Gold Catalyzed Asymmetric Synthesis Of Cyclic Ethers And Copper Catalyzed Hydrofunctionalization Of Alkynes

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Gold-catalyzed Asymmetric Synthesis of Cyclic Ethers and Copper-catalyzed Hydrofunctionalization of Alkynes

Author : Mycah R. Uehling
Publisher :
ISBN 13 :
Total Pages : 169 pages
Book Rating : 4.:/5 (932 download)

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Book Synopsis Gold-catalyzed Asymmetric Synthesis of Cyclic Ethers and Copper-catalyzed Hydrofunctionalization of Alkynes by : Mycah R. Uehling

Download or read book Gold-catalyzed Asymmetric Synthesis of Cyclic Ethers and Copper-catalyzed Hydrofunctionalization of Alkynes written by Mycah R. Uehling and published by . This book was released on 2015 with total page 169 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gold-catalyzed cyclization of enantioenriched trisubstituted allenols to form enantioenriched [unknown scientific symbol]-tetrasubstituted cyclic ethers has been developed. This structural motif can be found in many natural products that have useful biological properties. The cyclization reaction is compatible with multiple functional groups and can be used to prepare enantioenriched furans, pyrans, and chromans all containing an [unknown scientific symbol]-tetrasubstituted stereocenter. The reaction development, scope, and a preliminary mechanistic study are discussed. In addition, a method to synthesize the required enantioenriched trisubstituted allenols based on copper-catalyzed cross coupling of enantioenriched propargylic phosphates and organoboron reagents has been developed. This allows the overall sequence to be practical and convergent. Copper-catalyzed hydrobromination and hydroalkylation of alkynes have been developed. The reactions are compatible with many functional groups and can be used to prepare functionalized alkenes in high yield and as one regio- and diastereoisomer. The reaction development, scope, and preliminary mechanism studies are discussed for both reactions. The development of copper-catalyzed hydrobromination and hydroalkylation of alkynes demonstrates that copper-catalyzed hydrofunctionalization of alkynes is a general approach to the synthesis of different types of functionalized alkenes.

Copper-Catalyzed Asymmetric Synthesis

Author : Alexandre Alexakis
Publisher : John Wiley & Sons
ISBN 13 : 3527664599
Total Pages : 467 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Copper-Catalyzed Asymmetric Synthesis by : Alexandre Alexakis

Download or read book Copper-Catalyzed Asymmetric Synthesis written by Alexandre Alexakis and published by John Wiley & Sons. This book was released on 2013-12-30 with total page 467 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book reflects the increasing interest among the chemical synthetic community in the area of asymmetric copper-catalyzed reactions, and introduces readers to the latest, most significant developments in the field. The contents are organized according to reaction type and cover mechanistic and spectroscopic aspects as well as applications in the synthesis of natural products. A whole chapter is devoted to understanding how primary organometallics interact with copper to provide selective catalysts for allylic substitution and conjugate addition, both of which are treated in separate chapters. Another is devoted to the variety of substrates and experimental protocols, while an entire chapter covers the use on non-carbon nucleophiles. Other chapters deal with less-known reactions, such as carbometallation or the additions to imines and related systems, while the more established reactions cyclopropanation and aziridination as well as the use of copper (II) Lewis acids are warranted their own special chapters. Two further chapters concern the processes involved, as determined by mechanistic studies. Finally, a whole chapter is devoted to the synthetic applications. This is essential reading for researchers at academic institutions and professionals at pharmaceutical or agrochemical companies.

Development of Practical Synthetic Tools Using Copper and Gold Catalysis

Author : Nick Cox
Publisher :
ISBN 13 :
Total Pages : 126 pages
Book Rating : 4.:/5 (882 download)

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Book Synopsis Development of Practical Synthetic Tools Using Copper and Gold Catalysis by : Nick Cox

Download or read book Development of Practical Synthetic Tools Using Copper and Gold Catalysis written by Nick Cox and published by . This book was released on 2013 with total page 126 pages. Available in PDF, EPUB and Kindle. Book excerpt: The use of transition metal catalysis in the synthesis of complex organic molecules has dramatically expanded the role of synthetic chemistry across a broad spectrum of applications including drug discovery, chemical biology, and materials science. This is due in large part to the development of practical, transition-metal-catalyzed techniques for: 1) the construction of synthetically challenging molecular structures and 2) the selective activation of strong bonds. Our contribution in the first area has focused on the functionalization of C-C multiple bonds using copper and gold catalysts. I will begin by discussing the development of a convenient method for the asymmetric synthesis of cyclic ethers containing highly-substituted stereocenters: complex structures which are found in a wide variety of natural products. Our efforts in the second area have been directed at C-O bond activation using copper catalysts. I will describe our investigation of the copper-catalyzed reduction of alkyl triflates, and how this technique was applied in a new approach to the selective deoxygenation of primary alcohols that offers significant advantages over traditional methods. Finally, I will present an extension of this strategy to the copper-catalyzed reduction of primary and secondary halides which proceeds through a non-radical mechanism.

Copper Catalysis in Organic Synthesis

Author : Gopinathan Anilkumar
Publisher : John Wiley & Sons
ISBN 13 : 3527347372
Total Pages : 504 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Copper Catalysis in Organic Synthesis by : Gopinathan Anilkumar

Download or read book Copper Catalysis in Organic Synthesis written by Gopinathan Anilkumar and published by John Wiley & Sons. This book was released on 2020-12-07 with total page 504 pages. Available in PDF, EPUB and Kindle. Book excerpt: The most current information on growing field of copper catalysis Copper Catalysis in Organic Synthesis contains an up-to-date overview of the most important reactions in the presence of copper catalysts. The contributors—noted experts on the topic—provide an introduction to the field of copper catalysis, reviewing its development, scope, and limitations, as well as providing descriptions of various homo- and cross-coupling reactions. In addition, information is presented on copper-catalyzed C–H activation, amination, carbonylation, trifluoromethylation, cyanation, and click reactions. Comprehensive in scope, the book also describes microwave-assisted and multi-component transformations as well as copper-catalyzed reactions in green solvents and continuous flow reactors. The authors highlight the application of copper catalysis in asymmetric synthesis and total synthesis of natural products and heterocycles as well as nanocatalysis. This important book: Examines copper and its use in organic synthesis as a more cost-effective and sustainable for researchers in academia and industry Offers the first up-to-date book to explore copper as a first line catalyst for many organic reactions Presents the most significant developments in the area, including cross-coupling reactions, C–H activation, asymmetric synthesis, and total synthesis of natural products and heterocycles Contains over 20 contributions from leaders in the field Written for catalytic chemists, organic chemists, natural products chemists, pharmaceutical chemists, and chemists in industry, Copper Catalysis in Organic Synthesis offers a book on the growing field of copper catalysis, covering cross-coupling reactions, C–H activation, and applications in the total synthesis of natural products.

Copper-catalyzed Synthesis of Cyclic Ethers and Applications to the Synthesis of Varitriol and Goniothalesdiol

Author : Lindsay Ann Batory
Publisher :
ISBN 13 :
Total Pages : 292 pages
Book Rating : 4.:/5 (433 download)

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Book Synopsis Copper-catalyzed Synthesis of Cyclic Ethers and Applications to the Synthesis of Varitriol and Goniothalesdiol by : Lindsay Ann Batory

Download or read book Copper-catalyzed Synthesis of Cyclic Ethers and Applications to the Synthesis of Varitriol and Goniothalesdiol written by Lindsay Ann Batory and published by . This book was released on 2008 with total page 292 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Modern Gold Catalyzed Synthesis

Author : A. Stephen K. Hashmi
Publisher : John Wiley & Sons
ISBN 13 : 3527319522
Total Pages : 419 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Modern Gold Catalyzed Synthesis by : A. Stephen K. Hashmi

Download or read book Modern Gold Catalyzed Synthesis written by A. Stephen K. Hashmi and published by John Wiley & Sons. This book was released on 2012-05-21 with total page 419 pages. Available in PDF, EPUB and Kindle. Book excerpt: With its impressive features, gold has led to completely new reaction types in recent years, which in turn have strongly influenced both organic catalysis and material science. Other fields where a significant amount of new results has been obtained include nanotechnology, self assembly/supramolecular systems and biochemical/medicinal chemistry. As a result, gold is one of the hottest topics in catalysis at the moment, with an increasing amount of research being carried out in this field. While focusing on homogeneous catalysis, this monograph also covers the main applications in heterogeneous catalysis. Following a look at the gold-catalyzed addition of heteroatom nucleophiles to alkynes, it goes on to discuss gold-catalyzed additions to allenes and alkenes, gold-catalyzed benzannulations, cycloisomerization and rearrangement reactions, as well as oxidation and reduction reactions. The whole is finished off with a section on gold-catalyzed aldol and related reactions and the application of gold-catalyzed reactions to natural product synthesis. Of interest to synthetic chemists and inorganic chemists, as well as organic chemists working in homogeneous catalysis, physical and technical chemists.

Gold Catalysis: An Homogeneous Approach

Author : Veronique Michelet
Publisher : World Scientific
ISBN 13 : 1783265558
Total Pages : 564 pages
Book Rating : 4.7/5 (832 download)

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Book Synopsis Gold Catalysis: An Homogeneous Approach by : Veronique Michelet

Download or read book Gold Catalysis: An Homogeneous Approach written by Veronique Michelet and published by World Scientific. This book was released on 2014-06-20 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: Research on designing new catalytic systems has been one of the most important fields in modern organic chemistry. One reason for this is the predominant contribution of catalysis to the concepts of atom economy and green chemistry in the 21st century. Gold, considered catalytically inactive for a long time, is now a fascinating partner of modern chemistry, as scientists such as Bond, Teles, Haruta, Hutchings, Ito and Hayashi opened new perspectives for the whole synthetic chemist community. This book presents the major advances in homogeneous catalysis, emphasizing the methodologies that create carbon-carbon and carbon-heteroatom bonds, the applications that create diversity and synthesize natural products, and the recent advances and challenges in asymmetric catalysis and computational research.It provides readers with in-depth information about homogeneous gold-catalyzed reactions and presents several explanations for the scientific design of a catalyst. Readers will be able to understand the entire gold area and find solutions to problems in catalysis.Gold Catalysis — An Homogeneous Approach is part of the Catalytic Science Series and features prominent authors who are experts in their respective fields.

New Gold-Catalyzed Reactions and Applications for the Synthesis of Alkaloids

Author : Ana Escribano Cuesta
Publisher : Springer Science & Business Media
ISBN 13 : 3319007025
Total Pages : 202 pages
Book Rating : 4.3/5 (19 download)

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Book Synopsis New Gold-Catalyzed Reactions and Applications for the Synthesis of Alkaloids by : Ana Escribano Cuesta

Download or read book New Gold-Catalyzed Reactions and Applications for the Synthesis of Alkaloids written by Ana Escribano Cuesta and published by Springer Science & Business Media. This book was released on 2013-08-13 with total page 202 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ana Escribano Cuesta's thesis presents a detailed study of the inter- and intramolecular reactions of carbonyl compounds with 1,6-enynes using gold (I) complexes. An important part of the work involved streamlining the variables that allow the selective synthesis of different products such as tricyclic compounds, dihydropyrans, 1,3-dienes or cyclobutenes. The second chapter highlights the importance and difficulties in synthesising a cyclobutene subunit and the author includes a detailed description of how the products were prepared. The final chapter outlines the synthesis of lundurines using methodology developed by the author's research group for intramolecular gold-catalyzed cyclization of indoles with alkynes. The lundurine products developed in this work show significant in vitro cytoxicity toward B16 melanoma cells. The work in this thesis has led to a number of publications in high-profile chemistry journals.

Homogeneous Gold Catalysis

Author : LeGrande M. Slaughter
Publisher : Springer
ISBN 13 : 3319137220
Total Pages : 292 pages
Book Rating : 4.3/5 (191 download)

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Book Synopsis Homogeneous Gold Catalysis by : LeGrande M. Slaughter

Download or read book Homogeneous Gold Catalysis written by LeGrande M. Slaughter and published by Springer. This book was released on 2015-03-30 with total page 292 pages. Available in PDF, EPUB and Kindle. Book excerpt: The series Topics in Current Chemistry presents critical reviews of the present and future trends in modern chemical research. The scope of coverage is all areas of chemical science including the interfaces with related disciplines such as biology, medicine and materials science. The goal of each thematic volume is to give the non-specialist reader, whether in academia or industry, a comprehensive insight into an area where new research is emerging which is of interest to a larger scientific audience. Each review within the volume critically surveys one aspect of that topic and places it within the context of the volume as a whole. The most significant developments of the last 5 to 10 years are presented using selected examples to illustrate the principles discussed. The coverage is not intended to be an exhaustive summary of the field or include large quantities of data, but should rather be conceptual, concentrating on the methodological thinking that will allow the non-specialist reader to understand the information presented. Contributions also offer an outlook on potential future developments in the field. Review articles for the individual volumes are invited by the volume editors. Readership: research chemists at universities or in industry, graduate students.

Contemporary Boron Chemistry

Author : Matthew G Davidson
Publisher : Royal Society of Chemistry
ISBN 13 : 1847550649
Total Pages : 555 pages
Book Rating : 4.8/5 (475 download)

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Book Synopsis Contemporary Boron Chemistry by : Matthew G Davidson

Download or read book Contemporary Boron Chemistry written by Matthew G Davidson and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 555 pages. Available in PDF, EPUB and Kindle. Book excerpt: The continued and evolving significance of boron chemistry to the wider chemical community is demonstrated by the international and interdisciplinary nature of the research reported in this book. Contemporary Boron Chemistry encompasses inorganic and organic compounds as well as polymers, solid-state materials, medicinal aspects and theoretical studies. Covering many areas of chemistry with boron at its centre, topics include applications to polyolefin catalysis, medicine, materials and polymers; boron cluster chemistry, including carboranes and metal-containing clusters; organic and inorganic chemistry of species containing only 1 or 2 boron atoms; and theoretical studies of boron-containing compounds. New materials with novel optical and electronic properties are also discussed. Comprehensive and up to date, graduates and researchers in a wide range of fields, particularly those in organometallic and organic chemistry and materials science, will welcome this book.

Organic Reaction Mechanisms 2016

Author : A. C. Knipe
Publisher : John Wiley & Sons
ISBN 13 : 1119288738
Total Pages : 872 pages
Book Rating : 4.1/5 (192 download)

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Book Synopsis Organic Reaction Mechanisms 2016 by : A. C. Knipe

Download or read book Organic Reaction Mechanisms 2016 written by A. C. Knipe and published by John Wiley & Sons. This book was released on 2019-12-30 with total page 872 pages. Available in PDF, EPUB and Kindle. Book excerpt: Organic Reaction Mechanisms 2016, the 52nd annual volume in this highly successful and unique series, surveys research on organic reaction mechanisms described in the available literature dated 2016. The following classes of organic reaction mechanisms are comprehensively reviewed: • Reaction of Aldehydes and Ketones and their Derivatives • Reactions of Carboxylic, Phosphoric, and Sulfonic Acids and their Derivatives • Oxidation and Reduction • Carbenes and Nitrenes • Nucleophilic Aromatic Substitution • Electrophilic Aromatic Substitution • Carbocations • Nucleophilic Aliphatic Substitution • Carbanions and Electrophilic Aliphatic Substitution • Elimination Reactions • Polar Addition Reactions • Cycloaddition Reactions • Molecular Rearrangements

Chiral Ferrocenes in Asymmetric Catalysis

Author : Li-Xin Dai
Publisher : John Wiley & Sons
ISBN 13 : 3527322809
Total Pages : 433 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Chiral Ferrocenes in Asymmetric Catalysis by : Li-Xin Dai

Download or read book Chiral Ferrocenes in Asymmetric Catalysis written by Li-Xin Dai and published by John Wiley & Sons. This book was released on 2010-02-01 with total page 433 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book meets the long-felt need for a reference on ferrocenes with the focus on catalysis. It provides a thorough overview of the synthesis and characterization of different types of chiral ferrocene ligands, their application to various catalytic asymmetric reactions, and versatile chiral materials as well as drug intermediates synthesized from them. Written by the "who's who" of ferrocene catalysis, this is a guide to the design of new ferrocene ligands and synthesis of chiral synthetic intermediates, and will thus be useful for organic, catalytic and synthetic chemists working in academia, industrial research or process development.

Gold Catalysis

Author : F. Dean Toste
Publisher :
ISBN 13 : 9781848168534
Total Pages : 564 pages
Book Rating : 4.1/5 (685 download)

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Book Synopsis Gold Catalysis by : F. Dean Toste

Download or read book Gold Catalysis written by F. Dean Toste and published by . This book was released on 2014-08-01 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: Research on designing new catalytic systems has been one of the most important fields in modern organic chemistry, and one reason for this is the predominant contribution of catalysis to the concepts of atom economy and green chemistry in the 21st century. Gold, considered catalytically inactive for a long time, is now a fascinating partner of modern chemistry, as scientists such as Bond, Haruta, Hutchings, Ito and Hayashi opened new perspectives for the whole synthetic chemist community. This book presents the major advances in homogeneous catalysis, emphasizing the methodologies that create carbon-carbon and carbon-heteroatom bonds, the applications that create diversity and synthesize natural products, and the recent advances and challenges in asymmetric catalysis and computational research. The Handbook of Homogeneous Gold Catalysis provides readers with in-depth information about gold-catalyzed reactions and presents several explanations for the scientific design of a catalyst. Readers will be able to understand the entire gold area and find solutions to problems in catalysis. Featuring prominent authors, who are experts in their respective fields, this is the first book dedicated to homogeneous gold chemistry. Contents: From Gold in Nature to Gold Catalysts (S Kramer and F Gagosz); Oxidation and Reduction Reactions (L Zhang); Gold-Catalyzed Addition of Carbon Nucleophile to C-C Multiple Bond (B Simmons and H C Shen); Gold-Catalyzed Addition of Heteroatom Nucleophile to C-C Multiple Bond (N Asao, N Hatakeyama and Y Yamamoto); Gold-Catalyzed Synthesis of Heterocycles (A Arcadi); Multi-Component Reactions (R Skouta and C J Li); Gold Catalyzed Tandem and Cascade Reactions (R-S Liu); Cycloisomerization Reactions of 1, n -Enynes (N Huguet and A Echavarren); Gold-Catalyzed Reaction of Propargylic Esters (L Fensterbank, J-P Goddard, M Malacria and S Simonneau); Gold-Catalyzed Cross-Coupling Reactions (S Blum); Gold-Catalyzed Reactions: A Computational Approach (E Soriano & J Marco-Contelles); Asymmetric Gold-Catalyzed Reactions (P Y Toullec, A Pradal and V Michelet); Gold Catalysis in Natural Product Synthesis (M Gesinski and F D Toste). Readership: Student, professionals.

Axially Chiral Compounds

Author : Bin Tan
Publisher : John Wiley & Sons
ISBN 13 : 3527347127
Total Pages : 338 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Axially Chiral Compounds by : Bin Tan

Download or read book Axially Chiral Compounds written by Bin Tan and published by John Wiley & Sons. This book was released on 2021-11-22 with total page 338 pages. Available in PDF, EPUB and Kindle. Book excerpt: Axially Chiral Compounds Explore this comprehensive and current volume summarizing the characteristics, synthesis, and applications of axial chirality Appearing widely in natural products, biologically active molecules, asymmetric chemistry, and material science, axially chiral motifs constitute the core backbones of the majority of chiral ligands and organocatalysts in asymmetric catalysis. In a new work of particular relevance to synthetic chemists, Axially Chiral Compounds: Asymmetric Synthesis and Applications delivers a clearly structured and authoritative volume covering the classification, characteristics, synthesis, and applications of axial chirality. A must read for every synthetic chemist practicing today, the book follows the development history, research status, and applications of axial chirality. An introductory chapter familiarizes the reader with foundational material before the distinguished authors describe the different classes and the synthesis of axial chiral compounds used in asymmetric synthesis. The book concludes with a focus on the applications of chiral ligands, chiral catalysts, and materials. Readers will also benefit from the inclusion of: A thorough introduction to asymmetric synthesis, including biaryls atropisomers, heterobiaryls atropisomers, and non-biaryls atropisomers Explorations of chiral allene, spiro skeletons, and natural products Practical discussions of asymmetric transformation, chiral ligands, and chiral catalysts An examination of miscellaneous applications of axially chiral compounds Perfect for organic chemists, chemists working with or on organometallics, catalytic chemists, and materials scientists, Axially Chiral Compounds: Asymmetric Synthesis and Applications will also earn a place in the libraries of natural products chemists who seek a one-stop reference for compounds exhibiting axial chirality.

Modern Alkyne Chemistry

Author : Barry M. Trost
Publisher : John Wiley & Sons
ISBN 13 : 3527677917
Total Pages : 420 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Modern Alkyne Chemistry by : Barry M. Trost

Download or read book Modern Alkyne Chemistry written by Barry M. Trost and published by John Wiley & Sons. This book was released on 2014-10-08 with total page 420 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive and up-to-date overview of alkyne chemistry, taking into account the progress made over the last two decades. The experienced editors are renowned world leaders in the field, while the list of contributors reads like a "Who's Who" of synthetic organic chemistry. The result is a valuable reference not only for organic chemists at universities and in the chemical industry, but also for biologists and material scientists involved in the modern synthesis of organic compounds and materials.

Iron Catalysis

Author : Bernd Plietker
Publisher : Springer Science & Business Media
ISBN 13 : 3642146694
Total Pages : 227 pages
Book Rating : 4.6/5 (421 download)

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Book Synopsis Iron Catalysis by : Bernd Plietker

Download or read book Iron Catalysis written by Bernd Plietker and published by Springer Science & Business Media. This book was released on 2011-01-05 with total page 227 pages. Available in PDF, EPUB and Kindle. Book excerpt: Juan I. Padrón and Víctor S. Martín: Catalysis by means of Fe-based Lewis acids; Hiroshi Nakazawa*, Masumi Itazaki: Fe–H Complexes in Catalysis; Kristin Schröder, Kathrin Junge, Bianca Bitterlich, and Matthias Beller: Fe-catalyzed Oxidation Reactions of Olefins, Alkanes and Alcohols: Involvement of Oxo- and Peroxo Complexes; Chi-Ming Che, Cong-Ying Zhou, Ella Lai-Ming Wong: Catalysis by Fe=X Complexes (X=NR, CR2); René Peters, Daniel F. Fischer and Sascha Jautze: Ferrocene and Half Sandwich Complexes as Catalysts with Iron Participation; Markus Jegelka, Bernd Plietker: Catalysis by Means of Complex Ferrates.

Acetylene Chemistry

Author : François Diederich
Publisher : John Wiley & Sons
ISBN 13 : 3527604707
Total Pages : 528 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Acetylene Chemistry by : François Diederich

Download or read book Acetylene Chemistry written by François Diederich and published by John Wiley & Sons. This book was released on 2006-03-06 with total page 528 pages. Available in PDF, EPUB and Kindle. Book excerpt: Acetylenes are an important and valuable class of compounds in organic synthesis. This book expands on this historically well-established concept, while incorporating the many new developments that have widened the number of applications in this field. It remains the only handbook available that embodies all the important facets of acetylene chemistry. Following the first section on synthesis, the leading authors deal with advanced materials before turning to the properties and theory of acetylenes, while a final section looks at the biological aspects. With its range of experimental procedures, this book is a practical aid for both organic and organometallic chemists, as well as for materials scientists, biochemists, and industrial chemists.