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Author : Renkang Zhu
Publisher :
ISBN 13 :
Total Pages : 672 pages
Book Rating : 4.:/5 (16 download)
Download or read book Development and Applications of Scanning Electrochemical Microscopy (SECM). written by Renkang Zhu and published by . This book was released on 2007 with total page 672 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Adrian C. Michael
Publisher : CRC Press
ISBN 13 : 1420005863
Total Pages : 540 pages
Book Rating : 4.4/5 (2 download)
Download or read book Electrochemical Methods for Neuroscience written by Adrian C. Michael and published by CRC Press. This book was released on 2006-12-13 with total page 540 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the first implant of a carbon microelectrode in a rat 35 years ago, there have been substantial advances in the sensitivity, selectivity and temporal resolution of electrochemical techniques. Today, these methods provide neurochemical information that is not accessible by other means. The growing recognition of the versatility of electrochemi
Author : Allen J. Bard
Publisher : CRC Press
ISBN 13 : 9780203910771
Total Pages : 668 pages
Book Rating : 4.9/5 (17 download)
Download or read book Scanning Electrochemical Microscopy written by Allen J. Bard and published by CRC Press. This book was released on 2001-04-18 with total page 668 pages. Available in PDF, EPUB and Kindle. Book excerpt: Scanning Electrochemical Microscopy describes the theory and operating principles of scanning electrochemical microscopy (SECM), including instrumentation, tip preparation, imaging techniques and potentiometric probes. The book explores applications relevant to electron transfer reactions, reaction kinetics, chemical events at interfaces, biologica
Author : Allen J. Bard
Publisher : CRC Press
ISBN 13 : 1000584062
Total Pages : 1260 pages
Book Rating : 4.0/5 (5 download)
Download or read book Scanning Electrochemical Microscopy written by Allen J. Bard and published by CRC Press. This book was released on 2022-07-29 with total page 1260 pages. Available in PDF, EPUB and Kindle. Book excerpt: Because of its simplicity of use and quantitative results, Scanning Electrochemical Microscopy (SECM) has become an indispensable tool for the study of surface reactivity. The fast expansion of the SECM field over several years has been fueled by the introduction of new probes, commercially available instrumentation, and new practical applications. Scanning Electrochemical Microscopy, Third Edition offers essential background and in-depth overviews of specific applications in self-contained chapters. The vitality and growing popularity of SECM over the past 30+ years have largely been determined by its versatility and capability to remain useful in the changing scientific and technological environments. New applications reported during the last decade reflect significant current activity in biomedical and energy-related research. This thoroughly updated edition provides up-to-date comprehensive reviews of different aspects of SECM. New chapters by renowned professionals in the field cover recent advances in different areas of SECM including nanoSECM, surface reactions and films, batteries, and fuel cells. Expanded coverage of electrocatalysis and surface interrogation as well as photoelectrochemistry and photoelectrocatalysis are also provided. Useful for a broad range of interdisciplinary research—from biological systems to nanopatterning—this book is invaluable to all interested in learning and applying SECM.
Author : Allen J. Bard
Publisher : CRC Press
ISBN 13 : 1439831122
Total Pages : 673 pages
Book Rating : 4.4/5 (398 download)
Download or read book Scanning Electrochemical Microscopy, Second Edition written by Allen J. Bard and published by CRC Press. This book was released on 2012-04-16 with total page 673 pages. Available in PDF, EPUB and Kindle. Book excerpt: Because of its simplicity of use and quantitative results, Scanning Electrochemical Microscopy (SECM) has become an indispensable tool for the study of surface reactivity. The fast expansion of the SECM field during the last several years has been fueled by the introduction of new probes, commercially available instrumentation, and new practical applications. Scanning Electrochemical Microscopy, Second Edition offers essential background and in-depth overviews of specific applications in self-contained chapters. Recent methodological advances have greatly increased the capacity of SECM to characterize interfaces at the nanoscale and to obtain molecular-level chemical information. This thoroughly updated edition retains original chapters describing the principles of SECM measurements, instrumentation, preparation of SECM probes, imaging methodologies, and theory and offers: New chapters on studies of single biological cells, corrosion, electrocatalysis, and hybrid techniques Descriptions of recent advances of SECM in several areas of current interest: biotechnological applications, nanofabrication and surface patterning, and molecular transport across films and membranes Discussion of the ongoing shift from micrometer-scale experiments to the nanoscale Useful for a broad range of interdisciplinary research—from biological systems to probing reactions at the liquid–liquid interface—this book is invaluable to all interested in learning and applying SECM.
Author : Mario Alberto Alpuche Avilés
Publisher :
ISBN 13 :
Total Pages : 316 pages
Book Rating : 4.:/5 (696 download)
Download or read book Development of Multi-dimensional Methods for Scanning Electrochemical Microscopy (SECM) written by Mario Alberto Alpuche Avilés and published by . This book was released on 2005 with total page 316 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Fred Lisdat
Publisher : Springer
ISBN 13 : 3540752013
Total Pages : 515 pages
Book Rating : 4.5/5 (47 download)
Download or read book Biosensing for the 21st Century written by Fred Lisdat and published by Springer. This book was released on 2007-11-20 with total page 515 pages. Available in PDF, EPUB and Kindle. Book excerpt: With contributions by numerous experts
Author : Cynthia G. Zoski
Publisher : Elsevier
ISBN 13 : 0444519580
Total Pages : 935 pages
Book Rating : 4.4/5 (445 download)
Download or read book Handbook of Electrochemistry written by Cynthia G. Zoski and published by Elsevier. This book was released on 2007-02-07 with total page 935 pages. Available in PDF, EPUB and Kindle. Book excerpt: Electrochemistry plays a key role in a broad range of research and applied areas including the exploration of new inorganic and organic compounds, biochemical and biological systems, corrosion, energy applications involving fuel cells and solar cells, and nanoscale investigations. The Handbook of Electrochemistry serves as a source of electrochemical information, providing details of experimental considerations, representative calculations, and illustrations of the possibilities available in electrochemical experimentation. The book is divided into five parts: Fundamentals, Laboratory Practical, Techniques, Applications, and Data. The first section covers the fundamentals of electrochemistry which are essential for everyone working in the field, presenting an overview of electrochemical conventions, terminology, fundamental equations, and electrochemical cells, experiments, literature, textbooks, and specialized books. Part 2 focuses on the different laboratory aspects of electrochemistry which is followed by a review of the various electrochemical techniques ranging from classical experiments to scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry. Applications of electrochemistry include electrode kinetic determinations, unique aspects of metal deposition, and electrochemistry in small places and at novel interfaces and these are detailed in Part 4. The remaining three chapters provide useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials. * serves as a source of electrochemical information * includes useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials * reviews electrochemical techniques (incl. scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry)
Author : Ana Cristina Perdomo Marin
Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (19 download)
Download or read book Applications of Microelectrodes and Scanning Electrochemical Microscopy (SECM) to Complex Environmental Interfaces written by Ana Cristina Perdomo Marin and published by . This book was released on 2018 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Christoph Hartnig
Publisher : Elsevier
ISBN 13 : 085709548X
Total Pages : 522 pages
Book Rating : 4.8/5 (57 download)
Download or read book Polymer Electrolyte Membrane and Direct Methanol Fuel Cell Technology written by Christoph Hartnig and published by Elsevier. This book was released on 2012-02-20 with total page 522 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymer electrolyte membrane fuel cells (PEMFCs) and direct methanol fuel cells (DMFCs) technology are promising forms of low-temperature electrochemical power conversion technologies that operate on hydrogen and methanol respectively. Featuring high electrical efficiency and low operational emissions, they have attracted intense worldwide commercialization research and development efforts. These R&D efforts include a major drive towards improving materials performance, fuel cell operation and durability. In situ characterization is essential to improving performance and extending operational lifetime through providing information necessary to understand how fuel cell materials perform under operational loads. Polymer Electrolyte Membrane and Direct Methanol Fuel Cell Technology, Volume 2 details in situ characterization, including experimental and innovative techniques, used to understand fuel cell operational issues and materials performance. Part I reviews enhanced techniques for characterization of catalyst activities and processes, such as X-ray absorption and scattering, advanced microscopy and electrochemical mass spectrometry. Part II reviews characterization techniques for water and fuel management, including neutron radiography and tomography, magnetic resonance imaging and Raman spectroscopy. Finally, Part III focuses on locally resolved characterization methods, from transient techniques and electrochemical microscopy, to laser-optical methods and synchrotron radiography. With its international team of expert contributors, Polymer electrolyte membrane and direct methanol fuel cell technology will be an invaluable reference for low temperature fuel cell designers and manufacturers, as well as materials science and electrochemistry researchers and academics. Polymer electrolyte membrane and direct methanol fuel cell technology is an invaluable reference for low temperature fuel cell designers and manufacturers, as well as materials science and electrochemistry researchers and academics. Details in situ characterisation of polymer electrolyte membrane fuel cells (PEMFCs) and direct methanol fuel cells (DMFCs), including the experimental and innovative techniques used to understand fuel cell operational issues and materials performance Examines enhanced techniques for characterisation of catalyst activities and processes, such as X-ray absorption and scattering, advanced microscopy and electrochemical mass spectrometry Reviews characterisation techniques for water and fuel management, including neutron radiography and tomography, and comprehensively covers locally resolved characterisation methods, from transient techniques to laser-optical methods
Author : Lauro Tatsuo Kubota
Publisher : Springer Nature
ISBN 13 : 3030823814
Total Pages : 559 pages
Book Rating : 4.0/5 (38 download)
Download or read book Tools and Trends in Bioanalytical Chemistry written by Lauro Tatsuo Kubota and published by Springer Nature. This book was released on 2021-11-25 with total page 559 pages. Available in PDF, EPUB and Kindle. Book excerpt: This textbook covers the main tools and techniques used in bioanalysis, provides an overview of their principles, and offers several examples of their application and future trends in diagnosis. Chapters from expert contributors explore the role of bioanalysis in different areas such as biochemistry, physiology, forensics, and clinical diagnosis, including topics from sampling/sample preparation, chemometrics in bioanalysis to the latest techniques used in the field. Particular attention is given to the recent advances in the application of mass spectrometry, NMR, electrochemical methods and separation techniques in bioanalysis. Readers will also find more about the application of microchip-based devices and analytical microarrays. This textbook will appeal to graduate/advanced undergraduate students in Chemistry, Biology, Biochemistry, Pharmacy, and Chemical Engineering. It is also a useful resource for researchers and professionals working in the fields of biomedicine and veterinary sciences, with clear explanations and examples of how the different bioanalytical devices are applied for clinical diagnosis.
Author : Christian Iffelsberger
Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (119 download)
Download or read book Method Development for Scanning Electrochemical Microscopy and Its Application for Material Characterization written by Christian Iffelsberger and published by . This book was released on 2018 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Mark E. Orazem
Publisher : John Wiley & Sons
ISBN 13 : 111820994X
Total Pages : 510 pages
Book Rating : 4.1/5 (182 download)
Download or read book Electrochemical Impedance Spectroscopy written by Mark E. Orazem and published by John Wiley & Sons. This book was released on 2011-10-13 with total page 510 pages. Available in PDF, EPUB and Kindle. Book excerpt: Using electrochemical impedance spectroscopy in a broad range of applications This book provides the background and training suitable for application of impedance spectroscopy to varied applications, such as corrosion, biomedical devices, semiconductors and solid-state devices, sensors, batteries, fuel cells, electrochemical capacitors, dielectric measurements, coatings, electrochromic materials, analytical chemistry, and imaging. The emphasis is on generally applicable fundamentals rather than on detailed treatment of applications. With numerous illustrative examples showing how these principles are applied to common impedance problems, Electrochemical Impedance Spectroscopy is ideal either for course study or for independent self-study, covering: Essential background, including complex variables, differential equations, statistics, electrical circuits, electrochemistry, and instrumentation Experimental techniques, including methods used to measure impedance and other transfer functions Process models, demonstrating how deterministic models of impedance response can be developed from physical and kinetic descriptions Interpretation strategies, describing methods of interpretating of impedance data, ranging from graphical methods to complex nonlinear regression Error structure, providing a conceptual understanding of stochastic, bias, and fitting errors in frequency-domain measurements An overview that provides a philosophy for electrochemical impedance spectroscopy that integrates experimental observation, model development, and error analysis This is an excellent textbook for graduate students in electrochemistry, materials science, and chemical engineering. It's also a great self-study guide and reference for scientists and engineers who work with electrochemistry, corrosion, and electrochemical technology, including those in the biomedical field, and for users and vendors of impedance-measuring instrumentation.
Author : Ugne Mitrikeviciute
Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (119 download)
Download or read book Development of Quantitative Scanning Electrochemical Microscopy (SECM) Imaging of Single and Array Micro and Nanoband Edge Platinum Electrodes written by Ugne Mitrikeviciute and published by . This book was released on 2019 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Damien W. M. Arrigan
Publisher : Royal Society of Chemistry
ISBN 13 : 1849738319
Total Pages : 412 pages
Book Rating : 4.8/5 (497 download)
Download or read book Electrochemical Strategies in Detection Science written by Damien W. M. Arrigan and published by Royal Society of Chemistry. This book was released on 2016 with total page 412 pages. Available in PDF, EPUB and Kindle. Book excerpt: Electrochemical methods of chemical analysis have been widely used for many years, the purpose of this volume is to address research and development advances based on new and re-vitalised methods, new materials with enhanced properties and new devices that achieve better electroanalytical signal generation.
Author : Harry O. Finklea
Publisher : Elsevier Publishing Company
ISBN 13 :
Total Pages : 552 pages
Book Rating : 4.3/5 (91 download)
Download or read book Semiconductor Electrodes written by Harry O. Finklea and published by Elsevier Publishing Company. This book was released on 1988 with total page 552 pages. Available in PDF, EPUB and Kindle. Book excerpt: Semiconductors have been studied as electrodes in electrochemical systems since the mid-1950's. However, it was not until the 1970's that the search for alternative energy sources, especially solar energy, led to an enormous expansion in semiconductor electrode research. One attractive option for solar energy conversion is the semiconductor liquid-junction solar cell, which can be designed to produce either electrical power or fuel such as hydrogen. Consequently the number of papers published concerning semiconductor electrodes has rapidly increased. Previous books have principally focused on the underlying theory (largely from solid state physics) and principles of operation of all semiconductor electrodes. It therefore seemed both useful and appropriate to review the field with the intention of collating information for each semiconductor or family of semiconductors, with contributions from authors who are all recognized experts in their field. Each chapter is devoted to critically assessing the recent literature on a particular semiconductor or family of semiconductors.
Author : Laurence Danis
Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (979 download)
Download or read book Development of Micro-and Nano-scanning Electrochemical Microscopy Probes for Perspective Applications in Lithium Ion Batteries written by Laurence Danis and published by . This book was released on 2017 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: "Lithium ion batteries (LIBs) have become a common power source for most portable home electronic devices including cellular phones, computers, tablets, power tools, and, recently, electric vehicles. Despite their success, the commercial market demands portable energy storage which offers more charge/discharge cycles, shorter recharge times, and higher power densities. Therefore, LIB materials research aims to improve key electrochemical properties. The cubic spinel lithium manganese oxide (LixMn2O4) is an alternative to LiCoO2 and is one of the most investigated positive electrode materials for LIBs. LixMn2O4 is of particular interest due to its advantageous electrochemical performance at room temperature (i.e. high capacity and stable operating voltage), significant natural abundance, low cost, and low toxicity. Regardless of these advantages, LixMn2O4 experiences a fast capacity fade with charge/discharge cycling and poor storage performance, particularly at elevated temperatures. This hinders its widespread commercial use, especially for large-scale automotive applications. This capacity-fading phenomenon is believed to be due to numerous factors, such as the Jahn-Teller distortion, the decomposition of electrolyte solution on the negative electrode, and the dissolution of Mn2+ from the positive electrode into the electrolyte. Most research groups agree that dissolution of Mn2+ cations is the leading mechanisms for the decreased capacity and is primarily caused by the hydrogen fluoride (HF) contained in the electrolyte.In-depth understanding of the mechanism of Mn dissolution could provide insights for new methods to inhibit the dissolution pathway. However, standard manganese detection techniques are performed ex-situ, post cell disassembly and have potential risk of data alterations due to air sensitivity of these materials, creating a need for in-situ analysis techniques of battery materials. The presented dissertation investigates the use of scanning probe microscopy (SPM) analysis methods to provide localized information on the fundamental mechanisms, processes and degradation of LIBs. Herein, we present the step-by-step development of a high resolution scanning electrochemical microscopy (SECM) technique for the quantitative detection of Mn2+ cations. More precisely, we describe the development and characterization of Hg/Pt hemispherical micro- and nano- SECM probes used with anodic stripping voltammetry (ASV), for the quantitative detection of Mn2+ cations. We have successfully developed a simple, fast, and reproducible method for the fabrication of disk microelectrodes with controlled geometry. A second fabrication technique is presented for the production of well-defined Pt disk electrodes with the electroactive core in the nanometer scale. Both of these fabrication techniques produce electrodes that are are ideal backbones for the production of Hg-based hemispherical ASV sensors. Also presented is a systematic study of the shear force (SF) characteristics of these nanoelectrodes and a new methodology to identify SF sensitive frequencies. SF is used in SECM to maintain a constant tip-to-substrate distance for the deconvolution of the kinetic and topographic information received in SECM. The Hg/Pt hemispherical nanoelectrodes were used for the quantitative detection of manganese cations. The ASV technique has been used to evaluate the impact of using polymeric chelating macrocyles, such as crown ethers, as separator coatings. The coated separators would serve for the sequestration of Mn2+ cations, thus preventing their migration to negative electrodes, and therefore mitigating the undesirable consequences of manganese dissolution in LIBs. A transition from an aqueous environment to a more representative oxygen and water-free environment in propylene carbonate (PC) LiClO4, a typical a non-aqueous electrolyte for LIBs, has also been performed. " --
