Characterization Of Plastic Bonded Explosives By Pyrolysis Gas Chromatography And Multivariate Data Analysis Development Of The Procedure Karakterisering Van Kunststof Gebonden Explosieven Met Pyrolyse Gaschromatografie En Multivariate Data Analyse Ontwikkeling Van De Procedure

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Characterization of Plastic Bonded Explosives by Pyrolysis-Gas Chromatography and Multivariate Data Analysis, Development of the Procedure (Karakterisering Van Kunststof Gebonden Explosieven Met Pyrolyse-gaschromatografie en Multivariate Data Analyse. Ontwikkeling Van de Procedure).

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ISBN 13 :
Total Pages : 33 pages
Book Rating : 4.:/5 (227 download)

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Book Synopsis Characterization of Plastic Bonded Explosives by Pyrolysis-Gas Chromatography and Multivariate Data Analysis, Development of the Procedure (Karakterisering Van Kunststof Gebonden Explosieven Met Pyrolyse-gaschromatografie en Multivariate Data Analyse. Ontwikkeling Van de Procedure). by :

Download or read book Characterization of Plastic Bonded Explosives by Pyrolysis-Gas Chromatography and Multivariate Data Analysis, Development of the Procedure (Karakterisering Van Kunststof Gebonden Explosieven Met Pyrolyse-gaschromatografie en Multivariate Data Analyse. Ontwikkeling Van de Procedure). written by and published by . This book was released on 1994 with total page 33 pages. Available in PDF, EPUB and Kindle. Book excerpt: A further development of the procedure based on pyrolysis-gas chromatography (Py-GC) for the characterization of plastic bonded explosives (PBX's) is described. After grinding, the PBX samples were pressed on a pyrolysis wire followed by Py-GC analysis. The peak areas obtained were normalized and submitted to multivariate data analysis. The use of principal component analysis (PCA) was tested on 5 samples which differed slightly in composition and age. The results were promising and showed that PCA is a powerful tool for the differentiation between PBX samples. The pressure by which the samples were pressed on the pyrolysis wire appeared to be an important parameter. This parameter was optimized together with the pyrolysis temperature and the amount of sample. The optimization experiment was carried out with 2 PBX samples which differed only in crosslink density. It turned out that it was difficult to find optima in the parameters resulting in a maximal difference between the 2 samples. The following settings of the parameters were selected: 5.2 tonnes, 75 mg and 610 C.

Characterization of Plastic Bonded Explosives by Pyrolysis-Gas Chromatography and Multivariate Data Analysis. Applications of the Procedure (Karakterisering Van Kunststof Gebonden Explosieven Met Pyrolyse-gaschromatografie en Multivariate Data Analyse. Toepassing Van de Procedure).

Download Characterization of Plastic Bonded Explosives by Pyrolysis-Gas Chromatography and Multivariate Data Analysis. Applications of the Procedure (Karakterisering Van Kunststof Gebonden Explosieven Met Pyrolyse-gaschromatografie en Multivariate Data Analyse. Toepassing Van de Procedure). PDF Online Free

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ISBN 13 :
Total Pages : 28 pages
Book Rating : 4.:/5 (227 download)

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Book Synopsis Characterization of Plastic Bonded Explosives by Pyrolysis-Gas Chromatography and Multivariate Data Analysis. Applications of the Procedure (Karakterisering Van Kunststof Gebonden Explosieven Met Pyrolyse-gaschromatografie en Multivariate Data Analyse. Toepassing Van de Procedure). by :

Download or read book Characterization of Plastic Bonded Explosives by Pyrolysis-Gas Chromatography and Multivariate Data Analysis. Applications of the Procedure (Karakterisering Van Kunststof Gebonden Explosieven Met Pyrolyse-gaschromatografie en Multivariate Data Analyse. Toepassing Van de Procedure). written by and published by . This book was released on 1994 with total page 28 pages. Available in PDF, EPUB and Kindle. Book excerpt: Applications of the developed procedure based on pyrolysis-gas chromatography (Py-GC) and principal component analysis (PCA) for the characterization of plastic bonded explosives (PBX's) are described. Due to difficulties with the commonly used normalization method a new normalization method was developed and applied in this investigation. The patterns in the score plots obtained after PCA of the Py-GC results appeared much clearer using this new method. PBX samples were examined on homogeneity, influence of the amount of antioxidant (Flexzone) and the crosslink density. It appears that PBX's were inhomogeneous despite a thorough mixing of the constituents during the preparation. Aging experiments were performed on samples which differed in the amount of Flexzone and in the crosslink density. As more Flexzone was added the change in the pattern of the GC-peaks became less. No relation could be found between the stability of PBX's and the crosslink density. Finally, a comparison was made between Dutch samples and samples from the UK and Norway. Small differences were observed between the samples from the three nations.

Scientific and Technical Aerospace Reports

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ISBN 13 :
Total Pages : 376 pages
Book Rating : 4.:/5 (3 download)

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Book Synopsis Scientific and Technical Aerospace Reports by :

Download or read book Scientific and Technical Aerospace Reports written by and published by . This book was released on 1995 with total page 376 pages. Available in PDF, EPUB and Kindle. Book excerpt: Lists citations with abstracts for aerospace related reports obtained from world wide sources and announces documents that have recently been entered into the NASA Scientific and Technical Information Database.

Government Reports Announcements & Index

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ISBN 13 :
Total Pages : 878 pages
Book Rating : 4.3/5 (243 download)

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Book Synopsis Government Reports Announcements & Index by :

Download or read book Government Reports Announcements & Index written by and published by . This book was released on 1995 with total page 878 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition)

Author : Peter Kusch
Publisher : World Scientific
ISBN 13 : 1800613008
Total Pages : 383 pages
Book Rating : 4.8/5 (6 download)

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Book Synopsis Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) by : Peter Kusch

Download or read book Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) written by Peter Kusch and published by World Scientific. This book was released on 2023-08-28 with total page 383 pages. Available in PDF, EPUB and Kindle. Book excerpt: Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.

Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials

Author : Peter Kusch
Publisher : World Scientific
ISBN 13 : 1786345773
Total Pages : 267 pages
Book Rating : 4.7/5 (863 download)

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Book Synopsis Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials by : Peter Kusch

Download or read book Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials written by Peter Kusch and published by World Scientific. This book was released on 2018-10-08 with total page 267 pages. Available in PDF, EPUB and Kindle. Book excerpt: The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.

Pyrolysis - GC/MS Data Book of Synthetic Polymers

Author : Shin Tsuge
Publisher : Elsevier
ISBN 13 : 0444538933
Total Pages : 405 pages
Book Rating : 4.4/5 (445 download)

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Book Synopsis Pyrolysis - GC/MS Data Book of Synthetic Polymers by : Shin Tsuge

Download or read book Pyrolysis - GC/MS Data Book of Synthetic Polymers written by Shin Tsuge and published by Elsevier. This book was released on 2011-08-02 with total page 405 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. - Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification - Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique - All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification - Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample

Analytical Pyrolysis

Author : C.E.R. Jones
Publisher : Elsevier
ISBN 13 : 0444601406
Total Pages : 435 pages
Book Rating : 4.4/5 (446 download)

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Book Synopsis Analytical Pyrolysis by : C.E.R. Jones

Download or read book Analytical Pyrolysis written by C.E.R. Jones and published by Elsevier. This book was released on 2012-12-02 with total page 435 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Pyrolysis presents the Proceedings of the Third International Symposium on Analytical Pyrolysis, held in Amsterdam on September 7-9, 1976. It looks at newly emergent techniques in analytical pyrolysis, including pyrolysis mass spectrometry, gas chromatography, thin-layer chromatography, and pyrolysis-gas liquid chromatography. The book also covers topics ranging from automation and microbiology to forensic science and pharmacology, reproducibility and specificity, biochemistry, laser-induced pyrolysis, pyrolytic reaction mechanisms, and polymers. Comprised of 50 chapters, this book begins with a discussion of automatic analysis of tire rubber blends using computer-linked pyrolysis gas chromatography, thermal procedures in coupling with thin-layer chromatography, the role of pyrolysis-gas liquid chromatography in biomedical studies, and the identification of microorganisms by pyrolysis gas-liquid chromatography. It then examines forensic applications of analytical pyrolysis techniques, structure and degradation behavior of synthetic polymers using pyrolysis in combination with field ion mass spectrometry, determination of polysaccharides in fulvic acids by pyrolysis gas chromatography, and application of Curie-point pyrolysis mass spectrometry in fungal taxonomy. The reader is also introduced to pyrolysis mass spectrometry of model compounds labeled with stable isotopes, the use of pyrolysis/gas chromatography to determine the quality of porous polymers of styrene cross-linked with divinyl benzene, and application of pyrohydrolysis for a rapid and accurate determination of halides in silicate rocks and minerals. This volume will benefit students, researchers, chemists, and scientists working in the field of analytical pyrolysis.

Analytical Pyrolysis Handbook

Author : Karen D. Sam
Publisher : CRC Press
ISBN 13 : 0429574924
Total Pages : 354 pages
Book Rating : 4.4/5 (295 download)

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Book Synopsis Analytical Pyrolysis Handbook by : Karen D. Sam

Download or read book Analytical Pyrolysis Handbook written by Karen D. Sam and published by CRC Press. This book was released on 2021-03-23 with total page 354 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical pyrolysis allows scientists to use routine laboratory instrumentation for analyzing complex, opaque, or insoluble samples more effectively than other analytical techniques alone. Analytical Pyrolysis Handbook, Third Edition is a practical guide to the application of pyrolysis techniques to various samples and sample types for a diversity of fields including microbiology, forensic science, industrial research, and environmental analysis. The much-anticipated third edition incorporates recent technological advances that increase the technique’s sensitivity to trace elements, improve its reproducibility, and expand its applicability. The book reviews the types of instrumentation available to perform pyrolysis and offers guidance for interfacing instruments and integrating other analytical techniques, including gas chromatography and mass spectrometry. Fully updated with new sample pyrograms, figures, references, and real-world examples, this edition also highlights new areas of application including cultural materials, forensic analysis, and environmental studies. This book illustrates how the latest advances make pyrolysis a practical, cost-effective, reliable, and flexible alternative for increasingly complex sample analyses. Analytical Pyrolysis Handbook, Third Edition is an essential, one-stop guide for determining if pyrolysis meets application-specific needs as well as performing pyrolysis and handling the data obtained.

Pyrolysis and Combustion Studies of Polymers by Gas Chromatography and Thermal Analysis

Author : Matti Elomaa
Publisher :
ISBN 13 : 9789516532298
Total Pages : 55 pages
Book Rating : 4.5/5 (322 download)

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Book Synopsis Pyrolysis and Combustion Studies of Polymers by Gas Chromatography and Thermal Analysis by : Matti Elomaa

Download or read book Pyrolysis and Combustion Studies of Polymers by Gas Chromatography and Thermal Analysis written by Matti Elomaa and published by . This book was released on 1991 with total page 55 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Pyrolysis and GC in Polymer Analysis

Author : Michael N. Liebman
Publisher : CRC Press
ISBN 13 : 9780824771874
Total Pages : 576 pages
Book Rating : 4.7/5 (718 download)

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Book Synopsis Pyrolysis and GC in Polymer Analysis by : Michael N. Liebman

Download or read book Pyrolysis and GC in Polymer Analysis written by Michael N. Liebman and published by CRC Press. This book was released on 1984-12-28 with total page 576 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Polymer Characterization

Author : Clara D. Craver
Publisher :
ISBN 13 : 9780608035086
Total Pages : 808 pages
Book Rating : 4.0/5 (35 download)

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Book Synopsis Polymer Characterization by : Clara D. Craver

Download or read book Polymer Characterization written by Clara D. Craver and published by . This book was released on 1983 with total page 808 pages. Available in PDF, EPUB and Kindle. Book excerpt: