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Development Of A Technique For Mercury Speciation And Quantification Using Gas Chromatography
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Download or read book Gas Chromatography written by Colin Poole and published by Elsevier. This book was released on 2012-06-19 with total page 754 pages. Available in PDF, EPUB and Kindle. Book excerpt: A single source of authoritative information on all aspects of the practice of modern gas chromatography, from theory, to methods, to selected applications. It also provides access to core data for practical work, comparison of results, and decision making and facilitates the search for sources in related areas of study.
Book Synopsis Instrumental Methods in Metal Ion Speciation by : Imran Ali
Download or read book Instrumental Methods in Metal Ion Speciation written by Imran Ali and published by CRC Press. This book was released on 2006-03-14 with total page 265 pages. Available in PDF, EPUB and Kindle. Book excerpt: The knowledge of metal ion speciation is essential for predicting the exact toxicities of metal ion species in the environment. Metal ions can exist in various oxidation states, each of which possesses different physical and chemical properties as well as exhibit varying toxicities. Often, toxicity data is unreliable because it is based on metal io
Book Synopsis Practical Gas Chromatography by : Katja Dettmer-Wilde
Download or read book Practical Gas Chromatography written by Katja Dettmer-Wilde and published by Springer. This book was released on 2014-11-05 with total page 904 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.
Book Synopsis Speciation Studies in Soil, Sediment and Environmental Samples by : Sezgin Bakirdere
Download or read book Speciation Studies in Soil, Sediment and Environmental Samples written by Sezgin Bakirdere and published by CRC Press. This book was released on 2013-09-26 with total page 614 pages. Available in PDF, EPUB and Kindle. Book excerpt: Recent developments clearly indicate that speciation studies in biological and environmental matrices are much more important than the total element determination due to the tremendous difference in bioavailability and toxicity of various chemical forms of a particular element. Different separation-detection techniques and hyphenated systems—each with its own advantages and disadvantages with respect to precision, sensitivity and detection limit—have been developed for the identification and quantification of the species present in systems at ultra-trace levels. This book aims to evaluate the speciation analysis in depth and present a comprehensive review of state-of-the-art analytical approaches used for the speciation of elements in environmental samples.
Book Synopsis Vapor Generation Techniques for Trace Element Analysis by : Alessandro D'Ulivo
Download or read book Vapor Generation Techniques for Trace Element Analysis written by Alessandro D'Ulivo and published by Elsevier. This book was released on 2022-04-23 with total page 477 pages. Available in PDF, EPUB and Kindle. Book excerpt: Vapor Generation Techniques for Trace Element Analysis: Fundamental Aspects provides an overview and discussion of the fundamental aspects governing derivatization reactions of trace-level elements for analytical purposes. Vapor generation techniques coupled with atomic or mass spectrometry have been employed for over 50 years, but their popularity has dramatically increased in recent years, especially as alternative vapor generation approaches have been developed. This book bridges the knowledge gap of the derivatization mechanisms that yield volatile compounds and provides an update on recent developments in vapor generation techniques used for the determination and speciation of trace elements by atomic optical and mass spectrometry. It will serve as a comprehensive, single-source overview of recent developments, providing readers with an understanding of the correct implementation—and limitations—of applying vapor generation techniques to everyday analytical problems facing the trace element analyst. - Covers reaction mechanisms and fundamental processes of vapor generation in detail - Includes classical and alternative vapor generation approaches: alkylation, chelation, plasma, photochemical and electrochemical - Guides the interpretation of experimental results and implementation of vapor generation techniques in the laboratory
Book Synopsis Organometallics in Environment and Toxicology by : Astrid Sigel
Download or read book Organometallics in Environment and Toxicology written by Astrid Sigel and published by Walter de Gruyter GmbH & Co KG. This book was released on 2015-07-24 with total page 608 pages. Available in PDF, EPUB and Kindle. Book excerpt: Volume 7, devoted to the vital and rapidly expanding research area around metal-carbon bonds (see also MILS-6), focuses on the environment. With more than 2500 references, 35 tables, and nearly 50 illustrations, many of these in color, it is an essential resource for scientists working in the wide range from organometallic chemistry, inorganic biochemistry, environmental toxicology all the way through to physiology and medicine. In 14 stimulating chapters, written by 29 internationally recognized experts, Organometallics in Environment and Toxicology highlights in an authoritative and timely manner environmental cycles of elements involving organometal(loid) compounds as well as the analytical determination of such species. This book examines methane formation involving the nickel coenzyme F430, as well as the organometal(loid) compounds formed by tin, lead, arsenic, antimony, bismuth, selenium, tellurium, and mercury. In addition, it deals with the environmental bioindication, biomonitoring, and bioremediation of organometal(loid)s, and it terminates with methylated metal(loid) species occurring in humans by evaluating assumed and proven health effects caused by these compounds.
Book Synopsis Developing Ambient Water Quality Criteria for Mercury by : D. R. J. Moore
Download or read book Developing Ambient Water Quality Criteria for Mercury written by D. R. J. Moore and published by IWA Publishing. This book was released on 2003-07-31 with total page 184 pages. Available in PDF, EPUB and Kindle. Book excerpt: This project examined the development of ambient water quality criteria (AWQC) for the protection of wildlife for mercury. Mercury is considered a serious risk to wildlife in many areas. As a result, the Great Lakes Water Quality Initiative and others have developed AWQC. These AWQC have been controversial, however, because (1) the AWQC were single values that did not account for site-specific conditions; (2) derivation of the AWQC relied on a single NOAEL, and (3) the AWQC had an unknown level of conservatism because of reliance on both average and conservative assumptions and uncertainty factors. Rather than develop a single value AWQC for total mercury, we derive an AWQC model that explicitly incorporates factors controlling bioavailability, methylation rates and bioaccumulation in the aquatic environment (e.g., pH, DOC, sulfate). To derive our AWQC model, field data was collected including numerous water quality parameters and total mercury and methylmercury concentrations in whole body fish tissue from 31 lakes in Ontario and an additional 10 lakes in Nova Scotia. An independent dataset consisting of 51 water bodies in the United States was then used to confirm the validity and robustness of the AWQC model. Next we combined the results of chronic-feeding studies with similar protocols and endpoints, in a meta-analysis to derive a dose-response curve for mink exposed to mercury in the diet. Using this approach, one can derive an LD5 or other similar endpoint that can then be used as the basis for deriving -wildlife AWQC. In the final step, we used a probabilistic risk model to estimate the concentrations of methylmercury in water that would lead to levels in fish sufficient for there to be a 10% probability of exceeding the mink LD5. This analysis was repeated for various combinations of pH and DOC. The result is an AWQC model for mercury for the protection of wildlife that can be used for a variety of site-specific conditions. This publication can also be purchased and downloaded via Pay Per View on Water Intelligence Online - click on the Pay Per View icon below
Book Synopsis Sample Introduction Systems in ICPMS and ICPOES by : Diane Beauchemin
Download or read book Sample Introduction Systems in ICPMS and ICPOES written by Diane Beauchemin and published by Newnes. This book was released on 2020-03-15 with total page 588 pages. Available in PDF, EPUB and Kindle. Book excerpt: Sample Introduction Systems in ICPMS and ICPOES provides an in-depth analysis of sample introduction strategies, including flow injection analysis and less common techniques, such as arc/spark ablation and direct sample insertion. The book critically evaluates what has been accomplished so far, along with what can be done to extend the capabilities of the technique for analyses of any type of sample, such as aqueous, gaseous or solid. The latest progress made in fields, such as FIA, ETV, LC-ICP-MS and CE-ICP-MS is included and critically discussed. The book addresses problems related to the optimization of the system, peak dispersion and calibration and automatization. - Provides contributions from recognized experts that give credibility to each chapter as a reference source - Presents a single source, providing the big picture for ICPMS and ICPOES - Covers theory, methods, selected applications and discrete sampling techniques - Includes access to core data for practical work, comparison of results and decision-making
Book Synopsis Environmental Chemistry and Toxicology of Mercury by : Guangliang Liu
Download or read book Environmental Chemistry and Toxicology of Mercury written by Guangliang Liu and published by John Wiley & Sons. This book was released on 2011-11-07 with total page 435 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides the fundamentals, recent developments, and future research needs for critical mercury transformation and transport processes, as well as the experimental methods that have been employed in recent studies. The coverage discusses the environmental behavior and toxicological effects of mercury on organisms, including humans, and provides case studies at the end of each chapter. Bringing together information normally spread across several books, this text is unique in covering the entire mercury cycle and providing a baseline for what is known and what uncertainties remain in respect to mercury cycling.
Book Synopsis Elemental Speciation by : Joseph A. Caruso
Download or read book Elemental Speciation written by Joseph A. Caruso and published by Elsevier Science Limited. This book was released on 2000 with total page 581 pages. Available in PDF, EPUB and Kindle. Book excerpt: Hardbound. This book provides a comprehensive discussion of the major aspects involved in elemental speciation. Sample preparation, separation techniques, instrumentation and quality assurance are all discussed. In addition, individual chapters are devoted to speciation of environmental samples and speciation of biological, clinical, and nutritional samples. Individual chapters are written by leaders in the field, and the book has been organized so that the reader may learn how to collect a sample and prepare it. Ways to separate and detect analytes of interest, and steps to take to ensure the validity of the measurements are also discussed. This book is unique in its comprehensive treatment of this subject.
Book Synopsis Hyphenated Techniques in Speciation Analysis by : Ryszard Lobinski
Download or read book Hyphenated Techniques in Speciation Analysis written by Ryszard Lobinski and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 238 pages. Available in PDF, EPUB and Kindle. Book excerpt: Speciation analysis is a field of trace element analytical chemistry that deals with detection, identification and determination of individual chemical forms of metals and metalloids. There has been increased awareness of the importance of elemental speciation over the last 20 years and this has lead to growing demand for analytical techniques capable of providing species-specific information. Hyphenated Techniques in Speciation Analysis offers a brief but comprehensive overview of hyphenated techniques and their various applications for the determination of chemical forms of trace elements. It brings a succinct presentation of the concept of speciation analysis, gives an overview of techniques based on coupling of chromatography with element and molecule specific detection and summarises their applications in the fields of environmental and industrial chemistry, biochemistry, nutrition, toxicology and medicine. Fully referenced, Hyphenated Techniques in Speciation Analysis is an invaluable introduction to elemental speciation analysis and also provides a practising analyst with a critical overview of research carried out in the field.
Book Synopsis Toxicological Profile for Mercury by :
Download or read book Toxicological Profile for Mercury written by and published by . This book was released on 1994 with total page 388 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Extraction Chromatography written by and published by Elsevier. This book was released on 1975-06-01 with total page 585 pages. Available in PDF, EPUB and Kindle. Book excerpt: Extraction Chromatography
Book Synopsis Selected Water Resources Abstracts by :
Download or read book Selected Water Resources Abstracts written by and published by . This book was released on 1990 with total page 710 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Methods of Analysis of Food Components and Additives by : Semih Otles
Download or read book Methods of Analysis of Food Components and Additives written by Semih Otles and published by CRC Press. This book was released on 2005-04-26 with total page 451 pages. Available in PDF, EPUB and Kindle. Book excerpt: With diet and health news making headlines on a regular basis, the ability to separate, identify, and analyze the nutrients, additives, and toxicological compounds found in food and food compounds is more important than ever. This requires proper training in the application of the best methods, as well as knowledgeable efforts to improve existing methods to meet certain analytical needs. Methods of Analysis for Food Components and Additives is a concise guide to both new and established methods for the analysis of food components and additives. The book presents detailed explanations of modern methods of analysis by 32 leading scientists, many of whom personally developed or refined the techniques. They summarize key findings on novel methods of analysis of food components, additives, and contaminants, including the identification, speciation, and determination of components in raw materials and food products. Each chapter is structured to provide a description of the component or additive that can be analyzed, a simple method explanation of how it works, examples of applications, and references for more specific information. This comprehensive volume features all major classes of food components and contaminants, along with components of current interest to the nutraceutical and functional foods industries. It is an essential reference for food scientists and chemists, as well as food manufacturers and researchers interested in the many methods of food analysis.
Book Synopsis Perspectives and Challenges of Hair Analysis by : Pascal Kintz
Download or read book Perspectives and Challenges of Hair Analysis written by Pascal Kintz and published by Royal Society of Chemistry. This book was released on 2023-12-18 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Hair analysis is a reliable and widely used tool to evaluate drug exposure in many fields, including workplace testing, drug abuse history and withdrawal control, post-mortem toxicology, doping control, therapeutic drug monitoring of pharmaceuticals and even environmental exposure to toxic agents. Compounds incorporated into the hair structure resist hair growth and regular washing for several months, leading to a potential chronological trace of exposure, with farther periods corresponding to the hair segments more distant from the hair root. The relentless improvement of analytical procedures and instrumental technologies, together with the continuous introduction of new psychoactive substances, have led to an increasing number of studies and practical applications of hair analysis. This book is a comprehensive guide to hair analysis from general concepts, ideal for students and those new to the field, to interpretation and advanced methods for experts working in the area. With contributions from world-leading scientists in each field, this book describes state-of-the-art, emerging issues and recent analytical approaches to hair analysis that will serve as an essential tool to clinical and forensic toxicology laboratories across the globe.
Book Synopsis Traceability in Chemical Measurement by : Paul De Bièvre
Download or read book Traceability in Chemical Measurement written by Paul De Bièvre and published by Springer Science & Business Media. This book was released on 2005-12-06 with total page 308 pages. Available in PDF, EPUB and Kindle. Book excerpt: Metrological traceability of chemical measurement results means the establishment of a relation to metrological stated references through an unbroken chain of comparisons. This volume collects 56 outstanding papers on the topic, mostly published in the period 2000-2003 in the journal "Accreditation and Quality Assurance". They provide the latest understanding, and possibly the rationale why it is important to integrate the concept of metrological traceability including suitable measurement standards such as certified reference materials, into the standard measurement procedures of every analytical laboratory. In addition, this anthology considers the benefits to both the analytical laboratory and the user of the measurement results.
