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Synthesis And Characterization Of Novel Lithium Ion Battery Cathode Materials Produced Via Assisted Soft Chemistry
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Book Synopsis Synthesis and Characterization of Novel Lithium Ion Battery Cathode Materials Produced Via Assisted Soft Chemistry by : Jason Rogers Brown
Download or read book Synthesis and Characterization of Novel Lithium Ion Battery Cathode Materials Produced Via Assisted Soft Chemistry written by Jason Rogers Brown and published by . This book was released on 2002 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis and Electrochemical Characterization of Novel Electroactive Materials for Lithium-ion Batteries by : Karl Joseph Kreder (III)
Download or read book Synthesis and Electrochemical Characterization of Novel Electroactive Materials for Lithium-ion Batteries written by Karl Joseph Kreder (III) and published by . This book was released on 2017 with total page 254 pages. Available in PDF, EPUB and Kindle. Book excerpt: Lithium-ion batteries (LIBs) have become ubiquitous as energy storage devices for mobile electronics, electric vehicles, and are beginning to be used for electric grid-scale energy storage. Lithium-ion batteries offer higher efficiencies, energy density, and longer life compared to incumbent technologies such as lead-acid and nickel metal hydride. Applications in which LIBs are used are continuing to demand better performing batteries at lower cost, which requires improvement in electroactive materials. This dissertation investigates the low temperature synthesis and modification of LiCoPO4 as a potential high-voltage and therefore higher energy density polyanion cathode material for LIBs, as well as a new class of interdigitated metal foil anodes which promises to be an inexpensive, higher energy density, alternative to graphite. Chapter 1 is a brief introduction to lithium-ion batteries and the principle of operation of intercalation type electrochemical energy storage devices. The components of lithium ion batteries are introduced, specifically the anode, cathode, separator, and electrolyte. Some of the shortfalls of the current technologies are discussed and areas of research interest are highlighted. Chapter 2 is a brief overview of the various experimental methods that are generally applicable to more than one of the subsequent chapters. Methods which are specific to a given study are discussed in their respective chapters. Chapter 3 presents work on the low temperature microwave-assisted solovthermal synthesis (MW-ST) of three unique polymorphs of LiCoPO4, specifically the polymorphs belonging to the Pnma, Cmcm, and Pn21a space groups. Prior to this work, only the Pnma polymorph had been reported via MW-ST method, and electrochemistry had not yet been reported for either the Pn21a or Cmcm polymorph. The dependence of the polymorphs on both the water content, and ammonium hydroxide content of the solvent was shown. Although, the electrochemistry of both the Pn21a and Cmcm polymorphs was found to be inferior to the Pnma polymorph, the ability to synthesize phase pure materials was crucial to conducting the work presented in chapters 4 and 5. Chapter 4 presents the aliovalent substitution of V3+ for Co2+ in LiCoPO4 via a low-temperature MW-ST process. Substitution of up to 7% vanadium for cobalt was demonstrated and verified by changes in the lattice parameters with vanadium content. Both the ionic and electronic conductivity of LiCoPO4 was enhanced with increasing vanadium substitution, which was attributed to the introduction of both charge carriers as well as inter-tunnel cobalt vacancies. Finally, the first cycle capacity was enhanced (from 69 mAh/g to 115 mAh/g) as well as the capacity retention over cycling. Chapter 5 demonstrates a novel technique of MW-ST assisted coating of a thin (2-5nm) conformal coating of LiFePO4 on vanadium substituted LiCoPO4. Although the vanadium substitution was able to independently increase the performance of LiCoPO4, the materials still suffers from severe side reactions with the electrolyte. The coating of LiFePO4 effectively raises the Fermi energy of the cathode material above the high occupied molecular orbital (HOMO) of the electrolyte preventing side reactions and increase the coulombic efficiency to nearly 100%. Chapter 6 introduces a novel method of producing high surface area, electrically conductive, metal nanofoams via a MW-ST process. Nickel, copper, and silver metal nanofoams are made via an inexpensive yet scalable process whereby metal acetates are reduced by polyglycol under microwave irradiation. The nanofoams were characterized via BET, SEM, XRD, EDS, and TEM. The nanofoams have potential uses in many clean energy applications, particularly lithium-ion batteries. Chapter 7 introduces a new framework for making a new class of high capacity, low-cost alloying anodes for lithium ion batteries. A novel interdigitated metal foil anode (IMFA) in which a nanosized active material, such as tin, is interdigitated with an electrically conductive matrix, such as aluminum, is presented. The foils are formed by the rolling of a eutectic Al-Sn alloy into a foil, which is an extremely cheap and scalable process. The anodes demonstrate an approximately 70% increase in capacity compared to graphite over 100 cycles, at reasonably fast rates (C/5), and high coulombic efficiency (>99%). Finally, Chapter 8 gives a brief overview of the results of the prior work and proposes areas for future research
Book Synopsis Dodicesimo censimento generale della popolazione by :
Download or read book Dodicesimo censimento generale della popolazione written by and published by . This book was released on 1985 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis and Characterization of Novel Electrode Materials for Lithium Ion Batteries by : Ruigang Zhang
Download or read book Synthesis and Characterization of Novel Electrode Materials for Lithium Ion Batteries written by Ruigang Zhang and published by . This book was released on 2011 with total page 482 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis and Characterization of Lini0. 6mn0. 35co0. 05o2 and Li2fesio4/C As Electrodes for Rechargeable Lithium Ion Battery by : Pengda Hong
Download or read book Synthesis and Characterization of Lini0. 6mn0. 35co0. 05o2 and Li2fesio4/C As Electrodes for Rechargeable Lithium Ion Battery written by Pengda Hong and published by . This book was released on 2017-01-26 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This dissertation, "Synthesis and characterization of LiNi0.6Mn0.35Co0.05O2 and Li2FeSiO4/C as electrodes for rechargeable lithium ion battery" by Pengda, Hong, 洪鹏达, was obtained from The University of Hong Kong (Pokfulam, Hong Kong) and is being sold pursuant to Creative Commons: Attribution 3.0 Hong Kong License. The content of this dissertation has not been altered in any way. We have altered the formatting in order to facilitate the ease of printing and reading of the dissertation. All rights not granted by the above license are retained by the author. Abstract: The rechargeable lithium ion batteries (LIB) are playing increasingly important roles in powering portal commercial electronic devices. They are also the potential power sources of electric mobile vehicles. The first kind of the cathode materials, LiXCoO2, was commercialized by Sony Company in 1980s, and it is still widely used today in LIB. However, the high cost of cobalt source, its environmental unfriendliness and the safety issue of LiXCoO2 have hindered its widespread usage today. Searching for alternative cathode materials with low cost of the precursors, being environmentally benign and more stable in usage has become a hot topic in LIB research and development. In the first part of this study, lithium nickel manganese cobalt oxide (LiNi0.6Mn0.35Co0.05O2) is studied as the electrode. The materials are synthesized at high temperatures by solid state reaction method. The effect of synthesis temperature on the electrochemical performance is investigated, where characterizations by, for example, X-ray diffraction (XRD) and scanning electron microscopy (SEM), for particle size distribution, specific surface area, and charge-discharge property, are done over samples prepared at different conditions for comparison. The electrochemical tests of the rechargeable Li ion batteries using LiNi0.6Mn0.35Co0.05 cathode prepared at optimum conditions are carried out in various voltage ranges, at different discharge rates and at high temperature. In another set of experiments, the material is adopted as anode with lithium foil as the cathode, and its capacitance is tested. In the second part of this study, the iron based cathode material is investigated. Lithium iron orthosilicate with carbon coating is synthesized at 700℃ by solid state reaction, which is assisted by high energy ball milling. Characterizations are done for discharge capacities of the samples with different carbon weight ratio coatings. DOI: 10.5353/th_b4715029 Subjects: Lithium ion batteries Cathodes Lithium compounds - Synthesis Cobalt compounds - Synthesis Manganese compounds - Synthesis Silicon compounds - Synthesis Iron compounds - Synthesis
Book Synopsis Synthesis and Characterization of LiFeSO4F as Novel Cathode Material for Lithium-ion Batteries by : Leiting Zhang
Download or read book Synthesis and Characterization of LiFeSO4F as Novel Cathode Material for Lithium-ion Batteries written by Leiting Zhang and published by . This book was released on 2014 with total page 93 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis and Characterization of Novel Cathodes and Electrolytes for Lithium-ion Batteries by : Chang Woo Lee
Download or read book Synthesis and Characterization of Novel Cathodes and Electrolytes for Lithium-ion Batteries written by Chang Woo Lee and published by . This book was released on 2003 with total page 314 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Novel Decavanadate Compounds for Lithium-Ion Batteries by : Simon Greiner
Download or read book Novel Decavanadate Compounds for Lithium-Ion Batteries written by Simon Greiner and published by Springer Nature. This book was released on 2020-01-02 with total page 107 pages. Available in PDF, EPUB and Kindle. Book excerpt: Simon Greiner investigates the molecular-level stabilization of polyoxovanadate (POV) compounds by rational design for the application as active cathode material in lithium-ion batteries. Formation of a complex hydrogen-bonding network locks the POVs in place and prevents thermal decomposition during electrode fabrication. The molecular vanadium oxide clusters can be electrochemically analyzed and show promising results for storage of multiple electrons per cluster, making these materials highly attractive for energy storage applications. Analytical methods comprise ATR-FTIR, powder and single-crystal XRD, electron microscopy, EDX, electrochemical analysis and battery testing.
Book Synopsis The Synthesis and Characterization of Novel Materials for Use in Secondary Lithium-ion Batteries by : Richard L. Nafshun
Download or read book The Synthesis and Characterization of Novel Materials for Use in Secondary Lithium-ion Batteries written by Richard L. Nafshun and published by . This book was released on 1996 with total page 414 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis and Characterization of Carbon Nanotube Modified Electrode Materials for Li-ion Batteries by :
Download or read book Synthesis and Characterization of Carbon Nanotube Modified Electrode Materials for Li-ion Batteries written by and published by . This book was released on 2009 with total page 418 pages. Available in PDF, EPUB and Kindle. Book excerpt: Today, the Lithium ion (Li-ion) is the fastest growing and most promising rechargeable battery chemistry. For high current demands, there is an emphasis on the importance of very low cell resistance to allow unrestricted flow of current. The electrochemical performance of Li-ion batteries relies significantly on the properties of the cathode materials, the anode materials and the electrolytes. In this study, novel anode and cathode materials were synthesized and systematically studied for Li-ion battery application. Novel anode synthesis involved the substitution of the flat foil current collectors normally used by nano- or micro-wire arrays, as the higher surface area makes it possible to pack much more active material into an electrode. Ni or Cu wire arrays with wire thicknesses of 200 nm, 400 nm or 1 \03BCm were synthesised. Carbon nanotubes (CNTs) were chosen as the Li-insertion compound due to its high theoretical reversible lithium storage capacity. Synthesis of the Cu or Ni/CNT consolidated composite anodes were done using novel synthetic techniques, combining template synthesis via electrochemical deposition and chemical vapour deposition (CVD) techniques. XRD analysis of both the Ni and Cu wire arrays after carbon nanotube deposition, confirmed that the crystallinity of the wire arrays were not altered by the CVD of carbon nanotubes. The optimal results were obtained for the 200 nm Cu/CNT consolidated composite anode. The current density obtained for the Li de-intercalation (\03AFp) was 0.463 A/g. A reversible discharge capacity of 358 mAh/g was obtained in the subsequent charge/discharge cycling. The composite anode materials showed good charge/discharge cycling performances and a high capacity integrity was maintained in the cycling behaviour analyses.
Book Synopsis Lithium Process Chemistry by : Alexandre Chagnes
Download or read book Lithium Process Chemistry written by Alexandre Chagnes and published by Elsevier. This book was released on 2015-06-14 with total page 313 pages. Available in PDF, EPUB and Kindle. Book excerpt: Lithium Process Chemistry: Resources, Extraction, Batteries and Recycling presents, for the first time, the most recent developments and state-of-the-art of lithium production, lithium-ion batteries, and their recycling. The book provides fundamental and theoretical knowledge on hydrometallurgy and electrochemistry in lithium-ion batteries, including terminology related to these two fields. It is of particular interest to electrochemists who usually have no knowledge in hydrometallurgy and hydrometallurgists not familiar with electrochemistry applied to Li-ion batteries. It is also useful for both teachers and students, presenting an overview on Li production, Li-ion battery technologies, and lithium battery recycling processes that is accompanied by numerous graphical presentations of different battery systems and their electrochemical performances. The book represents the first time that hydrometallurgy and electrochemistry on lithium-ion batteries are assembled in one unique source. Provides fundamental and theoretical knowledge on hydrometallurgy and electrochemistry in lithium-ion batteries Represents the first time that hydrometallurgy and electrochemistry on lithium-ion batteries are assembled in one unique source. Ideal for both electrochemists who usually have no knowledge in hydrometallurgy and hydrometallurgists not familiar with electrochemistry applied to Li-ion batteries Presents recent developments, as well as challenges in lithium production and lithium-ion battery technologies and their recycling Covers examples of Li processes production with schematics, also including numerous graphical presentations of different battery systems and their electrochemical performances
Book Synopsis Materials for Lithium-Ion Batteries by : Christian Julien
Download or read book Materials for Lithium-Ion Batteries written by Christian Julien and published by Springer Science & Business Media. This book was released on 2000-10-31 with total page 658 pages. Available in PDF, EPUB and Kindle. Book excerpt: A lithium-ion battery comprises essentially three components: two intercalation compounds as positive and negative electrodes, separated by an ionic-electronic electrolyte. Each component is discussed in sufficient detail to give the practising engineer an understanding of the subject, providing guidance on the selection of suitable materials in actual applications. Each topic covered is written by an expert, reflecting many years of experience in research and applications. Each topic is provided with an extensive list of references, allowing easy access to further information. Readership: Research students and engineers seeking an expert review. Graduate courses in electrical drives can also be designed around the book by selecting sections for discussion. The coverage and treatment make the book indispensable for the lithium battery community.
Book Synopsis Synthesis and Characterization of Novel Cathode Material with Improved Specific Capacity and Safety for Lithium Ion Batteries by : Wassima El Mofid
Download or read book Synthesis and Characterization of Novel Cathode Material with Improved Specific Capacity and Safety for Lithium Ion Batteries written by Wassima El Mofid and published by . This book was released on 2016 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Die steigenden Anforderungen an Lithium-Ionen-Batterien mit hoher spezifischer Leistung und Energie haben zur Entwicklung von mehreren Klassen von Materialien für die positive Elektrode geführt. Darunter sind unter anderem die vielversprechenden LiNixMnyCo1-x-yO2 (NMC) Materialien. In diesem Zusammenhang ist das Thema dieser Arbeit eine umfangreichen Studie der elektrochemischen und strukturellen Eigenschaften des ursprünglichen Materials NMC (3:1:1) (LiNi0.6Mn0.2Co0.2O2) und der drei neuen Materialien, die entweder durch Mono-Substitution von Co mit Al oder Fe: NMCA (LiNi0.6Mn0.2Co0.15Al0.05O2) und NMCF (LiNi0.6Mn0.2Co0.15Fe0.05O2) oder durch doppelte Substitution von Co mit Al und Fe NMCAF (LiNi0.6Mn0.2Co0.15Al0.025 Fe0.025O2) hergestellt wurden. Im ersten Schritt wurde eine Optimierung der Synthesebedingungen durchgeführt. Dazu wurden verschiedene Verfahren (z.B. Röntgenbeugung, Rasterelektronenmikroskopie) verwendet, um homogene Phasen mit gut geordneter Struktur zu erhalten. Im zweiten Schritt wurden Struktur, morphologische und elektrochemische Eigenschaften der vier Materialien untersucht. Eine detailliertere Untersuchung wurde NMCAF gewidmet. Dieses Material zeigte die besten elektrochemischen Eigenschaften im Vergleich zu den ursprünglichen und den mono-substituierten Materialien. Ziel ist es zu verstehen, was die Mechanismen hinter der Verbesserung des elektrochemischen Verhaltens des doppelsubstituierten Materials sind. Schließlich wurde der Sicherheitsaspekt von NMCAF auf Basis einer detaillierten Untersuchung der thermischen Stabilität während der Lithium-Ionen-Deinterkalation diskutiert.
Book Synopsis Hydrothermal Synthesis and Characterization of Vanadyl Phosphate Based Cathode Materials for Lithium Ion Batteries by : Youngmin Chung
Download or read book Hydrothermal Synthesis and Characterization of Vanadyl Phosphate Based Cathode Materials for Lithium Ion Batteries written by Youngmin Chung and published by . This book was released on 2016 with total page 159 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis and Characterization of Vanadium-based Cathode Materials for Lithium Ion Batteries by : 李航空
Download or read book Synthesis and Characterization of Vanadium-based Cathode Materials for Lithium Ion Batteries written by 李航空 and published by . This book was released on 2018 with total page 189 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Synthesis, Characterization and Testing of Novel Anode and Cathode Materials for Li-Ion Batteries by :
Download or read book Synthesis, Characterization and Testing of Novel Anode and Cathode Materials for Li-Ion Batteries written by and published by . This book was released on 2002 with total page 35 pages. Available in PDF, EPUB and Kindle. Book excerpt: During this program we have synthesized and characterized several novel cathode and anode materials for application in Li-ion batteries. Novel synthesis routes like chemical doping, electroless deposition and sol-gel method have been used and techniques like impedance, cyclic voltammetry and charge-discharge cycling have been used to characterize these materials. Mathematical models have also been developed to fit the experimental result, thus helping in understanding the mechanisms of these materials.
Book Synopsis Design, Synthesis and Characterization of Novel Electrolytes for Lithium-ion Batteries by : Kan Luo
Download or read book Design, Synthesis and Characterization of Novel Electrolytes for Lithium-ion Batteries written by Kan Luo and published by . This book was released on 2009 with total page 244 pages. Available in PDF, EPUB and Kindle. Book excerpt:
