Analysis And Fractionation Of Polymers

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Polymer Fractionation

Author : Frieder Francuskiewicz
Publisher : Springer Science & Business Media
ISBN 13 : 3642787045
Total Pages : 230 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Polymer Fractionation by : Frieder Francuskiewicz

Download or read book Polymer Fractionation written by Frieder Francuskiewicz and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 230 pages. Available in PDF, EPUB and Kindle. Book excerpt: Fractionation of polymers via solubility has been a well known method in polymer characterization for a long time. The original object of analytical fractionations, the determination of the molecular weight distribution, is nowadays achieved more efficiently and conveniently by chromatographic methods. However, fractionation procedures, which were developed in great diversity, remain up~to-date and essential for obtaining preparative fractions with narrow distributions. Such fractions are wanted increasingly for the investigation of true structure-property relationships which are mostly influ~ enced by distributions of molecular weight or other parameters such as branching or chemical composition. Literature on the field of polymer fractionation is extensive and several reviews exist. However, there is a lack of systematically methodical instruc tions for carrying-out of diverse fractionation procedures. This volume repre sents an attempt to reduce this deficiency and is focussed on practical aspects of fractionation procedures. This laboratory manual is intended for polymer chemists, physicists, and technicians, for students of polymer science, and skilled laboratory assistants, all of whom are not dealing directly with fractionation but are in need of fractions to carry out further investigations.

Analysis and Fractionation of Polymers

Author : American Chemical Society
Publisher :
ISBN 13 :
Total Pages : 332 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Analysis and Fractionation of Polymers by : American Chemical Society

Download or read book Analysis and Fractionation of Polymers written by American Chemical Society and published by . This book was released on 1965 with total page 332 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Light Scattering, Size Exclusion Chromatography and Asymmetric Flow Field Flow Fractionation

Author : Stepan Podzimek
Publisher : John Wiley & Sons
ISBN 13 : 111810272X
Total Pages : 325 pages
Book Rating : 4.1/5 (181 download)

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Book Synopsis Light Scattering, Size Exclusion Chromatography and Asymmetric Flow Field Flow Fractionation by : Stepan Podzimek

Download or read book Light Scattering, Size Exclusion Chromatography and Asymmetric Flow Field Flow Fractionation written by Stepan Podzimek and published by John Wiley & Sons. This book was released on 2011-04-20 with total page 325 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive, practical approach to three powerful methods of polymer analysis and characterization This book serves as a complete compendium of three important methods widely used for the characterization of synthetic and natural polymers—light scattering, size exclusion chromatography (SEC), and asymmetric flow field flow fractionation (A4F). Featuring numerous up-to-date examples of experimental results obtained by light scattering, SEC, and A4F measurements, Light Scattering, Size Exclusion Chromatography and Asymmetric Flow Field Flow Fractionation takes an all-in-one approach to deliver a complete and thorough explanation of the principles, theories, and instrumentation needed to characterize polymers from the viewpoint of their molar mass distribution, size, branching, and aggregation. This comprehensive resource: Is the only book gathering light scattering, size exclusion chromatography, and asymmetric flow field flow fractionation into a single text Systematically compares results of size exclusion chromatography with results of asymmetric flow field flow fractionation, and how these two methods complement each other Provides in-depth guidelines for reproducible and correct determination of molar mass and molecular size of polymers using SEC or A4F coupled with a multi-angle light scattering detector Offers a detailed overview of the methodology, detection, and characterization of polymer branching Light Scattering, Size Exclusion Chromatography and Asymmetric Flow Field Flow Fractionation should be of great interest to all those engaged in the polymer analysis and characterization in industrial and university research, as well as in manufacturing quality control laboratories. Both beginners and experienced can confidently rely on this volume to confirm their own understanding or to help interpret their results.

Practical Polymer Analysis

Author : T.R. Crompton
Publisher : Springer Science & Business Media
ISBN 13 : 1461528747
Total Pages : 841 pages
Book Rating : 4.4/5 (615 download)

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Book Synopsis Practical Polymer Analysis by : T.R. Crompton

Download or read book Practical Polymer Analysis written by T.R. Crompton and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 841 pages. Available in PDF, EPUB and Kindle. Book excerpt: The aim of this book is to familiarize the reader with the practical aspects of polymer analysis. A wealth of practical detail, including some detailed methods is included. The book covers not only the analysis of the main types of polymers and copolymers now in use commercially, but also the analysis of minor non-polymeric components of the polymer formulation, whether they be deliberately added, such as processing additives, or whether they occur adventitiously, such as moisture and residual monomers and solvent. A broad scheme for the examination of polymers is discussed in Chapter 2. Practically all of the major newer analytical techniques and many of the older classical techniques, have been used to examine polymers and their additive systems. As so many different polymers are now used commercially it is also advisable when attempting to identify a polymer to classify it by first separating it into pure polymeric and gross non polymeric fractions (Chapter Z) and then carrying out at least a qualitative elemental analysis and possible a quantitative analysis (Chapters 3 and 4) and then in some cases, depending on the elements found, to carry out functional group analysis (Chapters 6 and 9).

Polymer Analysis/Polymer Theory

Author : Akihiro Abe
Publisher : Springer Science & Business Media
ISBN 13 : 9783540255482
Total Pages : 328 pages
Book Rating : 4.2/5 (554 download)

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Book Synopsis Polymer Analysis/Polymer Theory by : Akihiro Abe

Download or read book Polymer Analysis/Polymer Theory written by Akihiro Abe and published by Springer Science & Business Media. This book was released on 2005-09-29 with total page 328 pages. Available in PDF, EPUB and Kindle. Book excerpt: This series presents critical reviews of the present and future trends in polymer and biopolymer science including chemistry, physical chemistry, physics and materials science. It is addressed to all scientists at universities and in industry who wish to keep abreast of advances in the topics covered. Impact Factor Ranking: Always number one in Polymer Science. More information as well as the electronic version of the whole content available at: www.springerlink.com

Molecular Characterization of Polymers

Author : Muhammad Imran Malik
Publisher : Elsevier
ISBN 13 : 012822598X
Total Pages : 670 pages
Book Rating : 4.1/5 (282 download)

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Book Synopsis Molecular Characterization of Polymers by : Muhammad Imran Malik

Download or read book Molecular Characterization of Polymers written by Muhammad Imran Malik and published by Elsevier. This book was released on 2021-03-09 with total page 670 pages. Available in PDF, EPUB and Kindle. Book excerpt: Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. - Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity - Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material - Establishes a strong link between basic principles, characterization techniques, and real-life applications

HPLC of Polymers

Author : Harald Pasch
Publisher : Springer Science & Business Media
ISBN 13 : 3642582656
Total Pages : 234 pages
Book Rating : 4.6/5 (425 download)

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Book Synopsis HPLC of Polymers by : Harald Pasch

Download or read book HPLC of Polymers written by Harald Pasch and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 234 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymers are mainly characterized by molar mass, chemical composition, functionality and architecture. The determination of the complex structure of polymers by chromatographic and spectroscopic methods is one of the major concerns of polymer analysis and characterization. This lab manual describes the experimental approach to the chromatographic analysis of polymers. Different chromatographic methods, their theoretical background, equipment, experimental procedures and applications are discussed. The book will enable polymer chemists, physicists and material scientists as well as students of macromolecular and analytical science to optimize chromatographic conditions for a specific separation problem. Special emphasis is given to the description of applications for homo- and copolymers and polymer blends.

Characterization and Analysis of Polymers

Author : Wiley
Publisher : John Wiley & Sons
ISBN 13 : 0470233001
Total Pages : 987 pages
Book Rating : 4.4/5 (72 download)

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Book Synopsis Characterization and Analysis of Polymers by : Wiley

Download or read book Characterization and Analysis of Polymers written by Wiley and published by John Wiley & Sons. This book was released on 2008-02-08 with total page 987 pages. Available in PDF, EPUB and Kindle. Book excerpt: Based on Wiley's renowned Encyclopedia of Polymer Science and Technology, this book provides coverage of key methods of characterization of the physical and chemical properties of polymers, including atomic force microscopy, chromatographic methods, laser light scattering, nuclear magnetic resonance, and thermal analysis, among others. Written by prominent scholars from around the world, this reference presents over twenty-five self -contained articles on the most used analytical techniques currently practiced in polymer science.

Additives in Polymers

Author : Jan C. J. Bart
Publisher : John Wiley & Sons
ISBN 13 : 0470012056
Total Pages : 836 pages
Book Rating : 4.4/5 (7 download)

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Book Synopsis Additives in Polymers by : Jan C. J. Bart

Download or read book Additives in Polymers written by Jan C. J. Bart and published by John Wiley & Sons. This book was released on 2005-04-08 with total page 836 pages. Available in PDF, EPUB and Kindle. Book excerpt: This industrially relevant resource covers all established and emerging analytical methods for the deformulation of polymeric materials, with emphasis on the non-polymeric components. Each technique is evaluated on its technical and industrial merits. Emphasis is on understanding (principles and characteristics) and industrial applicability. Extensively illustrated throughout with over 200 figures, 400 tables, and 3,000 references.

Field-Flow Fractionation Handbook

Author : Martin E. Schimpf
Publisher : John Wiley & Sons
ISBN 13 : 9780471184300
Total Pages : 618 pages
Book Rating : 4.1/5 (843 download)

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Book Synopsis Field-Flow Fractionation Handbook by : Martin E. Schimpf

Download or read book Field-Flow Fractionation Handbook written by Martin E. Schimpf and published by John Wiley & Sons. This book was released on 2000-08-02 with total page 618 pages. Available in PDF, EPUB and Kindle. Book excerpt: Field flow fractionation (FFF) is an emerging separation technique, which has been proven successful in the analysis of pharmaceuticals, biotechnology products, polymers, soils, and foods, among others. In this book, Martin Schimpf joins forces with Karin Caldwell and J. Calvin Giddings, two of the primary developers of this technique, to bring you the first comprehensive, one-stop reference on the technique.

Analytical Methods for Polymer Characterization

Author : Rui Yang
Publisher : CRC Press
ISBN 13 : 135121313X
Total Pages : 287 pages
Book Rating : 4.3/5 (512 download)

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Book Synopsis Analytical Methods for Polymer Characterization by : Rui Yang

Download or read book Analytical Methods for Polymer Characterization written by Rui Yang and published by CRC Press. This book was released on 2018-01-09 with total page 287 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Methods for Polymer Characterization presents a collection of methods for polymer analysis. Topics include chromatographic methods (gas chromatography, inverse gas chromatography, and pyrolysis gas chromatography), mass spectrometry, spectroscopic methods (ultraviolet-visible spectroscopy, infrared spectroscopy, Raman spectroscopy, and nuclear magnetic resonance), thermal analysis (differential scanning calorimetry and thermogravimetry), microscopy methods (scanning electron microscopy, transmission electron microscopy, and atomic force microscopy), and x-ray diffraction. The author also discusses mechanical and dynamic mechanical properties.

Spectroscopic Techniques for Polymer Characterization

Author : Yukihiro Ozaki
Publisher : John Wiley & Sons
ISBN 13 : 3527830324
Total Pages : 500 pages
Book Rating : 4.5/5 (278 download)

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Book Synopsis Spectroscopic Techniques for Polymer Characterization by : Yukihiro Ozaki

Download or read book Spectroscopic Techniques for Polymer Characterization written by Yukihiro Ozaki and published by John Wiley & Sons. This book was released on 2021-10-29 with total page 500 pages. Available in PDF, EPUB and Kindle. Book excerpt: An insightful exploration of cutting-edge spectroscopic techniques in polymer characterization In Spectroscopic Techniques for Polymer Characterization: Methods, Instrumentation, Applications, a team of distinguished chemists delivers a comprehensive exploration of the vast potential of spectroscopic characterization techniques in polymer research. The book offers a concise outline of the principles, advantages, instrumentation, experimental techniques, and noteworthy applications of cutting-edge spectroscopy. Covering a wide range of polymers, from nylon to complex polymeric nanocomposites, the author presents recent developments in polymer science to polymer, analytical, and material chemists, assisting them in keeping track of the progress in modern spectroscopy. Spectroscopic Techniques for Polymer Characterization contains contributions from pioneers in modern spectroscopic techniques from around the world. The included materials bridge the gap between spectroscopists, polymer scientists, and engineers in academia and industry. The book also offers: A thorough introduction to the progress in spectroscopic techniques, including polymer spectroscopy and near-infrared spectroscopy Comprehensive explorations of topical polymers studied by spectroscopy, including polymer thin films, fluoropolymers, polymer solutions, conductive polymers Practical discussions of infrared imaging, near-infrared imaging, two-dimensional correlation spectroscopy, and far-ultraviolet spectroscopy In-depth examinations of spectroscopic studies of weak hydrogen bonding in polymers Spectroscopic Techniques for Polymer Characterization: Methods, Instrumentation, Applications is a must-read reference for polymer, analytical, and physical chemists, as well as materials scientists and spectroscopists seeking a one-stop resource for polymer characterization using spectroscopic analyses.

Polyolefin Characterization

Author : Joao B. P. Soares
Publisher : John Wiley & Sons
ISBN 13 : 9783527321926
Total Pages : 184 pages
Book Rating : 4.3/5 (219 download)

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Book Synopsis Polyolefin Characterization by : Joao B. P. Soares

Download or read book Polyolefin Characterization written by Joao B. P. Soares and published by John Wiley & Sons. This book was released on 2007 with total page 184 pages. Available in PDF, EPUB and Kindle. Book excerpt: The First International Conference on Polyolefin Characterization (ICPC) held in Houston, Texas, in October 2006, was organized to fill the important industrial and academic need for a discussion forum on the characterization and fractionation techniques of polyolefins. These proceedings represent an excellent and up-to-date overview of recent advances in this important area, providing much information and facts that are not available elsewhere. The result is a collection of top quality contributions by experienced editors and international authors on such fields as separation and fractionation, high throughput processes, thermal and crystallinity analysis, spectroscopy and rheology. Equally of high interest for the polymer industry.

Modern Methods of Polymer Characterization

Author : Howard G. Barth
Publisher : John Wiley & Sons
ISBN 13 : 9780471828143
Total Pages : 582 pages
Book Rating : 4.8/5 (281 download)

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Book Synopsis Modern Methods of Polymer Characterization by : Howard G. Barth

Download or read book Modern Methods of Polymer Characterization written by Howard G. Barth and published by John Wiley & Sons. This book was released on 1991-09-03 with total page 582 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents the methods used for characterization of polymers. In addition to theory and basic principles, the instrumentation and apparatus necessary for methods used to study the kinetic and thermodynamic interactions of a polymer with its environment are covered in detail. Some of the methods examined include polymer separations and characterization by size exclusion and high performance chromatography, inverse gas chromatography, osmometry, viscometry, ultracentrifugation, light scattering and spectroscopy.

Polymer Characterisation

Author : B.J. Hunt
Publisher : Springer Science & Business Media
ISBN 13 : 9401121605
Total Pages : 376 pages
Book Rating : 4.4/5 (11 download)

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Book Synopsis Polymer Characterisation by : B.J. Hunt

Download or read book Polymer Characterisation written by B.J. Hunt and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 376 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymers continue to play an ever increasing role in the modern world. In fact it is quite inconceivable to most people that we could ever have existed of the increased volume and variety of materials without them. As a result currently available, and the diversity of their application, characterisation has become an essential requirement of industrial and academic laboratories in volved with polymeric materials. On the one hand requirements may come from polymer specialists involved in the design and synthesis of new materials who require a detailed understanding of the relationship between the precise molecular architecture and the properties of the polymer in order to improve its capabilities and range of applications. On the other hand, many analysts who are not polymer specialists are faced with the problems of analysing and testing a wide range of polymeric materials for quality control or material specification purposes. We hope this book will be a useful reference for all scientists and techno or industrial laboratories, logists involved with polymers, whether in academic and irrespective of their scientific discipline. We have attempted to include in one volume all of the most important techniques. Obviously it is not possible to do this in any great depth but we have encouraged the use of specific examples to illustrate the range of possibilities. In addition numerous references are given to more detailed texts on specific subjects, to direct the reader where appropriate. The book is divided into II chapters.

Polymer Fractionation

Author : Manfred J. R. Cantow
Publisher : Elsevier
ISBN 13 : 1483271706
Total Pages : 540 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis Polymer Fractionation by : Manfred J. R. Cantow

Download or read book Polymer Fractionation written by Manfred J. R. Cantow and published by Elsevier. This book was released on 2013-10-22 with total page 540 pages. Available in PDF, EPUB and Kindle. Book excerpt: Polymer Fractionation focuses on the processes, reactions, and transformations involved in polymer fractionation, including chromatography, titration, and sedimentation. The selection first offers information on theoretical considerations and fractional precipitation. Topics include polydispersity of high polymers, phase relations for polydisperse systems, fractionation theory and efficiency, and fractionation by solvent evaporation. The manuscript then takes a look at fractional solution, chromatographic fractionation, and gel permeation chromatography. The book elaborates on thermal diffusion and turbidimetric titration, as well as methods of fractionation, studies of the variables, outline of the method and range of application, and elaboration of the method. The text then ponders on sedimentation, isothermal diffusion, and summative fractionation. Discussions focus on mathematical interpretation of summative data, experimental methods for the determination of diffusion constants, and methods for the determination of the diffusion coefficient distribution. The selection is a valuable source of information for readers interested in polymer fractionation.

Characterization of Polymer Blends

Author : Sabu Thomas
Publisher : John Wiley & Sons
ISBN 13 : 3527331530
Total Pages : 972 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Characterization of Polymer Blends by : Sabu Thomas

Download or read book Characterization of Polymer Blends written by Sabu Thomas and published by John Wiley & Sons. This book was released on 2015-02-09 with total page 972 pages. Available in PDF, EPUB and Kindle. Book excerpt: Filling the gap for a reference dedicated to the characterization of polymer blends and their micro and nano morphologies, this book provides comprehensive, systematic coverage in a one-stop, two-volume resource for all those working in the field. Leading researchers from industry and academia, as well as from government and private research institutions around the world summarize recent technical advances in chapters devoted to their individual contributions. In so doing, they examine a wide range of modern characterization techniques, from microscopy and spectroscopy to diffraction, thermal analysis, rheology, mechanical measurements and chromatography. These methods are compared with each other to assist in determining the best solution for both fundamental and applied problems, paying attention to the characterization of nanoscale miscibility and interfaces, both in blends involving copolymers and in immiscible blends. The thermodynamics, miscibility, phase separation, morphology and interfaces in polymer blends are also discussed in light of new insights involving the nanoscopic scale. Finally, the authors detail the processing-morphology-property relationships of polymer blends, as well as the influence of processing on the generation of micro and nano morphologies, and the dependence of these morphologies on the properties of blends. Hot topics such as compatibilization through nanoparticles, miscibility of new biopolymers and nanoscale investigations of interfaces in blends are also addressed. With its application-oriented approach, handpicked selection of topics and expert contributors, this is an outstanding survey for anyone involved in the field of polymer blends for advanced technologies.