Crystallization And Applications

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Crystallization

Author : Wolfgang Beckmann
Publisher : John Wiley & Sons
ISBN 13 : 3527650342
Total Pages : 370 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Crystallization by : Wolfgang Beckmann

Download or read book Crystallization written by Wolfgang Beckmann and published by John Wiley & Sons. This book was released on 2013-01-14 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.

Industrial Crystallization

Author : Alison Lewis
Publisher : Cambridge University Press
ISBN 13 : 1316299082
Total Pages : 354 pages
Book Rating : 4.3/5 (162 download)

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Book Synopsis Industrial Crystallization by : Alison Lewis

Download or read book Industrial Crystallization written by Alison Lewis and published by Cambridge University Press. This book was released on 2015-07-02 with total page 354 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bridging the gap between theory and practice, this text provides the reader with a comprehensive overview of industrial crystallization. Newcomers will learn all of the most important topics in industrial crystallization, from key concepts and basic theory to industrial practices. Topics covered include the characterization of a crystalline product and the basic process design for crystallization, as well as batch crystallization, measurement techniques, and details on precipitation, melt crystallization and polymorphism. Each chapter begins with an introduction explaining the importance of the topic, and is supported by homework problems and worked examples. Real world case studies are also provided, as well as new industry-relevant information, making this is an ideal resource for industry practitioners, students, and researchers in the fields of industrial crystallization, separation processes, particle synthesis, and particle technology.

Handbook of Industrial Crystallization

Author : Allan Myerson
Publisher : Butterworth-Heinemann
ISBN 13 : 0080533515
Total Pages : 329 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Handbook of Industrial Crystallization by : Allan Myerson

Download or read book Handbook of Industrial Crystallization written by Allan Myerson and published by Butterworth-Heinemann. This book was released on 2002-01-08 with total page 329 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes.The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design. Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the fieldCovers all aspects of industrial crystallization in a single, complete volume

Additives and Crystallization Processes

Author : Keshra Sangwal
Publisher : John Wiley & Sons
ISBN 13 : 9780470517826
Total Pages : 468 pages
Book Rating : 4.5/5 (178 download)

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Book Synopsis Additives and Crystallization Processes by : Keshra Sangwal

Download or read book Additives and Crystallization Processes written by Keshra Sangwal and published by John Wiley & Sons. This book was released on 2007-09-27 with total page 468 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystal growth technology involves processes for the production of crystals essential for microelectronics, communication technologies, lasers and energy producing and energy saving technology. A deliberately added impurity is called an additive and in different industries these affect the process of crystal growth. Thus, understanding of interactions between additives and the crystallizing phases is important in different processes found in the lab, nature and in various industries. This book presents a generalized description of the mechanisms of action of additives during nucleation, growth and aggregation of crystals during crystallization and has received endorsement from the President of the International Organization for Crystal Growth. It is the first text devoted to the role of additives in different crystallization processes encountered in the lab, nature and in industries as diverse as pharmaceuticals, food and biofuels. A unique highlight of the book are chapters on the effect of additives on crystal growth processes, since the phenomena discussed is an issue of debate between researchers

Crystallization and Applications

Author : Youssef Ben Smida
Publisher : BoD – Books on Demand
ISBN 13 : 1839693169
Total Pages : 189 pages
Book Rating : 4.8/5 (396 download)

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Book Synopsis Crystallization and Applications by : Youssef Ben Smida

Download or read book Crystallization and Applications written by Youssef Ben Smida and published by BoD – Books on Demand. This book was released on 2022-03-30 with total page 189 pages. Available in PDF, EPUB and Kindle. Book excerpt: The crystallization process may be used in chemistry, physics, or materials science to prepare materials for special applications such as batteries, fuel cells, and optics. In chemistry and physics, researchers prepare polycrystalline powders or thin films. In biology and pharmacology, proteins and drugs are obtained as polycrystalline powder and their structures are determined by X-ray powder diffraction or neutron diffraction. The synthesis of polycrystalline powder or thin films depends on several factors such as temperature, pressure, and operating parameters. This book discusses the phenomenon of crystallization in several fields and applications.

Crystallization

Author : Marcello Andreeta
Publisher : BoD – Books on Demand
ISBN 13 : 9535107577
Total Pages : 582 pages
Book Rating : 4.5/5 (351 download)

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Book Synopsis Crystallization by : Marcello Andreeta

Download or read book Crystallization written by Marcello Andreeta and published by BoD – Books on Demand. This book was released on 2012-09-19 with total page 582 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is one of the most ancient and interdisciplinary topics of research known to mankind. Crystals can be organic or inorganic and may be produced from melts, liquid solutions, vapors or even in solid state. Notwithstanding its inherently high complexity, the crystallization process is part of our everyday lives, from ice making in our homes to the most state-of-the-art chemical and electronic industry. In this book, our purpose was to present new insights to the reader, as well as crucial and very useful information for researchers working in this field, while simultaneously creating a comprehensive text about crystallization processes which may serve as a starting point for people with different backgrounds.

Crystallization of Organic Compounds

Author : Hsien-Hsin Tung
Publisher : John Wiley & Sons
ISBN 13 : 0470447788
Total Pages : 304 pages
Book Rating : 4.4/5 (74 download)

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Book Synopsis Crystallization of Organic Compounds by : Hsien-Hsin Tung

Download or read book Crystallization of Organic Compounds written by Hsien-Hsin Tung and published by John Wiley & Sons. This book was released on 2009-06-17 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: Filled with industrial examples emphasizing the practical applications of crystallization methodologies Based on the authors' hands-on experiences as process engineers at Merck, Crystallization of Organic Compounds guides readers through the practical aspects of crystallization. It uses plenty of case studies and examples of crystallization processes, ranging from development through manufacturing scale-up. The book not only emphasizes strategies that have been proven successful, it also helps readers avoid common pitfalls that can render standard procedures unsuccessful. The goal of this text is twofold: Build a deeper understanding of the fundamental properties of crystallization as well as the impact of these properties on crystallization process development. Improve readers' problem-solving abilities by using actual industrial examples with real process constraints. Crystallization of Organic Compounds begins with detailed discussions of fundamental thermodynamic properties, nucleation and crystal growth kinetics, process dynamics, and scale-up considerations. Next, it investigates modes of operation, including cooling, evaporation, anti-solvent, and reactive crystallization. The authors conclude with special applications such as ultrasound in crystallization and computational fluid dynamics in crystallization. Most chapters feature multiple examples that guide readers step by step through the crystallization of active pharmaceutical ingredients (APIs). With its focus on industrial applications, this book is recommended for chemical engineers and chemists who are involved with the development, scale-up, or operation of crystallization processes in the pharmaceutical and fine chemical industries.

Crystallization: Processes and Applications

Author : Garry Hollis
Publisher :
ISBN 13 : 9781639891313
Total Pages : 0 pages
Book Rating : 4.8/5 (913 download)

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Book Synopsis Crystallization: Processes and Applications by : Garry Hollis

Download or read book Crystallization: Processes and Applications written by Garry Hollis and published by . This book was released on 2022-09-13 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: A solid material whose constituents such as atoms, molecules, or ions are arranged in a highly ordered microscopic structure is referred to as a crystal. The physical transformation of a liquid, solution, or gas to a crystal is known as crystallization. Crystals are formed by phenomena such as precipitation, freezing, or deposition directly from a gas. The occurrence of crystallization involves two major steps, namely, nucleation and crystal growth. Its most prominent application is salt crystallization which is the most cost-effective way to produce salt. Applications of crystallization involve compound purification and crystal production. The book aims to shed light on some of the unexplored aspects of crystallization and the recent researches in this area. Also included herein is a detailed explanation of the various concepts and applications of this process. This book will serve as a reference to a broad spectrum of readers.

Synthesis Methods and Crystallization

Author : Riadh Marzouki
Publisher : BoD – Books on Demand
ISBN 13 : 1838802231
Total Pages : 138 pages
Book Rating : 4.8/5 (388 download)

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Book Synopsis Synthesis Methods and Crystallization by : Riadh Marzouki

Download or read book Synthesis Methods and Crystallization written by Riadh Marzouki and published by BoD – Books on Demand. This book was released on 2020-10-07 with total page 138 pages. Available in PDF, EPUB and Kindle. Book excerpt: New crystalline materials (organic, inorganic, hybrid) are promising for various applications, including electrical, piezoelectric, ferroelectric, magnetic, and catalytic processes. In addition, given their remarkable structural richness, these materials exhibit several interesting physical properties, such as ionic conduction, ion exchange, and others. Crystal growth, morphology, and grain size are factors influencing these physical properties. This book examines methods of synthesis of the most common crystalline materials and describes nucleation and crystal growth of various materials.

Crystallization of Organic Compounds

Author : Hsien-Hsin Tung
Publisher : John Wiley & Sons
ISBN 13 : 1119879469
Total Pages : 388 pages
Book Rating : 4.1/5 (198 download)

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Book Synopsis Crystallization of Organic Compounds by : Hsien-Hsin Tung

Download or read book Crystallization of Organic Compounds written by Hsien-Hsin Tung and published by John Wiley & Sons. This book was released on 2023-09-06 with total page 388 pages. Available in PDF, EPUB and Kindle. Book excerpt: Practical resource covering applications of crystallization principles with methodologies, case studies, and numerous industrial examples for emphasis Based on the authors' hands-on experiences as process engineers, through the use of case studies and examples of crystallization processes, ranging from laboratory development through manufacturing scale-up, Crystallization of Organic Compounds guides readers through the practical applications of crystallization and emphasizes strategies that have proven to be successful, enabling readers to avoid common pitfalls that can render standard procedures unsuccessful. Most chapters feature multiple examples that guide readers, step by step, through the crystallization of active pharmaceutical ingredients (APIs), including an analysis of the major methods of carrying out crystallization operations, their strengths and potential issues, as well as numerous examples of crystallization processes from development through manufacturing scale. Advancements in the field of crystallization have been integrated throughout the book in the newly revised Second Edition to ensure the content adequately reflects current state-of-the-art industrial know-hows and practice. The new edition also adds chapters addressing downstream operations after the crystallization, including filtration/washing and drying, together with industrial use cases. Crystallization of Organic Compounds includes detailed information on: Solubility and solid behavior, covering phase rule, polymorph, salt/coccrystals, chiral resolution and in-silico solubility prediction; and kinetics, covering seed, supersaturation, nucleation, crystal growth and model-based experimental design Critical issues in the crystallization practice, covering oiling out, seeding/wet-milling, agglomeration/aggregation, mixing scale-up and quality-by-design principles. Cooling, anti-solvent, evaporation and reactive crystallization process design, covering batch and continuous operations with industrial examples. Special applications, covering crystallization with ultrasound and computation fluid dynamics, and solid dispersion. With highly practical coverage of the subject, Crystallization of Organic Compounds is an essential resource for engineers and chemists involved with the development, scaling, or operation of crystallization process in the pharmaceutical and fine chemical industries, particularly those with degrees in chemical engineering and chemistry.

Crystallization

Author : J W Mullin
Publisher : Elsevier
ISBN 13 : 0080530117
Total Pages : 611 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Crystallization by : J W Mullin

Download or read book Crystallization written by J W Mullin and published by Elsevier. This book was released on 2001-05-09 with total page 611 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the first publication of this definitive work nearly 40 years ago, this fourth edition has been completely rewritten. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Incorporating all the recent developments and applications of crystallization technology, Crystallization gives clear accounts of the underlying principles, a review of the past and current research themes and guidelines for equipment and process design. This new edition introduces and enlarges upon such subjects as: Control and Separation of polymorphs and chiral crystals Micro- and macro-mixing and the use of computer fluid dynamics Seeding and secondary nucleation in batch crystallization processes Incorporation of upstream and downstream requirements into design procedures for crystallization plant Computer-aided molecular design and its use in crystal habit modifier selection Crystallization provides a comprehensive overview of the subject and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia. Crystallization is written with the precision and clarity of style that is John Mullin's hallmark - a special feature being the large number of appendices that provide relevant physical property data. Covers all new developments and trends in crystallization Comprehensive coverage of subject area

Crystallization

Author : Wolfgang Beckmann
Publisher : John Wiley & Sons
ISBN 13 : 3527327622
Total Pages : 370 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Crystallization by : Wolfgang Beckmann

Download or read book Crystallization written by Wolfgang Beckmann and published by John Wiley & Sons. This book was released on 2013-04-01 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.

Crystallization in Multiphase Polymer Systems

Author : Sabu Thomas
Publisher : Elsevier
ISBN 13 : 0128094311
Total Pages : 612 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Crystallization in Multiphase Polymer Systems by : Sabu Thomas

Download or read book Crystallization in Multiphase Polymer Systems written by Sabu Thomas and published by Elsevier. This book was released on 2017-09-15 with total page 612 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization in Multiphase Polymer Systems is the first book that explains in depth the crystallization behavior of multiphase polymer systems. Polymeric structures are more complex in nature than other material structures due to their significant structural disorder. Most of the polymers used today are semicrystalline, and the subject of crystallization is still one of the major issues relating to the performance of semicrystalline polymers in the modern polymer industry. The study of the crystallization processes, crystalline morphologies and other phase transitions is of great significance for the understanding the structure-property relationships of these systems. Crystallization in block copolymers, miscible blends, immiscible blends, and polymer composites and nanocomposites is thoroughly discussed and represents the core coverage of this book. The book critically analyzes the kinetics of nucleation and growth process of the crystalline phases in multi-component polymer systems in different length scales, from macro to nanoscale. Various experimental techniques used for the characterization of polymer crystallization process are discussed. Written by experts in the field of polymer crystallization, this book is a unique source and enables professionals and students to understand crystallization behavior in multiphase polymer systems such as block copolymers, polymer blends, composites and nanocomposites. Covers crystallization of multiphase polymer systems, including copolymers, blends and nanocomposites Features comprehensive, detailed information about the basic research, practical applications and new developments for these polymeric materials Analyzes the kinetics of nucleation and growth process of the crystalline phases in multi-component polymer systems in different length scales, from macro to nanoscale

Metal-Induced Crystallization

Author : Zumin Wang
Publisher : CRC Press
ISBN 13 : 9814463418
Total Pages : 317 pages
Book Rating : 4.8/5 (144 download)

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Book Synopsis Metal-Induced Crystallization by : Zumin Wang

Download or read book Metal-Induced Crystallization written by Zumin Wang and published by CRC Press. This book was released on 2015-01-28 with total page 317 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystalline semiconductors in the form of thin films are crucial materials for many modern, advanced technologies in fields such as microelectronics, optoelectronics, display technology, and photovoltaic technology. Crystalline semiconductors can be produced at surprisingly low temperatures (as low as 120C) by crystallization of amorphous semicon

Crystallization of Lipids

Author : Kiyotaka Sato
Publisher : John Wiley & Sons
ISBN 13 : 1118593928
Total Pages : 540 pages
Book Rating : 4.1/5 (185 download)

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Book Synopsis Crystallization of Lipids by : Kiyotaka Sato

Download or read book Crystallization of Lipids written by Kiyotaka Sato and published by John Wiley & Sons. This book was released on 2018-04-23 with total page 540 pages. Available in PDF, EPUB and Kindle. Book excerpt: An authoritative reference that contains the most up-to-date information knowledge, approaches, and applications of lipid crystals Crystallization of Lipids is a comprehensive resource that offers the most current and emerging knowledge, techniques and applications of lipid crystals. With contributions from noted experts in the field, the text covers the basic research of polymorphic structures, molecular interactions, nucleation and crystal growth and crystal network formation of lipid crystals which comprise main functional materials employed in food, cosmetic and pharmaceutical industry. The authors highlight trans-fat alternative and saturated-fat reduction technology to lipid crystallization. These two issues are the most significant challenges in the edible-application technology of lipids, and a key solution is lipid crystallization. The text focuses on the crystallization processes of lipids under various external influences of thermal fluctuation, ultrasound irradiation, shear, emulsification and additives. Designed to be practical, the book’s information can be applied to realistic applications of lipids to foods, cosmetic and pharmaceuticals. This authoritative and up-to-date guide: Highlights cutting-edge research tools designed to help analyse lipid crystallization with the most current and the conventional techniques Offers a thorough review of the information, techniques and applications of lipid crystals Includes contributions from noted experts in the field of lipid crystals Presents cutting-edge information on the topics of trans-fat alterative and saturated-fat reduction technology Written for research and development technologists as well as academics, this important resource contains research on lipid crystals which comprise the main functional materials employed in food, cosmetic and pharmaceutical industry.

Industrial Crystallization Process Monitoring and Control

Author : Angelo Chianese
Publisher : John Wiley & Sons
ISBN 13 : 3527645179
Total Pages : 253 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Industrial Crystallization Process Monitoring and Control by : Angelo Chianese

Download or read book Industrial Crystallization Process Monitoring and Control written by Angelo Chianese and published by John Wiley & Sons. This book was released on 2012-04-06 with total page 253 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallization is an important technique for separation and purification of substances as well as for product design in chemical, pharmaceutical and biotechnological process industries. This ready reference and handbook draws on research work and industrial practice of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges. First the instrumentation and techniques used to measure the crystal size distribution, the nucleation and solubility points, and the chemical composition of the solid and liquid phase are outlined. Then the main techniques adopted to control industrial crystallizers, starting from fundamental approaches to the most advanced ones, including the multivariable predictive control are described. An overview of the main crystallizer types is given with details of the main control schemes adopted in industry as well as the more suitable sensors and actuators.

The Handbook of Continuous Crystallization

Author : Nima Yazdanpanah
Publisher : Royal Society of Chemistry
ISBN 13 : 1839161310
Total Pages : 579 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis The Handbook of Continuous Crystallization by : Nima Yazdanpanah

Download or read book The Handbook of Continuous Crystallization written by Nima Yazdanpanah and published by Royal Society of Chemistry. This book was released on 2020-02-04 with total page 579 pages. Available in PDF, EPUB and Kindle. Book excerpt: Continuous crystallization is an area of intense research, with particular respect to the pharmaceutical industry and fine chemicals. Improvements in continuous crystallization technologies offer chemical industries significant financial gains, through reduced expenditure and operational costs, and consistent product quality. Written by well-known leaders in the field, The Handbook of Continuous Crystallization presents fundamental and applied knowledge, with attention paid to application and scaling up, and the burgeoning area of process intensification. Beginning with concepts around crystallization techniques and control strategies, the reader will learn about experimental methods and computational tools. Case studies spanning fine and bulk chemicals, the pharmaceutical industry, and employing new mathematical tools, put theory into context.