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Dynamics Control And Optimization Of Free Radical Solution And Emulsion Polymerization Processes
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Book Synopsis Dynamics, Control, and Optimization of Free-radical Solution and Emulsion Polymerization Processes by : Brian Marcus Louie
Download or read book Dynamics, Control, and Optimization of Free-radical Solution and Emulsion Polymerization Processes written by Brian Marcus Louie and published by . This book was released on 1984 with total page 710 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Control of Polymerization Reactors by : Joseph Schork
Download or read book Control of Polymerization Reactors written by Joseph Schork and published by Routledge. This book was released on 2017-09-20 with total page 378 pages. Available in PDF, EPUB and Kindle. Book excerpt: This reference and text provides an in-depth description of developments in control techniques and their application to polymerization reactors and offers important introductory background information on polymerization reaction engineering.;Discussing modelling, identification, linear, nonlinear and multivariable schemes, Control of Polymerization Reactors: presents all available techniques that can be used to control reactors properly for optimal performance; shows how to manipulate pivotal variables that affect reactor control; examines methods for deriving dynamic process models to improve reactor efficiency; reviews reactor control problems and points out end-use properties; supplies methods for measuring process variables, and ways to estimate variables that can't be measured; and explains how single-input, single-output (SISO) strategies can be effectively used for control.;Filled with illustrative examples to clarify concepts, including more than 730 figures, tables and equations, Control of Polymerization Reactors is intended for use as a reference for chemical, process development, process design, research and development, control systems, and polymer engineers; and polymer chemists and physicists; as well as a text for upper-level undergraduate and graduate students in polymerization reactor control courses.
Book Synopsis Dynamics and Control of Process Systems 2004 by : Sirish Shah
Download or read book Dynamics and Control of Process Systems 2004 written by Sirish Shah and published by Elsevier. This book was released on 2005-06-10 with total page 540 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Adaptive Dynamic Optimization of the Semibatch Emulsion Polymerization Process by : Mark Joseph Perri
Download or read book Adaptive Dynamic Optimization of the Semibatch Emulsion Polymerization Process written by Mark Joseph Perri and published by . This book was released on 1989 with total page 657 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Advances in Polymer Reaction Engineering by :
Download or read book Advances in Polymer Reaction Engineering written by and published by Academic Press. This book was released on 2020-10-31 with total page 350 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advances in Polymer Reaction Engineering, Volume 56 in the Advances in Chemical Engineering series is aimed at reporting the latest advances in the field of polymer synthesis. Chapters in this new release include Polymer reaction engineering and composition control in free radical copolymers, Reactor control and on-line process monitoring in free radical emulsion polymerization, Exploiting pulsed laser polymerization to retrieve intrinsic kinetic parameters in radical polymerization, 3D printing in chemical engineering, Renewable source monomers in waterborne polymer dispersions, Importance of models and digitalization in Polymer Reaction Engineering, Recent Advances in Modelling of Radical Polymerization, and more. Covers recent advances in the control and monitoring of polymerization processes and in reactor configurations Provides modelling of polymerization reactions and up-to-date approaches to estimate reaction rate constants Includes authoritative opinions from experts in academia and industry
Book Synopsis 23 European Symposium on Computer Aided Process Engineering by : Alireza Hosseini
Download or read book 23 European Symposium on Computer Aided Process Engineering written by Alireza Hosseini and published by Elsevier Inc. Chapters. This book was released on 2013-06-10 with total page 17 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this paper, a new control strategy that employs a mid-course correction to control the particle size distribution in emulsion polymerization is developed. In this approach, online and infrequent measurements are used to obtain the states of the system at the mid-course of the process. Then an optimization is performed to obtain the optimal trajectory of the input from the mid-course up to the end of the process. For this optimization, a hybrid model is used. This hybrid model consists of the Fokker-Planck particle size distribution model of emulsion polymerization and a data-driven component which corrects the predictions of the Fokker-Planck model based upon the estimated states of the system at the mid-course of the process.
Book Synopsis Emulsion-based Free-Radical Retrograde-Precipitation Polymerization by : Gerard Caneba
Download or read book Emulsion-based Free-Radical Retrograde-Precipitation Polymerization written by Gerard Caneba and published by Springer Science & Business Media. This book was released on 2011-07-02 with total page 196 pages. Available in PDF, EPUB and Kindle. Book excerpt: This monograph is a follow-up material to the first FRRPP book by Gerard Caneba in 2009. It includes additional conceptual results, implementation of the FRRPP process in emulsion media to produce various block copolymers, and other FRRPP-related supplementary topics. Conceptual topics include the application of the quantitative analysis presented in the first FRRPP monograph for the occurrence of the FRRPP process to the polysterene-styrene-ether (PS-S-Ether) and poly(methacrylic acid)-methacrylic acid-water (PMAA-MAA-Water) systems, as well as extensions through unsteady state analysis of the occurrence of flat temperature profiles. Also, the generalization of the quantitative analysis is done to consider molecular weight effects, especially based on changes of the phase envelope to an hourglass type. Topics in implementation of the FRRPP process from pre-emulsions of monomers and the solvent/precipitant are highlighted. Additional FRRPP topics are included in this monograph that pertain to more recent efforts of Gerard Caneba, such as oil spill control, oil dispersant system, and caustic sludge remediation from emulsion-based FRRPP materials, hydrolysis of vinyl acetate-acrylic acid-based copolymers, and other polymer modification studies from FRRPP-based emulsions.
Book Synopsis Monitoring Polymerization Reactions by : Wayne F. Reed
Download or read book Monitoring Polymerization Reactions written by Wayne F. Reed and published by John Wiley & Sons. This book was released on 2014-01-21 with total page 493 pages. Available in PDF, EPUB and Kindle. Book excerpt: Offers new strategies to optimize polymer reactions With contributions from leading macromolecular scientists and engineers, this book provides a practical guide to polymerization monitoring. It enables laboratory researchers to optimize polymer reactions by providing them with a better understanding of the underlying reaction kinetics and mechanisms. Moreover, it opens the door to improved industrial-scale reactions, including enhanced product quality and reduced harmful emissions. Monitoring Polymerization Reactions begins with a review of the basic elements of polymer reactions and their kinetics, including an overview of stimuli-responsive polymers. Next, it explains why certain polymer and reaction characteristics need to be monitored. The book then explores a variety of practical topics, including: Principles and applications of important polymer characterization tools, such as light scattering, gel permeation chromatography, calorimetry, rheology, and spectroscopy Automatic continuous online monitoring of polymerization (ACOMP) reactions, a flexible platform that enables characterization tools to be employed simultaneously during reactions in order to obtain a complete record of multiple reaction features Modeling of polymerization reactions and numerical approaches Applications that optimize the manufacture of industrially important polymers Throughout the book, the authors provide step-by-step strategies for implementation. In addition, ample use of case studies helps readers understand the benefits of various monitoring strategies and approaches, enabling them to choose the best one to match their needs. As new stimuli-responsive and "intelligent" polymers continue to be developed, the ability to monitor reactions will become increasingly important. With this book as their guide, polymer scientists and engineers can take full advantage of the latest monitoring strategies to optimize reactions in both the lab and the manufacturing plant.
Book Synopsis Control and Dynamic Optimization of Polymerization Reaction Processes by :
Download or read book Control and Dynamic Optimization of Polymerization Reaction Processes written by and published by . This book was released on 2004 with total page 466 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis The Dynamic Behavior of Free Radical Solution Polymerization Reactions in a Continuous Stirred Tank Reactor by : Fouad Abdel Rahman Teymour
Download or read book The Dynamic Behavior of Free Radical Solution Polymerization Reactions in a Continuous Stirred Tank Reactor written by Fouad Abdel Rahman Teymour and published by . This book was released on 1989 with total page 468 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Methods of Model Based Process Control by : R. Berber
Download or read book Methods of Model Based Process Control written by R. Berber and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 814 pages. Available in PDF, EPUB and Kindle. Book excerpt: Model based control has emerged as an important way to improve plant efficiency in the process industries, while meeting processing and operating policy constraints. The reader of Methods of Model Based Process Control will find state of the art reports on model based control technology presented by the world's leading scientists and experts from industry. All the important issues that a model based control system has to address are covered in depth, ranging from dynamic simulation and control-relevant identification to information integration. Specific emerging topics are also covered, such as robust control and nonlinear model predictive control. In addition to critical reviews of recent advances, the reader will find new ideas, industrial applications and views of future needs and challenges. Audience: A reference for graduate-level courses and a comprehensive guide for researchers and industrial control engineers in their exploration of the latest trends in the area.
Book Synopsis Stable Free Radical Polymerization Conducted In Emulsion Polymerization Systems by :
Download or read book Stable Free Radical Polymerization Conducted In Emulsion Polymerization Systems written by and published by . This book was released on 2002 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Free radical polymerization is the most common polymerization technique that is used for the manufacturing of polymers, due to the ease of the polymerization initiation, wide latitude of the material design for a large variety of monomers, and the excellent process robustness for commercial production. In the 1990's, research activities for the precise control of radical polymerization process resulted in the discovery of 'Living Radical Polymerization'. The discoveries opened the door for the next generation of radical polymerizations. Extensive research has been conducted to understand the mechanisms and kinetics for numerous practical applications, particularly for polymerization in bulk and solution systems. However, despite the interest of industry, the mechanistic understanding in aqueous dispersed systems such as emulsion and miniemulsion polymerization is far behind the aforementioned two systems. There are still major challenges from the production viewpoint. One reason for the poor understanding is the complexity of the heterogeneous system, which includes multiple reaction phases that are accompanied by the segregation and transfer of the reaction species among different phases. The purpose of this research was to investigate living radical polymerization or "Stable Free Radical Polymerization" (SFRP) in aqueous dispersed systems to obtain better mechanistic understanding of how the heterogeneous nature of the system interacts with the novel living radical chemistry. The theoretical and experimental feasibility of the SFRP emulsion process were studied in this research, in particular, focusing on the compartmentalization effect. Particle size influence on the polymerization kinetics and the polymer livingness was experimentally confirmed, and compared to bulk polymerization. In addition, a comprehensive mathematical model including all major chemical and physical events was developed to further our mechanistic understanding. Based on the results from the.
Book Synopsis 26th European Symposium on Computer Aided Process Engineering by :
Download or read book 26th European Symposium on Computer Aided Process Engineering written by and published by Elsevier. This book was released on 2016-06-17 with total page 2482 pages. Available in PDF, EPUB and Kindle. Book excerpt: 26th European Symposium on Computer Aided Process Engineering contains the papers presented at the 26th European Society of Computer-Aided Process Engineering (ESCAPE) Event held at Portorož Slovenia, from June 12th to June 15th, 2016. Themes discussed at the conference include Process-product Synthesis, Design and Integration, Modelling, Numerical analysis, Simulation and Optimization, Process Operations and Control and Education in CAPE/PSE. Presents findings and discussions from the 26th European Society of Computer-Aided Process Engineering (ESCAPE) Event
Book Synopsis Emulsion Polymerization by : Irja Piirma
Download or read book Emulsion Polymerization written by Irja Piirma and published by . This book was released on 1982 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Emulsion Polymerization by : Robert G. Gilbert
Download or read book Emulsion Polymerization written by Robert G. Gilbert and published by . This book was released on 1995 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a modern overview of the principles governing emulsion polymerization, a topic of both academic and industrial importance. The reader is provided with the mathematical, physical and technical tools to understand the mechanisms and physical chemistry of these systems, particularly the major advances of the last 15 years. The book describes the mechanisms that govern the various aspects of an emulsion polymerization, and how from appropriate experimental studies, the dominant mechanisms in a particular system may be deduced. From such deductions, the means are developed whereby the properties of the result of the emulsion polymerization can be quantitatively modelled and trends can be qualitatively understood and predicted. This book opens the way to the intelligent, knowledge-based design that is the future for improvements and innovations in products and processes from this important technology. Provides a thoroughly up-to-date overview of the principles and practices of emulsion polymerization Contains mathematical, physical, and technical tools which enable the reader to understand the mechanisms and physical chemistry used in the field Includes extensive exercises with model answers
Book Synopsis "Living"/controlled Radical Polymerization by : Delphine Chan-Seng
Download or read book "Living"/controlled Radical Polymerization written by Delphine Chan-Seng and published by . This book was released on 2007 with total page 306 pages. Available in PDF, EPUB and Kindle. Book excerpt: Emulsion polymerization is an important process for the industrial production of polymers. However, initial attempts at performing "living"/controlled radical polymerization under emulsion conditions were not particularly successful primarily due to latex instability. To address this problem a unique nanoprecipitation process was developed in our laboratory for the stable free radical polymerization (SFRP) process. The first part of this thesis describes attempts to generalize this process and extend it to the copper based atom transfer radical polymerization, ATRP, process. Details describing initial problems we had with reproducing some initial successful results are provided. Once the process was under control it was used to synthesize block copolymers. The ability of these block copolymers to self-assemble in aqueous solutions and in bulk were subsequently investigated and the results of these studies are detailed at the end of the discussion on the emulsion process. The second part of the thesis deals with the SFRP process and more specifically with the difficulty of the process to moderate the polymerization of acrylates. Two reasons have been advanced to account for this difficulty; a high bond dissociation energy between the C-O bond linking the nitroxide moiety to the end of the polymer chain and an accumulation of excess nitroxide, caused by unavoidable chain termination, which causes inhibition of the polymerization. To address the high bond dissociation energy a nitroxide, specifically, 1,1'-diadamantyl nitroxide, containing very bulky substituents that might cause the bond to weaken, was synthesized and studied. To address the accumulation of excess free nitroxide, high temperature additives, that would slowly dissociate over time and consume the excess nitroxides, were studied. The results of both of these approaches are provided enabling some insight into what might be actually restricting the polymerization of acrylates.
Book Synopsis Modeling, Process Monitoring and Optimizing Control of Emulsion Polymerization Processes by : Heiko Brandt
Download or read book Modeling, Process Monitoring and Optimizing Control of Emulsion Polymerization Processes written by Heiko Brandt and published by . This book was released on 2019 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
