X-ray microanalysis (EPXMA). Microscopic X-ray Fluorescence Analysis is the first single volume to bring together introductory and advanced information on the essential aspects of the technique, thereby providing an excellent overview of the developments and applications of μ-XRF. Topics discussed in the book include: * Interaction of X-rays with matter * Micro-focusing X-ray optics * Instrumentation for μ-XRF with laboratory and synchrotron sources * Evaluation and calibration of μ-XRF data * Comparison of μ-XRF to other microanalytical techniques. In addition, the final chapters of the book describe applications of μ-XRF in the geosciences, in art and archaeology, environmental and biological applications, and the use of μ-XRF for industrial purposes. Finally an overview is presented of some of the new directions both laboratory and synchrotron μ-XRF are likely to take in the 21st Century.

Handbook of Practical X-Ray Fluorescence Analysis

Author : Burkhard Beckhoff
Publisher : Springer Science & Business Media
ISBN 13 : 3540367225
Total Pages : 897 pages
Book Rating : 4.5/5 (43 download)

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Book Synopsis Handbook of Practical X-Ray Fluorescence Analysis by : Burkhard Beckhoff

Download or read book Handbook of Practical X-Ray Fluorescence Analysis written by Burkhard Beckhoff and published by Springer Science & Business Media. This book was released on 2007-05-18 with total page 897 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-Ray fluorescence analysis is an established technique for non-destructive elemental materials analysis. This book gives a user-oriented practical guidance to the application of this method. The book gives a survey of the theoretical fundamentals, analytical instrumentation, software for data processing, various excitation regimes including gracing incidents and microfocus measurements, quantitative analysis, applications in routine and micro analysis, mineralogy, biology, medicine, criminal investigations, archeology, metallurgy, abrasion, microelectronics, environmental air and water analysis. This book is the bible of X-Ray fluorescence analysis. It gives the basic knowledge on this technique, information on analytical equipment and guides the reader to the various applications. It appeals to researchers, analytically active engineers and advanced students.

Laboratory Micro-X-Ray Fluorescence Spectroscopy

Author : Michael Haschke
Publisher : Springer Science & Business Media
ISBN 13 : 3319048643
Total Pages : 356 pages
Book Rating : 4.3/5 (19 download)

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Book Synopsis Laboratory Micro-X-Ray Fluorescence Spectroscopy by : Michael Haschke

Download or read book Laboratory Micro-X-Ray Fluorescence Spectroscopy written by Michael Haschke and published by Springer Science & Business Media. This book was released on 2014-05-08 with total page 356 pages. Available in PDF, EPUB and Kindle. Book excerpt: Micro-X-ray fluorescence offers the possibility for a position- sensitive and non-destructive analysis that can be used for the analysis of non-homogeneous materials and layer systems. This analytical technique has shown a dynamic development in the last 15 years and is used for the analysis of small particles, inclusions, of elemental distributions for a wide range of different applications both in research and quality control. The first experiments were performed on synchrotrons but there is a requirement for laboratory instruments which offers a fast and immediate access for analytical results. The book discuss the main components of a μ-XRF instrument and the different measurement modes, it gives an overview about the various instruments types, considers the special requirements for quantification of non-homogeneous materials and presents a wide range of application for single point and multi-point analysis as well as for distribution analysis in one, two and three dimensions.

Materials Characterization

Author : Yang Leng
Publisher : John Wiley & Sons
ISBN 13 : 0470822996
Total Pages : 384 pages
Book Rating : 4.4/5 (78 download)

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Book Synopsis Materials Characterization by : Yang Leng

Download or read book Materials Characterization written by Yang Leng and published by John Wiley & Sons. This book was released on 2009-03-04 with total page 384 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers state-of-the-art techniques commonly used in modern materials characterization. Two important aspects of characterization, materials structures and chemical analysis, are included. Widely used techniques, such as metallography (light microscopy), X-ray diffraction, transmission and scanning electron microscopy, are described. In addition, the book introduces advanced techniques, including scanning probe microscopy. The second half of the book accordingly presents techniques such as X-ray energy dispersive spectroscopy (commonly equipped in the scanning electron microscope), fluorescence X-ray spectroscopy, and popular surface analysis techniques (XPS and SIMS). Finally, vibrational spectroscopy (FTIR and Raman) and thermal analysis are also covered.

Archaeological Soil and Sediment Micromorphology

Author : Cristiano Nicosia
Publisher : John Wiley & Sons
ISBN 13 : 1118941071
Total Pages : 496 pages
Book Rating : 4.1/5 (189 download)

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Book Synopsis Archaeological Soil and Sediment Micromorphology by : Cristiano Nicosia

Download or read book Archaeological Soil and Sediment Micromorphology written by Cristiano Nicosia and published by John Wiley & Sons. This book was released on 2017-08-10 with total page 496 pages. Available in PDF, EPUB and Kindle. Book excerpt: Archaeological Soil and Sediment Micromorphology goes beyond a mere review of current literature and features the most up to date contributions from numerous scientists working in the field. The book represents a groundbreaking and comprehensive resource covering the plethora of applications of micromorphology in archaeology. Archaeological Soil and Sediment Micromorphology offers researchers, students and professionals a systematic tool for the interpretation of thin sections of archaeological contexts. This important resource is also designed to help stimulate the use of micromorphology in archaeology outside Europe, where the technique is less frequently employed. Moreover, the authors hope to strengthen the proper application of soil micromorphology in archaeology, by illustrating its possibilities and referring in several cases to more specialized publications (for instance in the field of plant remains, pottery and phytoliths). Written for anyone interested in the topic, this important text offers: Contributions from most of the world's leading authorities on soil micromorphology A series of chapters on the major topics selected among the most recurrent in literature about archaeological soil micromorphology Systematic descriptions of all important micromorphological features Special analytical tools employed on thin sections, such as SEM/EDS, image analysis, fluorescence microscopy, mass spectrometry, among others Numerous cross-references 400 illustrated full-colour plates The resource provides the most current and essential information for archaeologists, geoarchaeologists, soil scientists and sedimentologists. Comprehensive in scope, Archaeological Soil and Sediment Micromorphology offers professionals and students a much-needed tool for the interpretation of thin sections of archaeological contexts.

Energy Dispersive X-ray Analysis in the Electron Microscope

Author : DC Bell
Publisher : Garland Science
ISBN 13 : 1135331391
Total Pages : 270 pages
Book Rating : 4.1/5 (353 download)

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Book Synopsis Energy Dispersive X-ray Analysis in the Electron Microscope by : DC Bell

Download or read book Energy Dispersive X-ray Analysis in the Electron Microscope written by DC Bell and published by Garland Science. This book was released on 2003-07-10 with total page 270 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides an in-depth description of x-ray microanalysis in the electron microscope. It is sufficiently detailed to ensure that novices will understand the nuances of high-quality EDX analysis. Includes information about hardware design as well as the physics of x-ray generation, absorption and detection, and most post-detection data processing. Details on electron optics and electron probe formation allow the novice to make sensible adjustments to the electron microscope in order to set up a system which optimises analysis. It also helps the reader determine which microanalytical method is more suitable for their planned application.

X-Ray Fluorescence in Biological Sciences

Author : Vivek K. Singh
Publisher : John Wiley & Sons
ISBN 13 : 1119645581
Total Pages : 692 pages
Book Rating : 4.1/5 (196 download)

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Book Synopsis X-Ray Fluorescence in Biological Sciences by : Vivek K. Singh

Download or read book X-Ray Fluorescence in Biological Sciences written by Vivek K. Singh and published by John Wiley & Sons. This book was released on 2022-04-11 with total page 692 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-Ray Fluorescence in Biological Sciences Discover a comprehensive exploration of X-ray fluorescence in chemical biology and the clinical and plant sciences In X-Ray Fluorescence in Biological Sciences: Principles, Instrumentation, and Applications, a team of accomplished researchers delivers extensive coverage of the application of X-ray fluorescence (XRF) in the biological sciences, including chemical biology, clinical science, and plant science. The book also explores recent advances in XRF imaging techniques in these fields. The authors focus on understanding and investigating the intercellular structures and metals in plant cells, with advanced discussions of recently developed micro-analytical methods, like energy dispersive X-ray fluorescence spectrometry (EDXRF), total reflection X-ray fluorescence spectrometry (TXRF), micro-proton induced X-ray emission (micro-PIXE), electron probe X-ray microanalysis (EPXMA), synchrotron-based X-ray fluorescence microscopy (SXRF, SRIXE, or micro-XRF) and secondary ion mass spectrometry (SIMS). With thorough descriptions of protocols and practical approaches, the book also includes: A thorough introduction to the historical background and fundamentals of X-ray fluorescence, as well as recent developments in X-ray fluorescence analysis Comprehensive explorations of the general properties, production, and detection of X-rays and the preparation of samples for X-ray fluorescence analysis Practical discussions of the quantification of prepared samples observed under X-ray fluorescence and the relation between precision and beam size and sample amount In-depth examinations of wavelength-dispersive X-ray fluorescence and living materials Perfect for students and researchers studying the natural and chemical sciences, medical biology, plant physiology, agriculture, and botany, X-Ray Fluorescence in Biological Sciences: Principles, Instrumentation, and Applications will also earn a place in the libraries of researchers at biotechnology companies.

X-Ray Fluorescence Spectroscopy for Laboratory Applications

Author : Michael Haschke
Publisher : John Wiley & Sons
ISBN 13 : 3527344632
Total Pages : 496 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis X-Ray Fluorescence Spectroscopy for Laboratory Applications by : Michael Haschke

Download or read book X-Ray Fluorescence Spectroscopy for Laboratory Applications written by Michael Haschke and published by John Wiley & Sons. This book was released on 2021-04-05 with total page 496 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides comprehensive coverage on using X-ray fluorescence for laboratory applications This book focuses on the practical aspects of X-ray fluorescence (XRF) spectroscopy and discusses the requirements for a successful sample analysis, such as sample preparation, measurement techniques and calibration, as well as the quality of the analysis results. X-Ray Fluorescence Spectroscopy for Laboratory Applications begins with a short overview of the physical fundamentals of the generation of X-rays and their interaction with the sample material, followed by a presentation of the different methods of sample preparation in dependence on the quality of the source material and the objective of the measurement. After a short description of the different available equipment types and their respective performance, the book provides in-depth information on the choice of the optimal measurement conditions and the processing of the measurement results. It covers instrument types for XRF; acquisition and evaluation of X-Ray spectra; analytical errors; analysis of homogeneous materials, powders, and liquids; special applications of XRF; process control and automation. An important resource for the analytical chemist, providing concrete guidelines and support for everyday analyses Focuses on daily laboratory work with commercially available devices Offers a unique compilation of knowledge and best practices from equipment manufacturers and users Covers the entire work process: sample preparation, the actual measurement, data processing, assessment of uncertainty, and accuracy of the obtained results X-Ray Fluorescence Spectroscopy for Laboratory Applications appeals to analytical chemists, analytical laboratories, materials scientists, environmental chemists, chemical engineers, biotechnologists, and pharma engineers.

Total-Reflection X-Ray Fluorescence Analysis and Related Methods

Author : Reinhold Klockenkämper
Publisher : John Wiley & Sons
ISBN 13 : 1118460278
Total Pages : 554 pages
Book Rating : 4.1/5 (184 download)

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Book Synopsis Total-Reflection X-Ray Fluorescence Analysis and Related Methods by : Reinhold Klockenkämper

Download or read book Total-Reflection X-Ray Fluorescence Analysis and Related Methods written by Reinhold Klockenkämper and published by John Wiley & Sons. This book was released on 2015-01-27 with total page 554 pages. Available in PDF, EPUB and Kindle. Book excerpt: Explores the uses of TXRF in micro- and trace analysis, and in surface- and near-surface-layer analysis • Pinpoints new applications of TRXF in different fields of biology, biomonitoring, material and life sciences, medicine, toxicology, forensics, art history, and archaeometry • Updated and detailed sections on sample preparation taking into account nano- and picoliter techniques • Offers helpful tips on performing analyses, including sample preparations, and spectra recording and interpretation • Includes some 700 references for further study

Advanced Scanning Electron Microscopy and X-Ray Microanalysis

Author : Patrick Echlin
Publisher : Springer Science & Business Media
ISBN 13 : 1475790279
Total Pages : 454 pages
Book Rating : 4.4/5 (757 download)

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Book Synopsis Advanced Scanning Electron Microscopy and X-Ray Microanalysis by : Patrick Echlin

Download or read book Advanced Scanning Electron Microscopy and X-Ray Microanalysis written by Patrick Echlin and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 454 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book has its origins in the intensive short courses on scanning elec tron microscopy and x-ray microanalysis which have been taught annually at Lehigh University since 1972. In order to provide a textbook containing the materials presented in the original course, the lecturers collaborated to write the book Practical Scanning Electron Microscopy (PSEM), which was published by Plenum Press in 1975. The course con tinued to evolve and expand in the ensuing years, until the volume of material to be covered necessitated the development of separate intro ductory and advanced courses. In 1981 the lecturers undertook the project of rewriting the original textbook, producing the volume Scan ning Electron Microscopy and X-Ray Microanalysis (SEMXM). This vol ume contained substantial expansions of the treatment of such basic material as electron optics, image formation, energy-dispersive x-ray spectrometry, and qualitative and quantitative analysis. At the same time, a number of chapters, which had been included in the PSEM vol ume, including those on magnetic contrast and electron channeling con trast, had to be dropped for reasons of space. Moreover, these topics had naturally evolved into the basis of the advanced course. In addition, the evolution of the SEM and microanalysis fields had resulted in the devel opment of new topics, such as digital image processing, which by their nature became topics in the advanced course.

Synchrotron Radiation Research

Author : Herman Winick
Publisher : Springer Science & Business Media
ISBN 13 : 1461579988
Total Pages : 767 pages
Book Rating : 4.4/5 (615 download)

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Book Synopsis Synchrotron Radiation Research by : Herman Winick

Download or read book Synchrotron Radiation Research written by Herman Winick and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 767 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book has grown out of our shared experience in the development of the Stanford Synchrotron Radiation Laboratory (SSRL), based on the electron-positron storage ring SPEAR at the Stanford Linear Accelerator Center (SLAC) starting in Summer, 1973. The immense potential of the photon beam from SPEAR became obvious as soon as experiments using the beam started to run in May, 1974. The rapid growth of interest in using the beam since that time and the growth of other facilities using high-energy storage rings (see Chapters 1 and 3) demonstrates how the users of this source of radiation are finding applications in an increasingly wide variety of fields of science and technology. In assembling the list of authors for this book, we have tried to cover as many of the applications of synchrotron radiation, both realized already or in the process of realization, as we can. Inevitably, there are omissions both through lack of space and because many projects are at an early stage. We thank the authors for their efforts and cooperation in producing what we believe is the most comprehensive treatment of synchrotron radiation research to date.

Chemical Imaging Analysis

Author : Freddy Adams
Publisher : Elsevier
ISBN 13 : 0444634509
Total Pages : 480 pages
Book Rating : 4.4/5 (446 download)

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Book Synopsis Chemical Imaging Analysis by : Freddy Adams

Download or read book Chemical Imaging Analysis written by Freddy Adams and published by Elsevier. This book was released on 2015-06-06 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemical Imaging Analysis covers the advancements made over the last 50 years in chemical imaging analysis, including different analytical techniques and the ways they were developed and refined to link the composition and structure of manmade and natural materials at the nano/micro scale to the functional behavior at the macroscopic scale. In a development process that started in the early 1960s, a variety of specialized analytical techniques was developed – or adapted from existing techniques – and these techniques have matured into versatile and powerful tools for visualizing structural and compositional heterogeneity. This text explores that journey, providing a general overview of imaging techniques in diverse fields, including mass spectrometry, optical spectrometry including X-rays, electron microscopy, and beam techniques. Provides comprehensive coverage of analytical techniques used in chemical imaging analysis Explores a variety of specialized techniques Provides a general overview of imaging techniques in diverse fields

X-Ray Optics and X-Ray Microanalysis

Author : H. H. Pattee
Publisher : Elsevier
ISBN 13 : 1483277038
Total Pages : 640 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis X-Ray Optics and X-Ray Microanalysis by : H. H. Pattee

Download or read book X-Ray Optics and X-Ray Microanalysis written by H. H. Pattee and published by Elsevier. This book was released on 2013-10-22 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-ray Optics and X-ray Microanalysis covers the proceedings of the Symposium on X-ray Optics and X-ray Microanalysis, held at Stanford University on August 22-24, 1962. The book focuses on X-ray microscopy, microradiography, radiation and irradiation, and X-ray microanalysis. The selection first offers information on the methods of X-ray microscopy and X-ray absorption microanalysis. Discussions focus on X-ray scanning microscopy, contact microradiography, point projection microscopy, and total dry-weight determinations. The text then takes a look at X-ray microanalysis in biology and medicine; electron microscopic enlargements of X-ray absorption micrographs; and automation in microradiography. The publication examines the production of Fresnel zone plates for extreme ultraviolet and soft X radiation; quantitative microradiographic studies of human epidermis; and irradiation effect on total organic nerve-cell material determined by integrating X-ray absorption. The manuscript then reviews the calculation of fluorescence excited by characteristic radiation in the X-ray microanalyzer and the method for calculating the absorption correction in electron-probe microanalysis. The selection is a valuable reference for readers interested in X-ray technology.

Quantitative X-Ray Fluorescence Analysis

Author : Gerald R. Lachance
Publisher :
ISBN 13 :
Total Pages : 432 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Quantitative X-Ray Fluorescence Analysis by : Gerald R. Lachance

Download or read book Quantitative X-Ray Fluorescence Analysis written by Gerald R. Lachance and published by . This book was released on 1995-01-31 with total page 432 pages. Available in PDF, EPUB and Kindle. Book excerpt: A systematic account concerning the basic theory of X-ray physics and spectrometer configurations leading to simple expressions quantifying primary and secondary fluorescence emissions. Discusses the fundamental parameters approach for converting intensities to concentrations in both its classical formalism and by a number of basic influence coefficient algorithms. Examines approximations underlying influence coefficient models and theoretical simulations are used to evaluate global methods. Includes numerous detailed examples as well as extensive tabulations of theoretical data.

Principles of Analytical Electron Microscopy

Author : Joseph Goldstein
Publisher : Springer Science & Business Media
ISBN 13 : 1489920374
Total Pages : 458 pages
Book Rating : 4.4/5 (899 download)

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Book Synopsis Principles of Analytical Electron Microscopy by : Joseph Goldstein

Download or read book Principles of Analytical Electron Microscopy written by Joseph Goldstein and published by Springer Science & Business Media. This book was released on 2013-11-11 with total page 458 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the publication in 1979 of Introduction to Analytical Electron Microscopy (ed. J. J. Hren, J. I. Goldstein, and D. C. Joy; Plenum Press), analytical electron microscopy has continued to evolve and mature both as a topic for fundamental scientific investigation and as a tool for inorganic and organic materials characterization. Significant strides have been made in our understanding of image formation, electron diffraction, and beam/specimen interactions, both in terms of the "physics of the processes" and their practical implementation in modern instruments. It is the intent of the editors and authors of the current text, Principles of Analytical Electron Microscopy, to bring together, in one concise and readily accessible volume, these recent advances in the subject. The text begins with a thorough discussion of fundamentals to lay a foundation for today's state-of-the-art microscopy. All currently important areas in analytical electron microscopy-including electron optics, electron beam/specimen interactions, image formation, x-ray microanalysis, energy-loss spectroscopy, electron diffraction and specimen effects-have been given thorough attention. To increase the utility of the volume to a broader cross section of the scientific community, the book's approach is, in general, more descriptive than mathematical. In some areas, however, mathematical concepts are dealt with in depth, increasing the appeal to those seeking a more rigorous treatment of the subject.

X-ray and Image Analysis in Electron Microscopy

Author : John J. Friel
Publisher :
ISBN 13 : 9783864606748
Total Pages : 118 pages
Book Rating : 4.6/5 (67 download)

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Book Synopsis X-ray and Image Analysis in Electron Microscopy by : John J. Friel

Download or read book X-ray and Image Analysis in Electron Microscopy written by John J. Friel and published by . This book was released on 2017-04-18 with total page 118 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Handbook of Sample Preparation for Scanning Electron Microscopy and X-Ray Microanalysis

Author : Patrick Echlin
Publisher : Springer Science & Business Media
ISBN 13 : 0387857311
Total Pages : 329 pages
Book Rating : 4.3/5 (878 download)

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Book Synopsis Handbook of Sample Preparation for Scanning Electron Microscopy and X-Ray Microanalysis by : Patrick Echlin

Download or read book Handbook of Sample Preparation for Scanning Electron Microscopy and X-Ray Microanalysis written by Patrick Echlin and published by Springer Science & Business Media. This book was released on 2011-04-14 with total page 329 pages. Available in PDF, EPUB and Kindle. Book excerpt: Scanning electr on microscopy (SEM) and x-ray microanalysis can produce magnified images and in situ chemical information from virtually any type of specimen. The two instruments generally operate in a high vacuum and a very dry environment in order to produce the high energy beam of electrons needed for imaging and analysis. With a few notable exceptions, most specimens destined for study in the SEM are poor conductors and composed of beam sensitive light elements containing variable amounts of water. In the SEM, the imaging system depends on the specimen being sufficiently electrically conductive to ensure that the bulk of the incoming electrons go to ground. The formation of the image depends on collecting the different signals that are scattered as a consequence of the high energy beam interacting with the sample. Backscattered electrons and secondary electrons are generated within the primary beam-sample interactive volume and are the two principal signals used to form images. The backscattered electron coefficient ( ? ) increases with increasing atomic number of the specimen, whereas the secondary electron coefficient ( ? ) is relatively insensitive to atomic number. This fundamental diff- ence in the two signals can have an important effect on the way samples may need to be prepared. The analytical system depends on collecting the x-ray photons that are generated within the sample as a consequence of interaction with the same high energy beam of primary electrons used to produce images.