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The Development Of Diode Laser Infrared Absorption Spectroscopy As A Plasma Diagnostic
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Book Synopsis The Development of Diode Laser Infrared Absorption Spectroscopy as a Plasma Diagnostic by : Robert Leslie McClain
Download or read book The Development of Diode Laser Infrared Absorption Spectroscopy as a Plasma Diagnostic written by Robert Leslie McClain and published by . This book was released on 1991 with total page 494 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis New Enhanced Sensitivity Infrared Laser Spectroscopy Techniques Applied to Reactive Plasmas and Trace Gas Detection by : Stefan Welzel
Download or read book New Enhanced Sensitivity Infrared Laser Spectroscopy Techniques Applied to Reactive Plasmas and Trace Gas Detection written by Stefan Welzel and published by Logos Verlag Berlin GmbH. This book was released on 2009 with total page 198 pages. Available in PDF, EPUB and Kindle. Book excerpt: Infrared laser absorption spectroscopy (IRLAS) employing both tuneable diode and quantum cascade lasers (TDLs, QCLs) has been applied with both high sensitivity and high time resolution to plasma diagnostics and trace gas measurements. TDLAS combined with a conventional White type multiple pass cell was used to detect up to 13 constituent molecular species in low pressure Ar/H2/N2/O2 and Ar/CH4/N2/O2 microwave discharges, among them the main products such as H2O, NH3, NO and CO, HCN respectively. The hydroxyl radical has been measured in the mid infrared (MIR) spectral range in-situ in both plasmas yielding number densities of between 1011 ... 1012 cm-3. Strong indications of surface dominated formation of either NH3 or N2O and NO were found in the H2-N2-O2 system. In methane containing plasmas a transition between deposition and etching conditions and generally an incomplete oxidation of the precursor were observed. The application of QCLs for IRLAS under low pressure conditions employing the most common tuning approaches has been investigated in detail. A new method of analysing absorption features quantitatively when the rapid passage effect is present is proposed. If power saturation is negligible, integrating the undisturbed half of the line profile yields accurate number densities without calibrating the system. By means of a time resolved analysis of individual chirped QCL pulses the main reasons for increased effective laser line widths could be identified. Apart from the well-known frequency down chirp non-linear absorption phenomena and bandwidth limitations of the detection system may significantly degrade the performance and accuracy of inter pulse spectrometers. The minimum analogue bandwidth of the entire system should normally not fall below 250 MHz. QCLAS using pulsed lasers has been used for highly time resolved measurements in reactive plasmas for the first time enabling a time resolution down to about 100 ns to be achieved. A temperature increase of typically less than 50 K has been established for pulsed DC discharges containing Ar/N2 and traces of NO. The main NO production and depletion reactions have been identified from a comparison of model calculations and time resolved measurements in plasma pulses of up to 100 ms. Considerable NO struction is observed after 5 ... 10 ms due to the impact of N atoms. Finally, thermoelectrically cooled pulsed and continuous wave (cw) QCLs have been employed for high finesse cavity absorption spectroscopy in the MIR. Cavity ring down spectroscopy (CRDS) has been performed with pulsed QCLs and was found to be limited by the intrinsic frequency chirp of the laser suppressing an efficient intensity build-up inside the cavity. Consequently the accuracy and advantage of an absolute internal absorption calibration is not achievable. A room temperature cw QCL was used in a complementary cavity enhanced absorption spectroscopy (CEAS) configuration which was equipped with different cavities of up to 1.3 m length. This spectrometer yielded path lengths of up to 4 km and a noise equivalent absorption down to 4 x 10-8 cm-1Hz-1/2. The corresponding molecular concentration detection limit (e.g. for CH4, N2O and C2H2 at 1303 cm-1/7.66 Aem) was generally below 1 x 1010 cm-3 for 1 s integration times and one order of magnitude less for 30 s integration times. The main limiting factor for achieving even higher sensitivity is the residual mode noise of the cavity. Employing a 0.5 m long cavity the achieved sensitivity was good enough for the selective measurement of trace atmospheric constituents at 2.2 mbar.
Book Synopsis Plasma Diagnostics and Spectroscopy Using Tuneable IR Diode Lasers by : W. Y. Fan
Download or read book Plasma Diagnostics and Spectroscopy Using Tuneable IR Diode Lasers written by W. Y. Fan and published by . This book was released on 1998 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Introduction to Complex Plasmas by : Michael Bonitz
Download or read book Introduction to Complex Plasmas written by Michael Bonitz and published by Springer Science & Business Media. This book was released on 2010-07-29 with total page 451 pages. Available in PDF, EPUB and Kindle. Book excerpt: Complex plasmas differ from traditional plasmas in many ways: these are low-temperature high pressure systems containing nanometer to micrometer size particles which may be highly charged and strongly interacting. The particles may be chemically reacting or be in contact with solid surfaces, and the electrons may show quantum behaviour. These interesting properties have led to many applications of complex plasmas in technology, medicine and science. Yet complex plasmas are extremely complicated, both experimentally and theoretically, and require a variety of new approaches which go beyond standard plasma physics courses. This book fills this gap presenting an introduction to theory, experiment and computer simulation in this field. Based on tutorial lectures at a very successful recent Summer Institute, the presentation is ideally suited for graduate students, plasma physicists and experienced undergraduates.
Book Synopsis Plasma Diagnostics with Semiconductor Lasers Using Fluorescence and Absorption Spectroscopy by : Douglas Steven Baer
Download or read book Plasma Diagnostics with Semiconductor Lasers Using Fluorescence and Absorption Spectroscopy written by Douglas Steven Baer and published by . This book was released on 1993 with total page 388 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Absorption Spectroscopy Studies in Low Pressure Non Equilibrium Molecular Plasmas Using Tunable Infrared Diode Lasers by : Frank Hempel
Download or read book Absorption Spectroscopy Studies in Low Pressure Non Equilibrium Molecular Plasmas Using Tunable Infrared Diode Lasers written by Frank Hempel and published by . This book was released on 2003 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Tunable infrared diode laser absorption spectroscopy (TDLAS) has been applied to investigate the chemical kinetics in reactive discharges. It was used to detect the methyl radical and nine stable molecules, CH4, CH3OH, C2H2, C2H4, C2H6, NH3, HCN, CH2O and C2N2, in H2-Ar-N2 microwave plasmas containing up to 7.2 % of methane or methanol, under both flowing and static conditions. The degree of dissociation of the hydrocarbon precursor molecules varied between 20 and 97 %. The methyl radical concentration was found to be in the range 1012 to 1013 molecules cm-3. By analysing the temporal development of molecular concentrations under static conditions it was found that HCN and NH3 are the final products of plasma chemical conversion. The fragmentation rates of methane and methanol and the respective conversion rates to methane, hydrogen cyanide and ammonia have been determined for different hydrogen to nitrogen concentration ratios. An extensive model of the chemical reactions involved in the H2-N2-Ar-CH4 plasma has been developed. Model calculations were performed by including 22 species, 145 chemical reactions and appropriate electron impact dissociation rate coefficients. The results of the model calculations showed satisfactory agreement between calculated and measured concentrations. The most likely main chemical pathways involved in these plasmas are discussed and an appropriate reaction scheme is proposed. Based on the model calculations the concentrations of non-measured species like CH2 or NH2 have been predicted.In addition, spectroscopic investigations of P- and R-branch lines of the fundamental bands of 12C14N and 13C14N in their ground electronic state have been performed at high resolution by tunable diode laser absorption spectroscopy. The radicals were generated in microwave plasmas containing methane with varying proportions of N2 and H2. From a fit to the spectra the origins of the fundamental bands of the two isotopomers were determined to be 2042.42104(84) cm-1 and 2000.08470(30) cm-1. The main product detected in the plasma was HCN. It showed concentrations which are about three orders of magnitude higher than that of CN.Moreover, the time and spatial dependence of the chemical conversion of CO2 to CO were studied in a closed glow discharge reactor (p = 50 Pa, I = 2 and 30 mA) consisting of a small plasma zone and an extended stationary afterglow. Tunable infrared diode laser absorption spectroscopy has been applied to determine the absolute ground state concentrations of CO and CO2. After a certain discharge time the concentrations of both species were observed to come into equilibrium. The spatial dependence of the equilibrium CO concentration in the afterglow was found to vary by less than 10 %. The feed gas was converted to CO more predominantly between 45 % and 60 % with increasing discharge current. The formation time of the stable gas composition decreased with increasing current too. For currents higher than 10 mA the conversion rate of CO2 to CO was estimated to be 1 x 1013 molecules J-1. Based on the experimental results a model of the CO2 conversion chemistry has also been established for this type of discharge. The calculated and measured temporal developments of species concentrations showed a satisfactory agreement for various discharge currents.Lastly, infrared tunable diode laser absorption spectroscopy has been used to analyse the fragmentation of TiCl4 into HCl in pulsed H2-Ar-N2 dc plasmas (p= 2 mbar). At small TiCl4 admixtures (0.04-0.31 %) HCl concentrations of 2-5 x 1014 molecules cm-3 were measured (current density: 0.6-1.15 mA cm2). A nearly complete conversion of Cl into HCl was found at TiCl4 admixtures below 0.2 %.
Book Synopsis Scientific and Technical Aerospace Reports by :
Download or read book Scientific and Technical Aerospace Reports written by and published by . This book was released on 1995 with total page 994 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Laser Processing and Analysis of Materials by : Walter W. Duley
Download or read book Laser Processing and Analysis of Materials written by Walter W. Duley and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 449 pages. Available in PDF, EPUB and Kindle. Book excerpt: It has often been said that the laser is a solution searching for a problem. The rapid development of laser technology over the past dozen years has led to the availability of reliable, industrially rated laser sources with a wide variety of output characteristics. This, in turn, has resulted in new laser applications as the laser becomes a familiar processing and analytical tool. The field of materials science, in particular, has become a fertile one for new laser applications. Laser annealing, alloying, cladding, and heat treating were all but unknown 10 years ago. Today, each is a separate, dynamic field of research activity with many of the early laboratory experiments resulting in the development of new industrial processing techniques using laser technology. Ten years ago, chemical processing was in its infancy awaiting, primarily, the development of reliable tunable laser sources. Now, with tunability over the entire spectrum from the vacuum ultraviolet to the far infrared, photo chemistry is undergoing revolutionary changes with several proven and many promising commercial laser processing operations as the result. The ability of laser sources to project a probing beam of light into remote or hostile environments has led to the development of a wide variety of new analytical techniques in environmental and laboratory analysis. Many of these are reviewed in this book.
Book Synopsis ERDA Energy Research Abstracts by : United States. Energy Research and Development Administration
Download or read book ERDA Energy Research Abstracts written by United States. Energy Research and Development Administration and published by . This book was released on 1977 with total page 1072 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Nonthermal Plasma Chemistry and Physics by : Jurgen Meichsner
Download or read book Nonthermal Plasma Chemistry and Physics written by Jurgen Meichsner and published by CRC Press. This book was released on 2012-11-13 with total page 566 pages. Available in PDF, EPUB and Kindle. Book excerpt: In addition to introducing the basics of plasma physics, Nonthermal Plasma Chemistry and Physics is a comprehensive presentation of recent developments in the rapidly growing field of nonthermal plasma chemistry. The book offers a detailed discussion of the fundamentals of plasma chemical reactions and modeling, nonthermal plasma sources, relevant diagnostic techniques, and selected applications. Elucidating interconnections and trends, the book focuses on basic principles and illustrations across a broad field of applications. Expert contributors address environmental aspects of plasma chemistry. The book also includes selected plasma conditions and specific applications in volume plasma chemistry and treatment of material surfaces such as plasma etching in microelectronics, chemical modification of polymer surfaces and deposition of functional thin films. Designed for students of plasma physics, Nonthermal Plasma Chemistry and Physics is a concise resource also for specialists in this and related fields of research.
Book Synopsis Infrared Diode Laser Absorption Spectroscopy Measurement of Gas Phase Radicals in C4F Discharges for Plasma Model Validation by : Karla Waters
Download or read book Infrared Diode Laser Absorption Spectroscopy Measurement of Gas Phase Radicals in C4F Discharges for Plasma Model Validation written by Karla Waters and published by . This book was released on 2000 with total page 214 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Diamond Films Handbook by : Jes Asmussen
Download or read book Diamond Films Handbook written by Jes Asmussen and published by CRC Press. This book was released on 2002-01-23 with total page 658 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Diamond Films Handbook is an important source of information for readers involved in the new diamond film technology, emphasizing synthesis technologies and diamond film applications. Containing over 1600 references, drawings, photographs, micrographs, equations, and tables, and contributions by experts from both industry and academia, it includes specific chapters that address film characterization methods and the physics and chemistry of film synthesis. Other topics include deposition chemistry, various techniques for diamond synthesis, diamond heat spreaders, thermal management diamond active electronic devices, and diamond film optics.
Download or read book Energy Research Abstracts written by and published by . This book was released on 1990 with total page 852 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Laser Spectroscopy and Laser Imaging by : Helmut H. Telle
Download or read book Laser Spectroscopy and Laser Imaging written by Helmut H. Telle and published by CRC Press. This book was released on 2018-04-17 with total page 1292 pages. Available in PDF, EPUB and Kindle. Book excerpt: "a very valuable book for graduate students and researchers in the field of Laser Spectroscopy, which I can fully recommend" —Wolfgang Demtröder, Kaiserslautern University of Technology How would it be possible to provide a coherent picture of this field given all the techniques available today? The authors have taken on this daunting task in this impressive, groundbreaking text. Readers will benefit from the broad overview of basic concepts, focusing on practical scientific and real-life applications of laser spectroscopic analysis and imaging. Chapters follow a consistent structure, beginning with a succinct summary of key principles and concepts, followed by an overview of applications, advantages and pitfalls, and finally a brief discussion of seminal advances and current developments. The examples used in this text span physics and chemistry to environmental science, biology, and medicine. Focuses on practical use in the laboratory and real-world applications Covers the basic concepts, common experimental setups Highlights advantages and caveats of the techniques Concludes each chapter with a snapshot of cutting-edge advances This book is appropriate for anyone in the physical sciences, biology, or medicine looking for an introduction to laser spectroscopic and imaging methodologies. Helmut H. Telle is a full professor at the Instituto Pluridisciplinar, Universidad Complutense de Madrid, Spain. Ángel González Ureña is head of the Department of Molecular Beams and Lasers, Instituto Pluridisciplinar, Universidad Complutense de Madrid, Spain.
Book Synopsis Wavelength Modulated Infrared Diode Laser Absorption Spectroscopy of Fluorocarbon Species in a Low-pressure High-density Plasma Reactor by : Michael Eugene Littau
Download or read book Wavelength Modulated Infrared Diode Laser Absorption Spectroscopy of Fluorocarbon Species in a Low-pressure High-density Plasma Reactor written by Michael Eugene Littau and published by . This book was released on 1998 with total page 458 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Plasma Spectroscopy by : Takashi Fujimoto
Download or read book Plasma Spectroscopy written by Takashi Fujimoto and published by Clarendon Press. This book was released on 2004-06-17 with total page 300 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book focuses on the characteristics of optical radiation, or a spectrum, emitted by various plasmas. In plasma, the same atomic species can produce quite different spectra, or colours, depending on the nature of the plasma. This book gives a theoretical framework by which a particular spectrum can be interpreted correctly and coherently. The uniqueness of the book lies in its comprehensive treatment of the intensity distribution of spectral lines and the population density distribution among the atomic levels in plasmas. It is intended to provide beginners with a good perspective of the field, laying out the physics in an extremely clear manner and starting from an elementary level. A useful feature of the book is the asterisked sections and chapters which can be skipped by readers who only wish to gain a quick and basic introduction to plasma spectroscopy. It will also be useful to researchers working actively in the field, acting as a guide for carrying out experiments and interpreting experimental observations.
Book Synopsis Volatile Organic Compound Analysis in Biomedical Diagnosis Applications by : Raquel Cumeras
Download or read book Volatile Organic Compound Analysis in Biomedical Diagnosis Applications written by Raquel Cumeras and published by CRC Press. This book was released on 2018-11-09 with total page 201 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume presents a thought-provoking state-of-the-art picture of how volatile compounds are used in metabolomics, currently a hot topic in the metabolomics field. It provides a thorough description of what volatile organic compounds (VOCs) are, why they are important in biomedicine, and what the analytical platforms are used. It also looks at multivariate analysis and databases needs. Because VOCs are end-up compounds of metabolic processes, volatiles can be linked to different diseases or pathologies for both diagnosis and prognosis. The authors provide authoritative information and guidance on the analytical and statistical techniques used and how to identify, and they review the main current areas of application, which include breath metabolomics, cancer diagnosis, and microbial volatiles. Key Features: Presents a thorough overview of volatile research in biomedical applications Examines both gold standard techniques (metabolomics based) and artificial olfactory systems Reviews all aspects of volatile metabolites in biomedicine research, from origin to detection platforms Describes relevant diseases diagnosis and prognosis achievements, including cancer
