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Download or read book ACTIVE METAL REDUCTION OF PLUTONIUM TRICHLORIDE. written by and published by . This book was released on 1960 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: The reduction characteristics of plutonium trichloride are investigated. A flowsheet for batch reduction with Ca is included. (J.R.D.).
Download or read book PLUTONIUM TRICHLORIDE written by and published by . This book was released on 1953 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Batches of plutonium dioxide were chlorinated by reaction with phosgene or carbon tetrachloride. Plutonium trichloride prepared by either method can be reduced to the metal in an hermetically sealed bomb by reaction with calcium. It has been demonstrated that a method for the reduction of plutonium trichloride to the metal without the use of a booster can be developed. Soluble plutonium in slag and crucible waste can be precipitated as the hydroxide and washed essentially free of chloride contamination. The concentrated nitric acid solution from dissolution of plutonium hydroxide and other solids contains less than 75 ppm chloride. Of the materials tested the Hastelloy alloys A, B, and C were found to be the most resistant to phosgene corrosion. The corrosion of these alloys was found to lie between 1 x 10−4 and 2 x 10−4 in. per month at 300 deg C and between 1 x 10−3 in. per month at 450 deg C. The logarithm of the corrosion rate plotted as a function of the temperature appears to be linear over the temperature range of 300 to 550 deg C. Above 550 deg C the corrosion rate of all materials tested is excessive. (auth).
Download or read book Plutonium Metal and Alloy Preparation by Molten Chloride Reduction written by and published by . This book was released on 1984 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Satisfactory reduction of molten plutonium trichloride (pure and in combination with 20 wt % sodium chloride) by calcium, lanthanum, and cerium has been demonstrated on the 10-g scale. The yields were satisfactory for this scale of operation, and it is indicated that these reductions may be useful for large-scale operations. Significant separations of plutonium from rare earth impurities was demonstrated for lanthanum and cerium reductions. Preparation of plutonium-cerium and plutonium-cerium-cobalt alloys during reduction was also demonstrated.
Author : M. H. Curtis
Publisher :
ISBN 13 :
Total Pages : 116 pages
Book Rating : 4.3/5 (91 download)
Download or read book Continuous Electrowinning of Plutonium Metal written by M. H. Curtis and published by . This book was released on 1964 with total page 116 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Major C. Thompson
Publisher :
ISBN 13 :
Total Pages : 16 pages
Book Rating : 4.3/5 (91 download)
Download or read book Reduction of Plutonium Dioxide to Plutonium Metal written by Major C. Thompson and published by . This book was released on 1965 with total page 16 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Rowland E. Felt
Publisher :
ISBN 13 :
Total Pages : 28 pages
Book Rating : 4.3/5 (91 download)
Download or read book A Pyrochemical Process for the Reduction of Plutonium Dioxide to Metal written by Rowland E. Felt and published by . This book was released on 1969 with total page 28 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author :
Publisher :
ISBN 13 :
Total Pages : 726 pages
Book Rating : 4.3/5 (91 download)
Download or read book Reactor Fuel Processing written by and published by . This book was released on 1963 with total page 726 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Metallurgical Society of AIME.
Publisher :
ISBN 13 :
Total Pages : 332 pages
Book Rating : 4.3/5 (91 download)
Download or read book Extractive and Physical Metallurgy of Plutonium and Its Alloys written by Metallurgical Society of AIME. and published by . This book was released on 1960 with total page 332 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book REDUCTION OF PLUTONIUM COMPOUNDS TO PLUTONIUM METAL. written by and published by . This book was released on 1964 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: A survey was made of the literature which was published on the reduction of plutonium compounds to plutonium metal between 1950 and April 1963. This report is a summary of the information which was gathered during the survey. (auth).
Author : W. Z. Wade
Publisher :
ISBN 13 :
Total Pages : 0 pages
Book Rating : 4.:/5 (972 download)
Download or read book The Production of Plutonium Metal by Direct Reduction of the Oxide written by W. Z. Wade and published by . This book was released on 1968 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author :
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ISBN 13 :
Total Pages : 11 pages
Book Rating : 4.:/5 (683 download)
Download or read book Dehydration of Plutonium Trichloride Hydrate written by and published by . This book was released on 1991 with total page 11 pages. Available in PDF, EPUB and Kindle. Book excerpt: A process of preparing anhydrous actinide metal trichlorides of plutonium or neptunium by reacting an aqueous solution of an actinide metal trichloride selected from the group consisting of plutonium trichloride or neptunium trichloride with a reducing agent capable of converting the actinide metal from an oxidation state of +4 to +3 in a resultant solution, evaporating essentially all the solvent from the resultant solution to yield an actinide trichloride hydrate material, dehydrating the actinide trichloride hydrate material by heating the material in admixture with excess thionyl chloride, and recovering anhydrous actinide trichloride is provided.
Download or read book REDUCTION OF PLUTONIUM DIOXIDE TO PLUTONIUM METAL. written by and published by . This book was released on 1965 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Oswald J. Wick
Publisher :
ISBN 13 :
Total Pages : 474 pages
Book Rating : 4.3/5 (91 download)
Download or read book Plutonium Handbook written by Oswald J. Wick and published by . This book was released on 1967 with total page 474 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author :
Publisher :
ISBN 13 :
Total Pages : 1472 pages
Book Rating : 4.3/5 (91 download)
Download or read book Nuclear Science Abstracts written by and published by . This book was released on 1972 with total page 1472 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author :
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ISBN 13 :
Total Pages : 2180 pages
Book Rating : 4.0/5 ( download)
Download or read book U.S. Government Research Reports written by and published by . This book was released on 1964 with total page 2180 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Dehydration of Plutonium Or Neptunium Trichloride Hydrate written by and published by . This book was released on 1992 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: A process of preparing anhydrous actinide metal trichlorides of plutonium or neptunium by reacting an aqueous solution of an actinide metal trichloride selected from the group consisting of plutonium trichloride or neptunium trichloride with a reducing agent capable of converting the actinide metal from an oxidation state of +4 to +3 in a resultant solution, evaporating essentially all the solvent from the resultant solution to yield an actinide trichloride hydrate material, dehydrating the actinide trichloride hydrate material by heating the material in admixture with excess thionyl chloride, and recovering anhydrous actinide trichloride is provided.
Author : Charles Allen Thomas
Publisher :
ISBN 13 :
Total Pages : 276 pages
Book Rating : 4.3/5 (91 download)
Download or read book The Chemistry, Purification and Metallurgy of Plutonium written by Charles Allen Thomas and published by . This book was released on 1944 with total page 276 pages. Available in PDF, EPUB and Kindle. Book excerpt:
